0 v. raw qc · 2018. 6. 19. · ai» .1 *,' • - *. 4 •onttchlorophenol rnponie, factor •...
TRANSCRIPT
0 V. RAW QCl
E.P.A. CASE NO.
•A, DfTPPBttifmet TICK 'F. Mtttnd flM SwU-VoW* (HSl) •«, HUM Spttt SunWottliPwhnninct Sunard Fom • Suragm Mcowy • SurrogM RKOVKV FormCnomMgrm ' - • TmtMniDUu • TmMMlDUMSmolrun • crrc»TW>gnm(i|/Ouinttitl«i . ctmnMognmWQwnmilonEBP moon n*S\MZUMng • MmSMdnni . MwSpKlnim
•B, WIMmncfTiM . ••UwnfSwh
OCR • ChromKognmdl/Quimiution • SungM (tooncy FomWZUMng , Btport • TMMnlOUM
•C, ChroMognprv CtMCk OtU ;H, Mtmoa Btok TCOOBmMMEICPi -• SwrogmRtcovnyFom . „_„...„PtjUcNorophtnolEICPV • Oraawgnmdi/Omntiutm . UbnyStnti
PwtomwctSWnoWdFoim '* Mtltwa B«* Ptwa* |M8l| -L OuplcM MM* Soft* Sw*SoKtm ., • SuragiH RKomy Forni V«M*
CoUimCnte* ., u-...«». VOA IHSU 'nunt iini i MWtt 8(*t VOA |HSl) . Sumgn, Ricoytiy FomMm(H9M • SwragMRwovwyForni • TtfMMIDIMTMMMlDUd • Clnimilognni|i|/QuMIMon fXaaCrnmngrmlil/QuMllillon . Htport ___ . Mm Omanim•f SpKtfunt"I'8'"01 'J, Oup(K!lttMKl1«S|l(MVOA|MSl)
•E. MMTMBMVOAIMSII • SuragM Rtconry FormSURMM Rtoonn • TfnMMIDLW
:fflwaru«,1£S" -utayawm .o.s Pr iion^ « QOFIO
• OCScmnDM•Stqunct rtpMKl •
The Items deUveraMt under Manka and matrix spikes and duplicate matrix spikes sectionshave been described In similar sections ol the Indexed tabs lor the samples. % Recoveryand RPD criteria era described m the Summary, Section II.C. Blank criteria applied are asfollows, from Exhibit E, page 8-9 ol 63:II an HSL compound la detected In the blank, the blank value Is utilized In the calculation otthe sample according to the following options, Results of reagent blank analysis sluH bereported using the Organic Analysis Data Sheet (see Exhibit B).1. It the concentration In the blank la lesa than or equal to '/• ol the method detection
Hmtt (reference Exhibit C: HSL Compounds and Method Detection Limits), the blankvalue Is Ignored,
2, If the concentration In the blank Is greater than 'A ol the method detection limit and laless than or equal to ft the concentration detected In a sample, subtract the concen-tration In the blank from the concentration In the sample, Record the corrected valueand indicate that thla has been done by placing a "C"ln the Hag column ol the datasheet,
3, II the concentration m the blank is greater than 'A ol the method detection limit and IIthe blank concentration la greater than Si the concentration detected In a sample,correction la not possible and the compound should be reported as "NO" but with a, "B" In the flag column ol the data sheet. The cause of this high blank should be deter-mined and corrected before additional samples are analyzed,
o
o
014207
O
CASELON1WTEK
B
fiil
a1L70
IT1»7)ie}M
?«.1.1 ft*n
?»441
'M?443
HO. .._„,., CONTRACTOR Held ComuChtm COKIRACT MO. «B.01.67«, 68-01-68EVEL ' NED. LEVEL " HIM LEVEL
/ / OFTPP FIU NMI: £>f/*<H>i)0C>$ite: l/H#« Shift: c ""AnTITit: 73V
BfT>PIon IMniaTnei Criteria30.00 to 60.00 « of mast 1QRIMS than g.nn < pf inn g9
•>tt •• iwlitlv* ifeundinei
loss thin 2.00X of MSS 69•40.00 tov60.00 t of Hit 118loit thin 1.00* nf HIM IDA
bite otik. 100 percent1.00 to a. on t of MM ioa10 DO tA 9A fli « «» uf| 100
ortiont but loit MII thin 443groittr thin 40.0K of MM 1;:.17.00 to 23.00* of HIM 419
DfTFp IM IMJ nrToraunct miuiti:
cc
1 Thi OFTPP pirforMnu multi MTcrlterli.
] DtvlitloniBite/Tine/ Initfument Flit tlunber
. I Itlatlve Abundance
—— ( . I1
5V ' ' '———— •*•- .-.. ;. ...... ,f ^ ,2
uV •••• — • - . . - •foO5&+9/Zj.O '"• •**?'"•'* " "•'y? C 77. )3
• rovlowd ind found to be within thi iptelflid
Initmi oneRtqulrid Obitrvid
CoHovnd •/! Abundinet Abundince
• ".r . ' ••••••, .' 'V
inuiait Bite"•• ""• •* • ;-!• • JA . :•*••• ••£ it ™Nnticliloroplwml Rnponufictor. Aria 118X w •1 1loniMlM Ditoctiblo fl»oi U*°Am (Count*) 40 ng OlFAnthncene •.?;D1>miuty1 Withiliti Siturittd Q Te» __^nijurtlBt . )1iIofMii 19 ' 014208\ Flouro 1n (\, ) 1i S of MII M igu>
) It i of MII *»2 itevlslon Pitc 1/31/84,rt n p» t- .••,» "EH
? £ 82- ifl " 8H o> ip rt « «
g-tF
•8 "—————ffi.«
-8
€"&-s
:=—Xn
.
s
014209
6*.
Ȥ-
8s.
5 g * 8 8 $ *» . . T
014210
HEAP COWUCHEnDABS LIST DATA: DHB40810C19 « 762 BABE H/E: 19B02/10/84 3:19:00 + 9:31 RJC; 11776SAMPLE: 1UL DFTPP (11003) |
0,00 MINIMA MIN INTEN: 0, MAX INTEN: 1660.443 ft. 0 MAXIMAMASS X DA
30 11,2091 47,1198 a. 4797 3,79A3 8,9369 93,9974 3.89 • '"79 9,6677 43.0778 ...aAS ••:.79 8, «W 'ei 4,1693 3 7399 8,99107 14,46108 8.99110 89,34111 3.43117 9,78127 .48,89
: 188 3, BO .":
186 9,46187 3,43198 100,00199 9,46809 3,43806 18,9B807 3,07817 9 18821 4, 16224 11,39229 2,47227 4,9B244 B, 67299 39.28296 9,84.238 2,71874 3,43279 24, 16276 3,73296 4,40 ,...*„323 2,69 ; '369 3,67423 9,00441 12,09 :442 90,24
16,81\
'»• 890055 5
SEHUVOLATILE INSTRUMENT TUNE AM KRmRHANCECASE KB, _____ CONTRACTOR Meid CemuCnmi CONTRACT NO. 6B.01.67M.6B-01-6BS6LOW LEVEL "" MED. LEVEL — HliM LEVEL.MATER
D
Nm1)IB
fl°TO
P7),7
1U
}I9
ITS
f8544}
442443
n. .. OFTPP File NOM: M&f Q1J2 6/fMi T.ll'UWi Shin: /T* TniTrtt! ' 5/ / J-- - t1
OFTPPIon Aburi3i7ce Criteria30.00 to. 60.1X1 1 nf MM 1QR]»|* thin 9 00 t nf Mf } 69
•ut M Mlitlv* abundanceloss thin 2.00* of mass 6940.00 to 60.00 ( of MIS 198IMI than 1.0M nf RUM 108bin peik. 100 percentS.90 to 9.00 t of MM 108
preterit but IHI MII thin 443greater than 40.001 of nut 19817 .on to 2a.nrn of HUM U9
ittTfi1 ind IFH ferrorwncf miuiti:
cz
in
y Relative Abundance37.20— v i . }lW.TSL -m __ r . >zU.-7. C._100.00
n.s<\\4. L$1.13-7.2.?
"" . 2-C. ""10. 63 (to.T8t3
3 The DfTPP ptrfonaince rnulti wire revlwed ind found to be within thi iptdflederitir1l< fofi 7//1/TV
1 DflvlitloniDit'i/TliM/InitruMnt Flit Nuntbtr
innrais ' ' oateRequired Obterved
Coawound •/« Abundinet Abundance. Ai» .1 *,'
• - *
.
4•onttchlorophenol Rnponie, Factor • Jnttantldlne Detectable IVTOI Quo .Am (Count i) 40 ng Dl~Anthrieent • <»/OI-Mutyl Phthilite Saturated y Yit1 Mguro In (' • ) It 1 of MM 192 Fljure In ( , ) Is t of MII «S Figure In ( . ) Is % nf MM MZ
.^inuiiu TJa'tt
.•V-EI '"
)• 2b
f)j)p; 5 3 Revision Dite 1/31/84,rtn
FORM VII
Tt
X
«
? a ;s" e «
*-F ali« ' . : • " • M 9<B,r——" ' ' » ' 5 w +
I-
P
i
— SI,_., _________________ .. ___ R g
VI m
•»• 8MN>
««
MEAD COnrUCHEM/~v MASS LIST DATA; DHB40212B14 » 591 BASE I'VE; 19B•J C2/12/B4 16:32:00 * 7:23 RiC: 36736.
SfMIPLEl 1UL DFTPP 11005(7090)ON*) 14•591
41 0. 00 MINIMA . MIN INTEN: 36. MAX INTEN: 4376.478 ft 0 MAXIMA(1AS8 X RA MASS 7. RA MASS X RA MASS X RA
41 0,62 116 0.79 IBS 2,06 '279 19,6342 0,66 117 7,27 1B6 11.11 276 3,6843 1. 98 11B 0.96 187 3.84 577 1.6744 1.67 122 1,33 1B8. 0.7B 278 0,7847 0.66 123 <.:. 01 189 0.91 2B6 0.7149.. 0.71 124 0.74 1*8 1.76 893 0.79 ••'•90 10.88 129 1.10 193 1.44 296 4.6611 37,20 127 42.69 194 0.96 297 1.1992 2.61 128 3,38 196 4.43 301 0,71M 149 139 19,38 198100,00 303 07196 1,69 120 1.90 199 7.99 306 0,6397 3,72 133 0.66 200 0,64 312 0,64
A 61 0.62 134 0,66 201 1,30 319 0,916? 0, 73 139 2,29 203 1.14., . 323 2.3963 2.19 136 1.17 204 2.99 324 0,8769 1.37 137 1.69 209 4.73 327 1,0167 0.94 138 0.64 206 18,46 334 3,0669 41.22 Ul 2.93 207 Z, 74 339 0.99 '7t 0.9t' 142 I 30 201 "'I; 03 33* • -AO. 6973 0.78 143 0,87 21-0 0.66 343 0,7874 3.29 144 0,71 211 1.90 346 0.9679 6.58 U9 0.78 213 1.12 348 1,3876 2. «9 147 1.93 213 0.79 392 1,3977 39. '0 14B 2, 33 217 4Y79 393 0. 7178 3. VQ 149 1.44 218 1.39 394 1.4979 2,81 151 0,94 221 8.73 398 0,7880 2,31 153 0,99 223 1.33 365 2,2981 3.86 193 1.17 224 10.93 366 1 01B? 1.99 194 091 229 3,24 371 0,6483 1,37 199 1,71 227 4.62 372 1.4404 0.82 156 2,03 228 0,79 373 0.7389 1.09 197 0,66- .-229 1,*7 374 0.7186 1,09 -15B 0,73 231 1.99 383 0.78*88 0,59 199 0.79 239 0,71 390 1.07-91 1,28 160 1.69 237 0,91 402 0,6992 1.17 161 1,69 243 1,71 403 1,0993 4.78 169 1.37 944 B. 29 ..417 0.9996 0.69 " 166 0.96 249 2,01 421 0.9897 0.66 167 4.41 '" '24eY" I.BB •...•-"• •4»'"-4.14 '98 2,99 168 3,90 247 0,69 '424 1.1099 3 94 ' 16? 0, 99 249 0,82 429 0.64101 2.08 172 0. 89 299 40, OB 439 0,71103 0.96 174 1,49 296 6.08 441 7.27104 1,21 179 1.37 298 3,27 448 48,26109 1.9B 176 0,96 260 0,99 443 10,03107 12,02 V l77 »• »4 264 0,64 444 1.46 014215108 2.96 179 3,09 269 1,21 468 0,37110 27,01 180 2,39 266 0,91 473 0,78111 4 97 181 1.49 273 1.76 ••• 479 0.79 OnffKO112 1,12 184 1, 19 274 4,00 b, « •!••!.t/M
SEH1-VOLAT1LE INSTRUMENT TUNE AND PERFORMANCE
CASE NO. ______ CONTRACTOR Maid'careuCne* CONTRACT NO. 6B-01.67<2.68-01-6666LOM LEVEL HP. LEVEL H1BH LtVELWTER . S01L/SED. "~~""~"~; OTHER BoielM
/ / OFTPP File NOM: _ ______Dite: z//7/rV SMtt: c. Jlnimt;
MmSI
M
It70
IFIf7in1(9
|7Ban44V442
443
PFTPPIon Abumlinci Criteria30.00 to. 60.00 1 nf matt 1<W
IM« thin g.nn < nf •»«*•" KO
•u| n pclitlw* akundinealoss thin 2.0M of MSI 6940.00 to 60.00 t Of MM 198lut than 1.0M of mitt 100.
ban peik. 100 percent1.00 to 9.00 < of IMM 1BB
10 00 *« M IM « nf .... 100
4lEUlir_thin LOOT of eiaia 19Boroient but Ini MII thin 443greiter thin 40. OW of mm 19817. on to 23. not of RUM U9
Jljtelatlve AbundanceS7.»rt
«—»,,*„. ( . rS1.9J!*""" ( . 1*srz ...,,...——/99££926.353.'¥/Q.S4
PrTrP ind irB rertominee miuitt;Thi OFTPP perforiince rotuUi wire reviewed ind found to be within the specifiedcriteria. . .1LA-
initials DateOtvlitloni Required ObiervedBite/TWlnitrument File Nunrber Coioound mtt Abundance Abundance
"' 40fontKhloroohenol Ruponii ictor • Area IN I
I! lonildlM Doteetiblo mei QM11 Arei (Counts) 40 ng DirAnthricene • "
D1-N-»ut»1 Phthilite Saturated [3 Yi
initiaii oate
»ri9ure1n( . )1i»of«i 192F1»ure1n( . )1sSofMssll3 Mour, in I , )U»of«««Z
u-i
8::.g
a————————35
*———*Pea!>8 g«s
0* M «H *•
8-~ ?8
••a
M
H— -a
i
,* -
jp,—s J01 17
003541 M
0 » s i 8 • 5 ? 5J
dmm..m™
oca•• Lfl
0« •|gjIs
5) w
HEAD COWUCHEnLIST DATA: PN84021$C19 ft 737 BABE M/E: 198
0"S713/B4 0:51:00+ 9:13 I RIG: 16928.SAMPLE; 1UL DFTPP (11009)
90 0,00 MINIMA MIN INTEN: 0, MAX INTEN: 2136.443 ft 0 MAXIMAMASS X RA MASS X RA
90 14.98 323 2.3991 97.49 369 3.1497 9.29 423 9.7663 2.67 441 10.8669 67.98 442 79,1274 4.87 443 14.1479 9.6976 3.2877 98.4378 3,1479 3.5680 3,1481 3.9393 3.9898 3.0999 4.40107 16.97110 32.9111 4.7B , ,.17 8.78 """' ""•'127 91.78128 4.03129 IB. 31139 2.43141 2.62167 3,37168 2.90 •179 2.90186 11,99187 3.98196 2,90198 100.00199 6,69204 .3.28209 4,92206 17,23207 3.28 .217 3.96 ...221 .440 • "'• " ' '•••'"•' • ~~ .224 11.14 .229 2.86227 4,12 ' '244 7,72246 • 3,09J99 41,90
°14213279 20,99276 2,39 -- ., * „ I277 2,90 ' P 89296 9,97 > i
SEHLVOUTILE INSTRUMENT TUNE AND PERFORMANCE
CASE NO. ______ CONTRACTOR Held CaamuChun CONTRACT NO. tfl.01.67«. 68-01 -6866LOM LEVEL "" P£0. LEVEL HZZZZI HIW UVEL __
- SOILED, ZZZZZ WHER (Specify)OFTPP File Netrii
Bite: 2.-W.-flV Shltt: &• 'AnalTtt! "76 3
HailSIM
«o70
J27J97
198inI7S
MS441
442443
DFTPPIon AbunfirTce Criteria30. 00 to 60.00 t nf mitt 1QR
IMS »h«n g.np | of |«MS 69
•u f<) nlitlv* abundinetloss thin 2.00* of mils 6940.00 to 60.00 * Of MM 198' •last thin l.fMK nf na« 10B
bin oeik. 100 percent1.00 to 9.00 t nf IM*C lOfi
10 no *« an nn * n* •!•• too
jttuier than i-00* °f "wsJSL.preient but leii MII thin 443groitor then 40.001 of nut 19817 .00 ta 23. tint of mice 449
» Relative Abundancetr/i .*.-.'r*ww { '. i1U-.,. .,*' ( m ,z
r t^ <|M.'
/00
k,1.
It.i
2.7. 1.1 ...-. '.•s.liLf.-*1!*!!***'*- '*»««••
»? ( - )3
DFTrP ind BFB perTenainee miulti;Thi DFTPP perfomanci rnuUi Mere revlewid end found to bt within the iptdfledcriteria.
initials BiteDavlitlont Required ObservedBite/Hin/'lnttrmnent File Number Coroound •/» Abundinee Abundance
r-jultl" • « ..;:.;'!3j_. -;, i—*»_ "PO* no. I .,•entechlorepnenol Aeiponie,Fictor • Am IN X M • ('<»lenildlneDetectible Rlei Quo ——Am (Counts) 40 ng DltrAnthricene • iyn±.01-N.lutyl Phthilati Saturated Q Vos Q No1 Figure In ( . ) Is I of MII M2 Figure 1n 0 , ) Is I of MII II3 Figure 1n( .) Is « of MII 442 "
a
rt
"I I I I I
8<
«
______ ?, =————s „ •t_______———sHi
p
. . . t9*r
8
m
;.
sp
*i4- -I -F "\ I8?T 1 -1 «rjt
BIS
I5
i
«« aM P 014222
MEAD COMPUCHCM *MA88 LXBT DATA: DHB40?.14Ca0 « 687 BASE M/Ei 19802/14/84 iiU!00 + 8:38 RXCi 24704.i UL DFTPP 070so<ii0e5> OWA 020 .
TO 0686 BUMMED - fflSS XL 00 '
44 I. M MINIMA MIN INTEN: B. MAX INTEN> 2904,481 0 • MAXIMAMA88 X RA MASS X RA MASS X RA MABB X RA
44 111 191 •. 48 263 0.94 391 16244 188 ,191 0.79 286 0.72 392 17147 4.17 193 0.83 291 148 398 2.1049 a 89 195 0.86 294 0.9* 399 16980-7.09 19B100.00 296 4.81 402 2.4481 47,73 199 416 298 141 403 117BA 19* 800 188 3002,79404 0.9687 7,47 202 14B 303 .1.14 406 17289 4.30 203 172 308 148 408 10*48 124 204 117 307 0.93 409 0.9049 48.77 208 8.10 309 179 410 0.7471 & 13 20* 17.43 311 179 411 17478 0.90 20B a 03 313 138 412 19377 23.89 213 124 318 0.93 413 10081 188 214 176 316 182 418 103H 3.88 218 100 316 0.74 418 0.8984 0,41 217 4.92 322 0.79 419 0.7499 3,81 218 1,14 323 3.27 423 S, 44108 110 22014B 326 1 S3 424 0.93
|2i 4.27 327 0.79 426 0.90,224 14X47. . ...-•.»!, ,,.4V34 428 0.794an 223 a 68 332 0.79 429 172
111 8.41 227 4,13 334 182 430 0.74118 100 229 2.44 338 0.90 431 131120 0.98 231 0.96 336 134 436 0.28122 148 232 110 338 0.69 437 193123 131 234 1,93 339 2,93 438 0.93127 46.14 237 0,41 342 0.52 440 a 03129 B, 98 238 0.66 346 1.45 441 6.20133 100 240 0.76 347 0.72 442 82.27138 0.34 242 185 348 0.79 443 10.71134 169 243 2,24 349 141 444 110137 2.51 244 5.92 350 0.72 447 0.72144 .0.96 245 0.93 353 0.83 ,.,,,.449 14S147 £24 247 3.20 384 194 482 1B3148 138 280 0.86 386 & 24 483 0.72188 169 252 2.00 388 2.13 484 0.34140 0.48 255 39.12 340 124 48B 188144 174 286 2,31 342 0.84 - 489 0. B4171 0.79 287 0.83 348 2.72 441 0.84172 'EM' •"238.148 347 0.93 443 0.48 • •-••174 184 289 a 75 370 0.04 448 0.85 -;,,>,178. 114 242 148 372 189 447 0.31177 100 268 a 34 373 a 24 449 179179 107 271 1.83 375 158 472 179180 3.24 273 3.00 380 0.49 473 & 07
8.10 275 14.43 382 148 474 S, 033.82 274. 3.99 386 114 47B 131 014223
188 18S 27? 149 387 131 479 & 34 UA'*6*190 & 03 2B2 1.17 389 194 461 a 17 n
o
014224
Ys' ;
VOLATILE INSTRUMENT TUNE AND PERFORMANCE
CASE NO. ______ CONTRACTOR Held CaacuChen CONTRACT NO. 68-01-6762.68-fll.6Bf iION LEVEL -" PSD. LEVEL "~~ H16H LEVELIHATER SOIL/SEP. OTHER
IFB File NOM:Date: aAhx Shift; ft helm;
Nit
M75
15n173j74
175176
J77
BFBIon AbunilirTce Criteria15.00 to 40.00 X of mass 9530.00 to 60.00 X of MSS 95baie peek. 100 oereent5.00 to 9.00 X of niss 95lost than 1,00 X of miss 95oreiter then 50.00 X of miss 955.00 to 9.00 X of miss 174greatar then 95.00 X, but lossthin 101.00 X, of miss 1745.00 to 9.00 X of MOSS 176
% Relative Abundinee
MS.,57100
YT>—&.si5.1/7 (LAoMl
2
tkia ( « .13 ,»2OIFI nrfonaince Results: ••••••• •
n^t The BFB perfonwnc* results Mere reviewed and found tocriteria. \
1 —— 1 iJevletlonilate/Tinoj
initials
Instrument File Number Comound R/x
be within the specifiedollil?'?
oiteRequired ObservedAbundinee Abundinee
Initials• .tite
!55nntt;
. ... .•
lvalue In ( .* Value 1n( .
O ' Valui In ( .
) Is X of MSS 174) Is X of MSS 176IMsXof MSS174 FORHM1 014225
Revision Date 1/31/84
3014226
;• • MEAD COMPVCKKMMASS LIST DATA: BG840203A12 4 22B BABE M/E: 9502/03/84 12tt3i 00 + Us 35 FttC; 83328.
10 ML K20 + 5 UL 10936 + 10941
37 0, H MINIMA M» INTEN: 0. MAX INTEN: 13728.281 0 0 MAXIMAHAM X RA MAM X RA |
37 3.80 103 14238 142 117 14939 & 34 119 19140 9.78 133 19741 9. 74 133 „ , 0. 4748 4.17 174 82,9143 1440 ITS 14744 83.81 174 82, 8048 33.80 177 4.3244 0.84 193 0.7747 141 207 a 4849 in 281 11580 AS, 89si 4.9458 17484 2.0087 12.8990 20,0589 14540 180 . .<41 188 ' • •O43 13947 0.9448 14849 118270 18371 4,8572 2.3673 114974 110575 418774 12477 14078 0.72 "'-• '79 17281 10482 0.8283 13384 0.4088 134 ..-•-,, ,i ••••-.•',• '•84 4.10 ••;;• '%;;,;87,10.31 • •"= r ••*•**•••
•» *4« . . ' v. x Iffll•«'.: 118 ' . . . . .••:;fe. «i fW93; '144 ... . .-. ''•;'tii'.':g'n8&'.y.!?'n$;m)f4 10.11 , i - •:.;, ' 014.?<o g||r 9 B 100.00 ^ . . . . - • • : • • : - '\ :-n m; m« t.77: ,. :•-. . - • • • • : .,.-• ^ ^ ISji,IM .«.40 • i. •••-.., ./:."••; •\ ;i ;:v:;'s jiiiH
• i • . : ' . . . . ; . . . i . . • • ' .••:ilr. )-r';r$*;;;:X '!yi!®M:&-&:isti®mmm
VOLATILE INSTRUMENT TUNE AND PERFORMANCE
CASE NO. ______ CONTRACTOR Mead CcwuCrim CONTRACT NO. 6B.Q1.6762.6B.Ql.6Bf6LOW LEVEL — NED. LEVEL —— HIGH LEVEL
- HATER ________ SOIL/SED.BFB File/ , , a _ _ _ _
Date: */&/£/ Shift: A r AnalvTt; 633
KmU75ISK
m174175
176
r'7
12Ion AbuiHInee Criteria15.00 to 40.00 X of miss 95
Sp.OO to 60.00 X of miss 95base peak. 100 percent5.00 to 9.00 S of miss 95loss than 1,00 X of mass 95greater than 50.00 X of mass 955.00 to 9.00 X of MSS 174greater than 95.00 X, but lessthan 101. 00 X, ofmisi 1745.00 to 9.00 X of miss 176
X Relative Abundance
V607-• /OO
•« , 7W,*/%<MV.LIo (S.lW
O '/Jk ftliT.Of )
£,o£" ( 7 . 02. )2m Pirronunce naiuiu: .,, . „»tm The BFB perfonaance results were reviewed and found
criteria. o. _uOJJ
initials!""""! devlitlons
Oite/TlM/Instrument File Number Compound M/X
to be within the specifiedA/sAywte
Required ObservedAbundinee Abundinee
,'initials •one
Comentii •• . .;; :",'•,
. . . . • •.,«„„„
ivilue1n( . ) lit of MII 174«tfal«t1n( . Hiiofojmm Q1MW> V.luo in ( . X U X of «ss 174 FORMjm . _ .„ .„
PEM
ft-
c^r*^=-8
S
8i' • • • •v i• • ;ji
:;-:. si'
MEAD COrtPUCHEnMAU8 LIST DATA: BC848283A18 « 288 BASE rVE: 95Ofi/03/84 12:41:08 + 14:38 RIC: 771B4.SAMPLE: £ UL BFB 018939 ON 4)18
TO «2B9 SUMMED - #300 XI. 80
BY 8.80 MINIMA MIN INTEN: 8, MAX INTEN: 16144.177 » 0 MAXIMA
MA8B % RA
37 3,15 t38 1.8839 0.7348 0.394 S 0.31 • • • • • ' .43 0.4444 1.9545 0.87 . : .49 131.510 19, 0881 4.7356 2.16
•V..WT 4.73SB 1.0561 2,13
:67 9.95AB 12,93
O71 1,89' '. x'?7Tv;,,3,41'
".'••'' • 7B 46'0976 4.0477 0.0579 2,03
;' ea e'as, 84 0.47
K> 0,68, 86 8.46
87 4.1488 5.489P 1.8893 6.07
, 94 11,89i wiee.ee• .: -?«V-.-.--T.-t*. .• . ,,.., . . ...„, .' 1'Mi, 0,63 ' '
1*9 1,05lift 8.61
,.> •llVV;',j.e5I 124 0.47 ,„' 74 98.5B «-.-..,. 'I
R 4.66g/TO 4. Ob ' 4 IF - .-J.76 86.12 ' i I. 9« '.177 6,85 . »» 014232
VOLATILE INSTRUMENT TUNE AND PERFORMANCE
. CASE NO. ______ CONTRACTOR Held ConauChem CONTRACT NO. 68.Q1.676Z .68.01-6866LOH LEVEL iX* — NED, LEVEL —— HI6H LEVEL
Q HH« __HZZI! SOIL/SED. ^ OTHERBFB File Name: _____
Date; <M Shift; c_ Analyst;
misSO75ISM'"173174
175
176
177
8FBIon Abunlince Criteria15.00 to 40.00 % of mass 9530.00 to 60.00 t of mass 95base ooak. 100 oereent"5.00 to 9.00 X of mass 95less than 1,00 % of mass 95greater than 50.00 S of mass 955.00 to 9.00 X of mass 174greater than 95.00 X, but lossthan 101.00 X. of MSS 1745.00 to 9.00 X Of MSS 176
t Relative Abundance/<..$•)•HZ.
/ ...«*:•
•797t,
<}«Y7t.S.1 i S.lS
U~,SY (9F.U)3Stf ( t l* l*
IFB Ptrronmnce KCSUUI:PPn The BFB perfonunco results were reviewed ind found to
crltirla. ,,TnlH als
r~~l tfev1it1onsMte/Tlme/Instrument File Number Compound mil
be within the specified
biteRequired ObservedAbundinee Abundinee
•inltiilt Dite
icajunti;•
• •>
* Viluo In ( . ) Is X of MSS 1742 Viluo In ( . ) 1s X of MSS 1763 Valuo 1n { . )*1s X of MSS 174 FORM VII 014233
Revision Date 1/31/84PEH
Pi «9 005SP7
X•n
0"
—£
=————8==———————————————————a
6
tsfir Ml
014234
MEAD CO/IPUCHEM"MSB LISI DATA: BF84e283ClB 'it 2B5 BASE M/E: 95OS/03/84 2:88:80 + 14:29 Rid 44288,3iO).,E! 2 UU BFB 18939
37 8.88 MINIMA MIN INTEN: 0. MAX INTEN: 8432,177 t 0 MAXIMAMA&6 X RA
37 2, 6498 3, 6948 6.2741 1.1342 1.5843 . 7. 7714 23.1845 9.20?,e 16.51SI 4,1836 1.16M7 6,69SB 11. 2761 3,1462 1,6468 6.7969 9,3373 5,5474 IS, 6875 42.93
2.911, 53
fa a. 19K7 S, 22(33 IB, 1792 1.4593 3,87V4 9,7195 108. 8896 7. 97174 89, 47.1.7B 7.29176 85.58J77 S. 65
014236
W.AT11E INSTRUMENT TUNE MB PIRFORMAMCE
CASE NO. ______ CONTRACTOR Head CMOuCheai CtatTIACr bfl. 6fl.Ql.6762.68-01.6866SOIL/SO. " OnCR tlnedM
:O
1
^
BO71ti"ff\nP*)7I
171
\TI
/ , . Ifl File tan:ate: gL ff ' Shift: A
Ion AbutSince Criteria15.00 to 40.00 S of MSI 9530.00 to 60.00 X of MSS 95ban Mik. 100 Mitont6.00 to 9.00 X of MSS 95IMS than 1.00 X of MSS 95•rater than 80.00 X of MSS 955.00 to 9.00 X Of MSS 174greater than 95.00 X, but IMSthan 101.00 X, of MSS 1745.00 to 9.00 X of MSS 176
Bl=p-/oa.(3/4Ji>«naijrsi:Lii6Js»
| Relative Abundinee*H3ftX/IOQ
• fcA 4-; 4l*A
ia.itvS",&5 ( ".7»T)»
,,, 32 (tt-a/)37£.0 ( Sr AQ H
•ra PtrTorvnca MUUI:Pg t DM BFI perforMnce results were 'reviewed and found
"iflWiUm fcvlatlons
Date/riM/ Instrument File Nuobor Compound •/!
to be within the specifiedMfBate
Required ObservedAbundance Abundinee
: .;,•*•• *"•*•••'inuiiu . Bate
oaaentii.
..-.;.
I»al»o1n( . ) US of MSS 174«Val«1n( . ) US of MSI 176' Value In ( . • ) Is X of MSS 174 FORM Hi
* " To^RI
n—-—a
1"
O
-
II!
•» 6
|
R >Z
ri .!'i' : 1
JOB
SB
iii
MEAD COMPUCHEM1A3S LIST DATA: BFB40213A,18 * 894 BASE M/E: 95J2/13/84 19:20:80 + 14:57 RIC: 62144.
8 UL BFB «10987 ON MB- «2B8 XI 00
37 0.00 MINIMA MIN INTEN: 0. MAX INTEN: 7880.80S 0 • MAXIMAMABB X RA MASS X RA
37 8.83 174 98,18 •'${.;•, sfV •38 4.94 179 9,3339 8. *8 17* SB, 3241 0.38 177 7. *0'.7TV . • .43 0.79 208 1,41 '49 1 IS90 817351 10. 4852 11455 0.1387 4.4858 7.2061 4.9*62 4.2863 118765 7.0268 1188*9 8.110 ...70 a. 47 .
164 •• • . ' , '"*4.96
74 15,0575 46.247* 4*877 5.9378 5.6379 4.4981 a 1783 0.23B7 7.26B8 5.2489 7.0890 1.9191 15.13 •92 4.3393 4 8794 115595 100. 009* Ea 8497 frl *5 ,,.'.'*•
1»3 9.43 . , ': ': " •185 29.9510* 4.7*119 26.9911* 8.1*
SS . 0142*o9 *. 75 *
120 10. 79141 1.04
VOLATILE INSTRUMENT TUNE AND PERFORMANCE
CASE NO. _ CONTRACTOR Mead CoaauChem CONTRACT NO. 6B.D1.6762.6B-01-6Bf;LOH LEVEL ts> KD. LEVEL —— HUH LEVEL**TER _.Z__I_ S01L/SED. L - OTHER (SpeeTTyT
O ! ,, BFB File Name: ft>ftW;uoe.t81Date; Al,oW Shin; L- toilyst; TV
MissSO7595
96
173
174
175
176
U7
BFBIon Abundance Criteria15.00 to 40.00 X' Of MSS 95
30.00 to 60.00 t of mass 95beie oeik. 100 oereent5.00 to 9.00 X Of mass 95less thin 1.00 X of mass 95greater thin 50.00 X of mass 955.00 to 9.00 X of mass 174greater thin 95.00 X, but lessthan 101.00 X, of mass 1745.00 to 9.00 X of mass 176
| Relative AbundineeILS1HO2.JDO*Cf e) Q
0ti. asUtr4 t.02. ( k.dO )l
ii,w-- . I*.*)1U, .( la.ffjt
IFI Pirronaanci NHUUI:n The BFB perfoTMnci results were' reviewed and found to
criteria. ^ ..ftfltr
f~~l Oev1at1oinitials
nsDlte/Tlme/lnitrurwnt File number compound n/i
be within the specifiedpl/pfj'V
DateRequired ObservedAbundance Abundance
•*....• .. ..inTEuu • Date
coimtnis;.
"' J Value 1n ( '.2 Value In ( ,
O 3value1n( .
', ' .* I-*,.) Is X of MSS 174) Is X of MSS 176) Is X Of MSS 174 FORHV11
01 M O M 1V A IBM *z J.
Revision Date 1/31/B4PEM
Fa;S.Wtf
<RII &
: *
- i!s014242
n
|S
SB-
MEAD COMPURHEMMASS. LIST DATA: BFF40210C1B « 291 BABE M/E: 9992/10/84 0:13:08 + 14:48 > «IC: 45S24.SIMPLE: 2 UL BFB 10987 //
""37 0.00 ;MIN1MA MIN INTEN: 0. MAX INTEN: 8288.261 0 0 MAXIMAMA88 X RA
37 4,4638 1.9939 a 6040 7.4941 5,2143 13.2344 19.7445 9.0950 14 99SI a 7895 1795* 12257 8.7898 10. 0862 4.2562 1,3663 £.4668 9.6269 10.1*71 196
.-73 4*9 .QT4 13.50 -. -. ...*79 41*27* 3,86fll 2.81B7 9.38BB 17.48B9 1109D 2.2594 9.6195 100.009* B. 99174 91.23175 6.0217* 9181177 43B ' .287 2.10281 11.11
014244
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19.49
83.48
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28.97
•24.18
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014254
INSTRUMENT BLANKLM um taie
kattratri MM MMII etauctifi. Cat* (Mr .'"" " "•auctifi.cjgyItt Mpla ID Me. CjgWflfgfl fl. ISfT Aiioclitfd |MB!M nS&t.lCMtO
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INSTRUMENT BLANKVOLATILE LOW SOLID
OLib Maine. Held CompuCrmrt .Lift Smple 1.0. No;
A. SURROGATE SPIKE RESULTS
COMPOUNDIB-Toluene
d4-l,2-D1chloroethini
Ironofluorobenzene
VI-
'•'•:;<,.
FRACTIONVOA
VOA
VOA
CONC(ug/kg )
9-974
. /!.•!• »5l;
.. .,™.
• *'
isurrogiteiSpineAddidiug/kg )
10
10!'!••' f •• • •• .."m--
10.•tfi . .
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ft'rt ..'¥".'
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PROCEDURE! m DIAGNOSTIC REPORT S/03/B4 14:36:87DATA FILE: CEB40203A12REFERENCE! V23BO METHOD! V83B INITIALIZATION OPTION! 8 PROCESSING OPTION: 3-• REPORT: V23881
< ——- BTANOAROB ——— X —— PLUB UNKNOWNS —— X, - LitBT NMKB - 9PROC UMO P08B RUB PROC USED POflB RI18 BTANOARD/VNKNOWN
3 3 1 104 44 7 1 66 VBSOBl/VBSSUl
COWPOWW X ———————— MARCH ———————— X BAT >< ———— CHRO ————— >D LXB ENTRY REP PRED BEL DELTA PEAKS TXT PEAKS T\ft TOP DELTA PEAKS
PS 1 -199 194 194 1 936 IM 194P6 1 -818 378 9T9 1 1 760P7 1 -4*3 4*0 499 -1 ,-„ 1 984PS 8 -37 31PS 3-3* 80PS 4 -70 *4PS S -91 BSPS * -13S 130PS 7 -14* 141PS 8 -14* 141PS 9 -1*1 IS*PS 10 -17* 171PS 11 -1** 1*1PS 18 -190 183PS 13 -81* 811PS 14 -889 8B4PS IS -241 236PS 1* -898 2S1PS 17 -2S3 248PS 18 -2B2 278PS 19 -890 M*P* 2 -291 287P6 3 -299 293P6 4 -327 323P* S -331 327P* * -342 338P* 7 -3S4 350 351P6 8 -397 353P6 9 -397 353P* 10 -393 351P* 11 -379 379P* 12 -409 406P6 13 -419 416P7 2 -490 447P7 3 -43* 453P7 4 -48* 453P7 8 -484 481P7 * -909 90*P7 7 -538 956P7 B -Ml 659P7 9 -*93 *91P8 2 -294 249 249PB 3 -4B0 . 477 477PB 4 -621 ' *19 619
933
1 9471 9811 964
79 37959 4999094626484 13B98 1419693 . .10176 16196699*83 2376272 2909T11743127697313078 3319779
127 -.63173989883 4321*492 4BB112 50*106 594104 69B106 69269 249100 47i176 61'
OOF.pi.S3**
flUANTZTATZON REPORT PILE: GEB40EP3A12*
QATAi CEB40203A12. ni V03/84 12: 43:00iWiMPLEi 10 ML H20 * 9 UL 10941 •«• 10936BUBMXTTEP BYi 12 ANALYST: 877
AMOUNT-AREA * REP. AMNT/tREF. AREA)* RE8P. FACT)REBP. FAC. FROM LIBRARY ENTRY
NO NAME • ,11 t BROnOCHLOROMETHANE (IB)2 881 CHLOROnETHANE3 82B BROMOMETHANE4 231 VINYL CHLORIDEB 109 CHLOROETHANE* 888 HETHYLENE CHLORIDE7 858 ACETONE (2-PROPANONE)8 801 ACROLEZNf 802 ACRYLONXTRXLE10 838 TRICHLOROFLUOROMETHANE11 854 CARBON OX8ULFZDE12 81* i. 1-DXCHLOROETHYLENE13 814 Ii 1-OXCHLOROETHANE14 88* TRANB-i,C-OXCHLOROETHYLENE15 211 CHLOROFORM1* 215 It t-OICHLOROETHANE17 893 2-BUTANONE
227 1.1. 1-TRXCHLOROETHANE80* CARBON TETRACHLORXDE• 2-8ROfW-l-CHLWW>PROPANE
21 257 VINYL ACETATE22 212 BROmOXCHLOROnETHANE23 217 i. 2-DXCHLOROPROPANE24 25B TRANB-i,3-DXCHLOROPROPENE25 229 TRXCHLOROETHYLENE2* 203 BENZENE27 228 1. li 2-TRXCHLOROETHANE26 21B CIB-1, 3-OXCHLOROPROPENE29 20B DXBROMOCHLOROMETHANE30 210 2-CHLOROETHYL VINYL ETHER31 205 BROHOFORM32 25* 4-METHYL-2-PENTANONE33 * DXCHLOROBUTANE34 299 2-HEXANONE35 223 1.1.2, 2-TETRACHLOROETHANE3* 224 TETRACHLOROETHENE37 225 TOLUENE38 207 CHLOROBENZENE39 219 rTHYLBENZENE4B 251 8TYRENE n. .„_.41 239 0-XYLENE 01426042 0 D4-1.2-OXCHLOROETHANE43 0 OB-TOLUENE44 0 BROMOFLUOROBENZENE
3 M/E SCAN TIHB REF RRT METH AREA(HCHT) AMOUNT XTOT
$ a* OftF.fi
NO M/E SCAN TIME REF RRT METH AREMHCHT) AMOUNT XTOT130 194 9:92 1 1.000 ABB 71133. 10.000 UC/KC 14.99NOT FOUND
3 NOT FOUND4 NOT FOUNDS NOT FOUND* 84 130 *: 3* 10.670 A BB 24703. 2.433 UC/KC 3,947 SB 141 7:10 1 0.727 A BB 2992. 3.000 UC/KC 4.378 NOT FOUNDf NOT FOUND . •?!" •• • •••• • •10 NOT FOUND11 76 161 8:11 1 0.830 ABB 2923. 0.074 UC/KC. 0.1112 NOT FOUND13 NOT FOUND14 NOT FOUND19 83 237 12:03 i 1222 A BB 4278. 0.257 UC/KC 0.371* NOT FOUND17 72 290 12:42 1 1289 A BB 5096. 3.337 UC/KC 4.8918 NOT FOUND19 NOT FOUND20 79 379 19:1* 20 1.000 A BB 61498. 10.000 UC/KC 14,9921 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND2* 78 391 17)51 1 1809 A VB 10299. 0.362 UC/KC 0.9327 NOT FOUND
NOT FOUNDNOT FOUND
30 NOT FOUND31 NOT FOUND32 NOT FOUND33 99 499 23:20 33 1.000 A BB 179120. 10.000 UC/KC 14,9934 NOT FOUND39 83 492 22:99 1 2.330 ABB 2016, 0.092 UC/KC 0.133* NOT FOUND37 92 480 24:24 1 2,474 A BB 1961 0.080 UC/KC 0.1238 112 906 29:43 1 2.608 A BB 1943, 0.069 UC/KC 0.1039 106 994 28:10 1 2.856 A VB 294. 0.027 UC/KC 0.0440 104 *5B 33:27 1 a 392 AtVB 1941 0.101 UC/KC 0.1541 10* 692 39:11 1 a 567 A BV 939. 0. 050 UG/K£ 0.0842 69 249 12:39 11284 A BB 93347. 7.467 UC/KP 10.8643 100 476 24:12 1 2,434 A BV 200520, 9.927 UC/KC 14.4444 176 619 31:2B 1 3,191 ABB 13B020. 11.460 UC/KC 16.67
NO RET(L) RATIO RRT(L> RATIO AMNT AMNT(L) R. FAC R.FACU.I RATIO1 19:04 ft. 98 1000 100 10.00 10.00 1000 1000. 1002 X<93,. 0.187 40.00 ... 11273 2:54 " 0.288 ' 40.00 •••"'.•• 2.1154 '3:33 0.354 40.00 1,4415 4:38 0.460 40.00 0.838* 6:32 0.96 0. *B2 0.98 2.43 40.00 0.087 14277 7:29 0.97 0.737 0.99 3.00 299.99 0.001 0.140
,.,B 7:23 0.737 399.99 0.1998:11 0,813 399.99 0.3978:97 0. BB9 40.00 2.023 fjOF'ift')
11 8:23 0.98 0,833 1,00 0.07 40.00 0,009 4.822 0.O2 9:36 0.959 40.00 1,097HI 10:96 1086 40.00 0.649Ji'4 11:3B 1197 40.00 127419 12:12 0.99 1.212 101 0.26 40.00 .0.019 2.337 0.0116 12:99 1,283 40.00 139417 12:49 0,99 1273 1,01 3,34 299.99 0.002 0,219 0.01IB 14:17 1419 ,40.00 174119 14:41 14*0 40.00 1*8020 19:22 0,99 1000 100 10.00 10.00 1000 1000 10021 14:44 14*9 40.00 2.06122 19:09 1505 40.00 0.18*23 1*:34 1*4* 40.00 0.53124 1*: 5* 1*72 40.00 a*13-25 17:2* 1722 40.00 15032* 17:97 0.99 1783 101 0.3* 40.00 0.036 3.999 0.0127 18:0* 1798 40.00 199488 18:0* 1798 ,40.00 128629 18:00 1788 40.00 18**3* 19:13 1909 40. M 0.94431 20:44 2.0*1 40.00 13*332 21:15 2, Ul M. 00 0,69433 23:2* 100 1000 100 10.00 10.00., 1000 1000 10034 22:49 ft 2*8 ' 40.00 *'•"" 0.5*035 23:08 0.99 2. 298 101 0.09 40. M 0.007 3.093 0.003* 23:08 2.298 40.00 . 133137 24:33 0.99 2,439 101 0.00 40.00 0.009 2.743 0.0038 25.49 100 at B** 102 0.07 40.00 0,003 3,31* 0.003f 28:16 100 2, BOB 102 0, 03 40. 00 0, 001 ' 1 517 0.00!0 33:30 100 3,328 102 0.10 40. M 8.005 £145 0.0041 35: n 100 3.495 1.02 0,06 40.00 0,002 1300 0.0042 12:52 0.98 127B 100 7,47 10.00 1312 175B 0.7543 24:21 0.99 2,419 101 9.93 M. 00 2.819 2. B40 0.9944 31:31 100 3.131 102 11.46 10.00 1940 1693 1.15
OV
INSTRUMENT BLANK
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INSTRUMENT BLANKVOLATILE LOW SOLID
Olib Hue; Meid ComuChea
A. SURROGATE SPIKE RESULTS
COMPOUND
•••Toluene
de>l,2-D1chbroethine
IroMfluorobeniene
FRACTION
mVOA
VOA
CONC(ug/kg )
/M<?:/
. /i* "''
.>
^Sufrogites only)Addedlug/kg )
10
10
10
•
SRecovery
/<?/
91 -/'*
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PROCEDURE: RK DIAGNOSTIC REPORT 2/03/84 3:67:2'.DATA FILE: 06840203618REFERENCE: V23Q-METHOD: V238 INITIALIZATION OPTION; S PROCESSING OPTION: 3'JlEPQRT: V23SS1
.{ ——. STANDARDS ——— X —— PLUS UNKNOWNS —— X - LIST NAI-IEB - >, PHOC USF.D POBB RMB PROC USED FOBS RMB STANDARD/UNKNOWN
3 3 1 96 44 6 i 33 V23BS1/VS3BU1
44 COMPOUNDS PROCESSED, 6 FOUND
< COMPOUND X ———————— SEARCH —————-—— >< SAT X ———— CHRO ————- ';NO U» ENTRY REF PRED SEL DELTA PEAKS RET PEAKS M/E TOP DELTA PEAK'1J PS 1 230 229 229 1 951 . 130 2292 P6 i 412 411 411 . 1 7B7 79 4113 P7 1 491 , 491 491 . 1 988 , 35 4914 PS 2 56 ' 58 . , . , SO . .5 PS 3 87 86 , , , , , 94 . ,6 PS 4 10S 104 , . , . .62 . .•I PS 5 130 129 . . . . 64f) PS 6 178 17i . , , , .84 171 . i9 PS 7 1B2 1B1 , . , SB10 PS 8 -1B2 181 . , . , . 5611 PS 9 195 194 . , , S312 PS 10 212 211 ' , .••''"• , . 10113 PS 11 202 201 . , . 76 204 i14 PS IS 224 223 , , , 9615 PS 13 248 247 . . , , .6514 PS 14 262 2*1 , . . .-«. 96O PS IS 271 '270 , ... , B3 270 ;.28 PS 16 286 2BS , , , . , 6219 PS 17 204 283 , , , • , 72 2B4 . '..20 PS 18 313 312 , , , . 9721 PS 19 321 320 11728 P6 3 322 321 , . . 4323 F6 3 328 327 , , , , 12721 P6 4 357 356 , . , , 632G P6 5 361 360 , , , . 7526 P6 6 372 371 , , , . . 13027 P6 7 384 383 , , , , 78 3852B P4 8 386 383 . . , , 97Z't P6 9 -387 386 . , , , 75 ...3d P6 10 -384 383 , , , 1273J P6 11 408 407 , . - , , . 63 4l{l38 P6 12 437 436 , , , , , 17333 P6 13 449 448 . , , , . SB34 P? 2 479 478 , 58 4BO /•35 P7 3 -484 483 , . , B336 P7 4 485 484 „• ' . . '. ' , 16437 P7 5 517 516 , , . , , ,92 516" . 130 P7 6 546' 543 , , , , . 11239 P7 7 609 608 , , , , 10640 P7 8 749 749 . . . , . 1044.1 P7 9 793 793 , . , , , '1064!> FQ 2 -284 283 283 , 1 992 65 2B3OP6 3 S12 . 511 512 1 1 97B . 100 311 -1
P8 4 693 ' 693 692 -1 1 968 . 176 693 1 <
( >f
QUANTITATXON REPORT FILE: GBB4«ae3CXB
DATA: 08840203018. TX8H/03/B4 2: 20; (10C >LE: 10 ML H20 + 5 UL (10936 .0741)SUBMITTED BY: IB ANALYST: 714
AMOUNT-ARE* * REF. AMNT/( REF. AREA)* RESP, FACT)RESfP. FAC. FROM LIBRARY ENTRY
NO NAME1 ft BROHOCHLOROHETHANE (IS)S 221 CHLOROMETHANE3 220 BROMOMETHANE4 231 VINYL CHLORIDES 209 CHLOROETHANE6 222 HETHYLENE CHLORIDE7 252 ACETONE (2-PROPANONE) " **8 201 ACROLEIN9 202 ACRYLONXTRILE10 230 TRICHLOROFLUOROMETHANE11 254 CARBON DI8ULFIDE13 216 1, 1-DICHLOROETHYLENE13 214 1, 1-DICHLOROETHANE14 226 TRAN8-1, 2-DICHLOROETHYl.E'NEIS 211 CHLOROFORM16 215 1, 2-DICHLOROETHANE17 253 S-BUTANONEID 227 1, 1, 1-TRICHLOROETHANE . . ........19 206 CARBON TETRACHLORIOE „,..,,„..,..
* 2-BROMO-l-CHLOROPROPANF. ..9. 257 VINYL ACETATE2S 212 BROMODICHLOROMETHANE23 217 1, 2-DICHLOROPROPANE24 250 TRANS-1, S-DICHLOROPROPENE2S 229 TRICHLOROETHYLENE26 203 BENZENE27 228 1, 1, 2-TRZCHLOROETHANE20 21B CIS-1, 3-DICHLOROPROPENE:2<V 208 DIBROMOCHLOROMETHANE30 . 210 R-CHLOROETHYL VINYL ETHER31 205 BROMOFORM3? 256 4-METHYL-2-PENTANONE3:i * DICHLOROBUTANE3-1 255 2-HEXANONE »•3L 223 1, 1, 2, 2-TETRACHLOROETHANE-36 224 TETRACHLOROETHENE37 225 TOLUENE30 207 CHLOROBENZENE3<y 219 ETHYLBENZENE '..-...40 251 STYREME '"' ' . • ,;• •r'"'1" '41 239 0-XVLENE ' •4& '0 D4-1, 2-DICHLOROETHANE r'49 « DB-TOLUENE44 « BROMOFLUOROBENZENE
ttfto M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT
A
0NO M/E SCAN TIME REF RRT METH AREA(HCHT) AMOUNT WOT
130 229 11:38 1 i. 000 A 8V 74901, 10, 000 UC/KC IB, 04NOT FOUNDNOT FOUNDNOT FOUND
S NOT FOUND6 84 171 8:42 1 0, 747 A BB 16016, 2. 302 UC/KC 3,467 NOT FOUNDB NOT FOUND9 NOT FOUND10 NOT FOUND1J 76 204 10:22 1 0. 891 A BB 469, . 0.020 UC/KC 0,0312 NOT FOUND13 NOT FOUND14 NOT FOUND15 83 270 13:43 "'I 1,17? ABB -.2635, 0,221 UC/KC 0.3316 NOT FOUND '17 72 284 14:26 1 1,240 ABE) 1864, 2,044 UC/KC 3,07IB NOT FOUND1? NOT FOUND20 79 411 20:54 20 1,000 A BB 30737, 10,000 UC/KC 15. 0481 NOT FOUND2? NOT FOUND23 NOT FOUND24 NOT FOUND .•........." .,„.,,,-,•.25 NOT FOUNDSt< 78 385 19:34 1 1.681 A BB 593, 0, 037 UC/KC 0, 0627 NOT FOUND- . . . . .... j,,.•,„.28..NQJ FOUND ' • '*"*••<*3""NO'r FOUND . •'''$ 63 410 20:30 1 1.790 A BV 232. 0.032 UC/KC 0, OS31 NOT FOUND3£» NOT FOUND33 S3 491 24: SB 33. 1000 A BV 69203. 10,000 UC/KC 13, 0434 38 4B0 24:24 1 2,096 A*BV 1263. 0.360 UC/KG 0, 843i! NOT FOUND36 NOT FOUND37 92 316 26:14 1 2, 253 A BB 476, 0. 040 UC/KC 0. 0638 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND4& 65 283 14:23 1 123A A BB 69703. 9.123 UC/KC 13,7249 100 511 25:39 1 2,231 A BB 138678, 10,781 UC/K0 16. 2144 176 693 33:14 1 3,026 A 68 1BS499, 11 354 UC/KC 17. 07
NO RET<L> RATIO RRT(L) RATIO AMNT AMNT(L) R. FAC R.FAC(L) RATIOX 19:55 1.17 1000 1.00 10,00 10.00 1,000 1000 1,00•f. ' 2:31 .' 0,243 20,00 0.3953 4:2li 0.37B 20.00 .., 2.199 •/> 5:SO 0,457 20.00 :•• '2.159a "6:36 0,563 20.00 0.4116 6:32 1.27 0,743 1.00 2,30 20,00 0.107 0,929 0,12V 9:15 0,791 149,99 • 0.076U 9:18 0,796 199,79 0,090
9: Si 0,848 199,99 0.19610:47 0.9.22 20.00 1.
ft1.1 10i 1,6 1, 01 0, 878 1, 01 0,02 20, 00 0, 003 3,1.35 0. 00:20 0, 970 20. 00 0.721
12:36 i, 078 20. 00 0. 31914 13:19 1 139 20, 00 0,006115 13:4Y 1, 00 1178 1. 00 0,22 20. 00 0, 01B 1,592 0, 0116 14i 32 1243 20, 00 1, 05317 14; 26 100 1 235 1, 00 2, 04 149. 99 0. 002 0,122 0, 01111 13: SS 1.361 20. 00 1,22519 16:19 1396 20.00 138420 19:13 1,09 1000 1 00 10,00 10.00 1000 1000 100Si, 16:22 1.400 20.00 1.10923 16:40 1426 20.00 0.19323 18:09 1,552 20.00 0,21824 18:21 1570 20,00 1,3652!! 18:55 1617 20.00 129626 19:31 1,00 1670 1, 01 0,04 20.00 0.004 2,115 0,0027 19:37 1.67B 20.00 10132& 19137 167B 20. 00 0,73429 19: SB 1665 20,00 1,50730 20:44 100 1774 1. 01 0,03 20.00 0,002 0,955 0.0031 22:10 1,896 20,00 1,7223£> 22:49 1,952 30.00 0,33233 23:17 1,07 1000 100 10.00 10.00 1000 1,000 1.0034 24:21 1,00 2,083 101 0.36 30.00 0.006 0,301 0.023K 24:33 Z. 100 20.00 1,75136 24:39 & 109 20,00 1.32337 26:17 1,00 & 246 1.00 0,04 20.00 0.003 1600 0,00§27:42 2.374 20.00 .... 2.408
30! 97 2.648 • 20,00 1,13038:07 3,261 20. N 2,745
41 40,' 19 3, 446 20. 00 1, 7244!! 12:39 1 14 1235 1, 00 9. 12 10. 00 0, 931 1,020 0. 9143 24:2J 107 2.226 1, 00 10,78 10. 00 1 851 1,717 1 0844 33:33 1 05 3,013 1, 00 11,35 10. 00 2, 477 2, 181 1 14
O
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INSTRUMENT BLANKLM HUB. MUC
^ID He. C4.B{r(WCJr>i >Q toioetatad lM«il
(Natrfrlrnr NM«ta*t HnriM Matawaal ' '
HI014273
INSTRUMENT BLANKVOLATILE LOW SOLID
OLib Kami; Haad CcmpuCImn
A. SURROGATE SPIKE RESULTS
' ' COMPOUND
dB-Toluint
d4-l,2.Dicn1oroithine
Iromfluorobinzini
. ,
.•;.. •••
FRACTION
VOA
VOA
VOA
/ •
CONC(ug/kg )
H.'f1.1
. TP. f$g$&»;
.... .
..**•*
(Surrogitu inly)Sptkt
Addid(ug/k9 )
10
10
10
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PROCEDURE: RK DIAGNOSTIC REPORT 2/03/84 13: 37: SiOAT A FILE: CD840203A1BREFERENCE: V23BOMfeTHODi V238 INITIALIZATION OPTION: S PROCESSING OPTION: 3~ REPORT: V23BS1
< ...— STANDARDS ——— X —— PLU8 UNKNOWNS •—— X - LIST NAMES - >PROC USED POS8 RM8 PROC USED POSS KM8 STANDARD/UNKNOWN
3 3 1 36 44 7 1 ' 3» V23B01/V23BU1
44 COMPOUNDS PROCESSED, 7 FOUND * '"" ' " ** '
1 PS 1 -230 229 229 . 1 937 130 2298 P6 1 -412 411 411 . .1 781 . 79 4113 P7 . 1 -491 491 491 . 1 991 55 4914 P5 , 2 -54 52 , . , , . 505 PS 3 -87 85 , . . , .946 PS 4 -106 104 , . ' . .627 P S 5 -130 1 2 9 . . . . . 6 48 PS 6 -171 170 170 . 1 ' 952 . B4 1709 PS 7 -1B2 181 , . , 5810 PS B -1B2 181 . . 5611 PS 9 -194 193 , . , , . 53 .12 PS 10 -211 210 , . , 10113 PS 11 -202 201 , . , , 7614 PS 12 -223 .222 , , . . ' . -:96IS PS 13 -248 247 , , . . , 63 .
PS 14 -261 260 . . , , 96 .PS IS -270 269 , . , , , 83 269
IS P5 16 -2BS 284 , , , . 6219 PS 17 -284 283 , . . . . 72 28320 PS 18 -313 312 . . , . 972J PS 19 -320 319 , , , , 11722 P6 2 -321 320 . , , 4323 P6 3 -327 32d . , , . 1272/) P6 ' 4 -357 356 . . . . 652 5 P 6 5 -361 3 6 0 . . . . . 7 526 P6 6 -372 371 . , . , 1302? P6 7 -384 3B4 , , ... 78 3862B P6 B -385 385 . . . 972'/ P6 9 -386 386 . , , 7530 F6 10 -383 383 12731 P6 11 -408 406 , . , , 63 4103« F6 12 -436 436 . . . 17333 P6 13 -448 448 , , , SB34 P7 2 -479 479 , . , . .58 4783S P y. 3 -483 483 , . . 8336 P7 4 -483 483 . . . , , _M .,37 P7 S -516 516 . , . , . 92 .30 P7 6 -546 546 , . , 11239 P7 7 -609 609 , , , 1064« P7 8 -748 749 . , . , 1044,1 P7 9 -793 794 , , . , 9 9 9 106
PB 2 -284 283 2B3 , 1 991 63 2B3/,PB 3 -512 '512 512 . 1 981 100F8 4 -692 693 693 , 1 989 176 693§
aUANHTATION REPORT FILE: CDB40203A1B
T/i: CDB40203A1B. TI, ,33/84 13:01:00SAMPLE: 10 ML H20 + 5 UL 10941*10936 ON «18SUBMITTED BY: 4UB ANALYST: 633
AMOUNT-AREA * REF, AUNT/(REF, AREA)* RESR FACT)RE8P. FAC, : FROM LIBRARY ENTRY
NCi NAME •••••' •'*•'1 * BROMOCHLOROMETHANE (IS)B 221 CHLOROMETHANE3 220 BROMOMETHANE4 231 VINYL CHLORIDES 209 CHLOROETHANE6 222 METHYLENE CHLORIDE7 252 ACETONE (2-PROPANONE)B 201 ACROLEIN? 202 ACRYLONXTRILE10 230 'I RICHLOROFLUOROMETHANE11 254 CARBON DI8ULFXDEi?. 216 Ii 1-DXCHLOROETHYLENE19 214 Ii 1-DXCHLOROETHANE14 226 TRAN8-JU 2-DICHLOROETHYl.E'NEIB 211 CHLOROFORM16 213 1,2-OXCHLOROETHANE17 253 2-BUTANONE • • T3?».-.IB 227 1,1,1-TRICHLOROETHANEO "206 CARBON TETRACHLORIDEEP * 2-BROMO-l-CHLOROPROPANE:'21 257 VINYL ACETATEKi 212 BROMODICHLOROMETHANE23 217 Ii 2-DXCHLOROPROPANE24 250 TRAN8-1 3-DICHLOROPROPENK211 229 TRICHLOROETHYLENE26 203 BENZENES't 228 1, 1, 2-TRICHLOROETHANt;20 21B CIS-1, 3-DICHLOROFROFENP2? 208 DIBROMOCHLOROMETHANE30 210 g-CHLOROETHYL VINYL ETHL-R3.1. 205 BROMOFORM3B 256 4-METHYL-2-PENTANONE33 « DICHUOROBUTANE34 255 2-HEXANONE31! 223 1,1, 2, 2-TETRACHLOROETHANE:36 224 TETRACHLOROETHENE3V 225 TOLUENE3D 207 CHLOROBENZENE39 219 ETHYLBENZENE40 251 BTYRENE41 239 0-XYLENE4& « 04-1,2-DICHLOROETHANE43 « OS-TOLUENE44 « BROMOFLUOROBENZENE
O H/E SCAN HME1- REF RRT METH AREA(HCHT) AMOUNT XTOT
NO M/E SCAN TIME REF RRT METH AREA(HGHT) AMOUNT XTOT1 130 229 11: SB 1 1, 000 A BV 80456, 10, 000 UC/KG 14, 47f~\ NOT'FOUNDV NOT FOUND4 NOT FOUNDf$ NOT FOUND6 84 170 B: 38 1 0, 742 A 88 21058, 3,856 UC/KC 5. 587 NOT FOUND& NOT FOUND9 NOT FOUND "••«• " •10 NOT FOUND11 NOT FOUND12 NOT FOUND13 NOT FOUND14 NOT FOUNDif, 83 '269 13:40 1 1175 ABB 2670, 0.21S UC/KC 0.3216 NOT FOUND17 72 283 14:23 1 1236 A BB 2003, 2.609 UC/KC 3.77IB NOT FOUNDj? NOT FOUND20 79 411 20:54 20 1000 A BB 38666. 10,000 UC/KC 14.4721 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND2!!> NOT FOUND26 7B 386 19:37 1 1 686 A BB ' 600, 0.033 UC/KC 0.05 •27 NOT FOUND{a* NOT FOUND~W> NOT FOUND3d 63 410 20:50 1 1, 790 A BV 283, 0.112 UC/KC 0. 1631 NOT FOUNDSB NOT FOUND33 53 491 24:58 33 1,000 ABB 75911 10.000 UC/KC 14.4734 58 478 24: IB 1 2, OB7 A BB 3065, 1.696 UO/KC 2. 453!i NOT FOUND36 NOT FOUND37 NOT FOUND3d NOT FOUND39 NOT FOUftID40 NOT F0l!?ir>--41 NOT FOUND • •""""""•'41' 6!) 283 14:23 1 1 236 A BV 67642, 7,503 UC/KC. 10. 8643 100 512 26:02 1 2, 236 A BB 143348, 11. 353 UC/KC 16. 4344 176 693 35:14 1 3,026 ABB 186099, 11. 748 UC/KC 17. 00
NO RETIU RATIO RRT(L) RATIO AMNT AMNT(L) R. FAC R, FAC(L) RATIOA. in 4i 100 1000 100 10, ee io. 00 i oeo i eoe . 100S 2:45 0, 235 60.00 0. 432 . ,.3 4:25 0,37B 60.00 16944 3:23 0.461 60.00 1708ft 6:36 0, 365 60,00 0, 313A 8:42 0,99 0! 743 1. 00 3, 86 60! 00 0. 044 0,679 0. 067 9:J,5 0,791 449,98 0,0580 9:3.8 0,791 599.98 0.074
*S2 O. B43 599.98 0.176lO:44 0.917 60.00 1.
10:16 0. 878 60. 00 S, 819;M 11: a<?> 0. 970 60, 00 0. 70S13 12:36 1078 60,00 0,31114 13:16 1135 60.00 0.780M 13:43 1. OH 1.174 1 00 0. 22! 60. 00 0, 006 1, 519 0.0016 14:29 1239 60. 00 0, 996IV 14:26 1.00 1235 100 2,61 449.98 0.001 0.095 0.011(1 15: S3 1361 60. 00 . 1 241IV 16:16 1.391 60, 00 • ' • 1, 48020 20:57 1.00 1000 1,00 10,00 10.00 1.000 1000 1.0021 16:19 1396 60, 00 1, 02322 16:37 1422 60. 00 0, 19123 18:09 1552 60. 00 0. 21124 18:21 1.570 '60.00 1.404SK 18:55 1617 60.00 1266SA 19:31 1, 01 1 670 1 01 0,03 60. 00 0, 001 2. 241 0.0027 19:34 1674 60,00 0.98823 19:37 1,678 60.00 0.74929 19:26 1,665 60.00 155330 20:44 1,00 1774 1,01 0,11 60.00 0.001 0,313 0.0031 22:10 1,896 60.00 17063? 22:46 1948 90.00 ... 0.28039 24:58 1.00 1000 1.00 10,00 10.00 1000 1000 1.0034 24:21 100 2,083 1, 00 1, 70 90.00 0. 004 0, 223 0.023S 24:33 2,100 60.00 1.67236 24:39 2,109 60.00 131937 26:14 2.243 M. 00 --:•,;•,„,,, 1532027:415 2,374 66.00 " 2,2943T 30:57 2.648 60.00 . 110940 38:01 3,252 60. 00 2, 3234.1 40:4 9 3.448 60,00 14574?; 14:26 100 1,235 100 7.50 10.00 0.841 1,120 0.754fl 26:02 1,00 2,226 1.00 11,36 10.00 1782 1569 11444 35:11 1, 00 3, 009 1, 01 11, 73 10, 00 2, 313 1 969 1 17
O \
1NSTRUMEHT ILANK
'ftgy
'! ,'!f
4281 onsRnu"I" ts
INSTrUMENT HANKVOLATILE LOW SOLID
0Ub BiMt Hild CnauChtiB
• "'MJiWttV
A. SURROGATE IP Itt K$UU$
«*yii..
COMPOUND
M-TOIMM
<4>l,{-D1eMBretthim
InaKfluorotriniini
,.
• ' "•'
FRACTION
VOA
VOA.'• i' **' **
VOA
;' .-!•
CONC (us/kg )
' '94*.r
. £•!(
••
-
, ,
purrooitiiHIMAddtd(ug/kg )
10
10
10
' ' ' ' •
inly)-niUteoviry
?>•9r/p/
•
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t*i-a*
o , B T84
DXACNOBTXC REPORT 2/10/H4 1:27:44OBB40210C1B
XNXTZALXZATXON OPTION: 2 PROCESSING OPTION: 3
PLUS UNKNOWNS —— X - LXBT NAMEB - > -*~USED POSB RUB BTANDARO/UNKNOWN
4 1 43 V23BB1/V238U1
NMM) • • • • . . •• ..;•:• T ,«tf,.arwwTwr . ''*.•' **• • ' '"' •••'•'•M fiV ' i
SEARCH ——————— X SAT X ——— CHRO ———— >DELTA PEAKS FIT PIWKS H/E TOP DELTA PEAKS
940 130 238 -1 1
C13 313-494 494 494
1 781'
2B4 -1 1 990974973
79 412 -188 4928894
84 1728884831017494489483 2714272 2B59711743127AS7813078 38897781274317358
144,91 .818112104104'104AS 2B4IM 81317A A9A 0142&3
,01) 5
laVAMTXTATXON REPORT PILE: Gt»10tlOClB
lOATA: OM40210CJL8. TI1/84 0:33:00
18 ML H20 + 8 UL (10985+10990)ISUmXTTtD BY: 18 ANALYST: 714
EA * RIF.AMNT/CREF, AREA>« RESP.FACT)FAC. PROM LIBRARY ENTRY
I j1* 4) • B VnUGnLwnft VTrinNC CX8)221 CJJLOROMETHANE
avnOVfOflETHriNB ,VINYLCHLORnEWTWi rA rJt TflMwJi
METHYLENE CHLORIOEACETONE (2-PROPANONE)
ACRYLONITOILE .TKCHLOROPLUORORCTHANECARBON DXSULPXDElil-OTCHLOROETHYLENE!• 1-OXCHLOROETHANETRA«-laH«CHLOROETHYtlJNE .... ..,„.;„.CHLOROFORM!• 2-OICHLOROETHANit-8UTANONE1,11-TRKHLOROETHANECARBON TETRACHLORXDE
* 2-0ROMO-l-CHLOROPROPANi287 VINYL ACETATE
«2 212 BROMODICHLOROMETHANE•89 217 1.2-01CHLOROPROPANEM 280 TRANB-1 3-DZCHLOROPROPENE89 229 TRXCHLOROETHYLENE24 203 BENZENE27 228 1,12-TRICHLOROETHANE29 218 CIB-l 3-OICHLOROPROPENE29 2M DZ6ROMOCHLOROMETHANE30 210 2-CHLOROETHYL VINYL ETHER,31 205 BROMOFORM1 3S 25A 4-METHYL-2-PENTANONE33 t DICHLOR08UTANE34 2S3.2-HEXANONE .35 223 l,l.aa-TETRACHLOROETHANE34 224 TETRACHLOROETHENE37 225 TOLUENE '36 M7 CHLOROBENZENE -"'.'.. >•'•>,:,•• -•• ;39 219 ETHYLBENZENE .,,,,•<«...,,.:....•,• ^ ••• . ^ 40 281 8TYRENE .V.. - .'"' . . ""- ' • '41 239 0-XYUNE '42 O D4-12-DICHLOROETHANE43 0 DB-TOLUENE44 0 IJROMOFLUOROBENZENE ' 014286
SCAN TIME i REF RRT METH AREA(HGHT) AMOUNT XTOT
H/E SCAN TIME REF RRT HETH AREA(HCHT) AMOUNT XTOT130 230 11:41 1 10M A BV 73909. 10.000 UC/KC IS. 37•NNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND84 172 .B>43 1 8.748 AM 4B9B. 8.987 UC/KC 182NOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUNDNOT FOUND " TNOT FOUNDNOT FOUND • 'S3 871 13:47 1 1 i.78 AM 4883. 8.349 UC/KC 0.S7
NOT FOUND •''•' ••72 285 14:29 1 1239 AM 1474. & 711 UC/KC 4.17NOT FOUNDNOT FOUND79 412 28:87 20 1OM A 8V 27023. 18.8M UC/KC 15,37NOT FOUNDNOT FOUND'MOT FOUNDNOT FOUNDNOT FOUNDa 383 19.'34 1 1474 AM 987. B.U72UC/KO 0.11 ,
NOT FOUNDi NOT FOUND "" *''•''>NOT FOUNDNOT FOUND
31 NOT FOUNDSS NOT FOUND'55 88 492 25:01 33 1 MO A BV A4091 10.000 UC/KC 15,3734 58 4B0 24:24 1 2.087 AtBB 758. B. 149 UC/KC 0.2935 NOT FOUND34 NOT FOUND37 92 SIB 26:20 1 2.252 AM 810. 0.088 UC/KC 0.14SB NOT FOUND99 NOT FOUND40 NOT FOUND41 NOT FOUND ' •42 AS 284 14:26 1 1235 A M A4729. 8.874 WC/K013.1043 108. 813 24:08 1 2.230 A BV 128843. 9.968 UC/KC'15,3244 17A A9A 33:23 1 3.024 A M 217243. 12,143 UC/KC 18. AT
NO RET(L) RATIO RRT(L) RATIO AMNT AHNT(L) R. FAC RFAC(L) RATIOJ 11:48 100 10M 100 10. M 10. M 1MB 1 MO JLM2 2:48 8.238 40. M M.. 8.4203 4(28 ..''•,381 40. M '•" 1784'4 8:24 0.-4A3 40. M 1797 'S A:40 0.SA7 40. M 0.299 Ql-4 8:45 IM f. 748 IM 0.99 48, M 0.023 8.945 .B.12142877 9:18 0.792 299.98 • 0. OA4B 9:18 0.792 399.98 8.0A6
9:55 0.844 399.98 0.125"10:47 0.918 40. M 1121 flfRPri
t V .ai
«ET(L> RATIO RRT<L> RATIO AUNT AMNT(L) R. FAC R.FAC(L> RATIO18:19 0.B79 48. M 2.308
. , 11:23 0.970 . 40. MkJ 12:39 107B 40. M" 13:19 1134 08. M
13:47 IM >4L173 ;L M 8,97 48. M 0.01414:32 .'1238 40. M14:29 IM 1234 IM 2,71 299.98 0. Ml
721302840
1 484 0. 01771084 0.01
18:88 '.;.,*. 339 48.0014:22 *.394 . 40.M *?-*• A.*** >'21: H IM 1000 IM 10.M 10. M 1MO 1 MO IM14:28 1398 48. M 0.88416:40 1420 40. M 016518:12 1880 48. M 0.204
•4 18:24 1347 40.00 1128*5i 18:88 1418 48. M 1288at 19:37 100 1471 IM 8.87 . 48.M 0. M3 1788 0. M.17 19:40 1475 40. M 0.929ia 19:40 1475 . 40. M 0.88419 19:31 1442 48. M 1434as 28:47 1771 40. M 0.344/31 22:14 1894 40. M 144432 22:82 194B 40. M 0.232JB 28:84 100 10M IM 1000 10.00 1000 1000 IM*4 24.27 IM 2.M2 IM 8.15 40. M 0.802 0. AST 0. MOS 24:36 2.095 40. M 1473pb 24:42 2.184 40. M 1344$7 24:83 IM 2.247 1M 8.89 40. M 8.883 1248 0. M•R 27:81 2,372 40.M 2.281*U 31:87 £449 .. 40. M 0.919*B 38:20 3.244 40. M 184441 48:25 3.457 40. M 1477•J42 14:29 IM 1234 IM 8.58 10. M 0.874 1021 0.84*3 24: M IM & 223 1M 9.97 10. M 1739 1745 IM44 35:26 IM 3.017 IM 12.14 10. M 2939 2.421 121
Q t 014288
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INSTRUMENT BLANKVOLATILE LOW SOLID
OUb teat; Mud CanpuCriam .
A. SURROGATE SPIKE RESULTS
COMPOUND
diVToluim
d4>l,2>D1eh1orMthin(
IroMflMorobtnzint
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FRACTION
VOA
VOA
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coNc(ug/kg )
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PROCEDURE: RK DIAGNOSTIC REPORT 2/13/B4 11:26:47DATA FILE: CB840213A1BREFERENCE: V238JIETHODi V238 INITIALIZATXON OPTION: 2 PROCESSING OPTION: 3rjEPORT: V23BS1
< —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - LIST NAMES - 3r PROC USED P08B RM8 PRDC USED POBB RMB STANDARD/UNKNOWN' 3 2 1 0 44 S 1 6B V23B81/VE3BU1
44 COMPOUNDS PROCESSED, S FOUND
< COMPOUND X ——NO LIB ENTRY REF1 PS 1 -2318 PA 1 -4133 P7 1 -4934 PS 2-553 PS 3 -896 PS 4 -1087 PS 5 -1328 PS 6 -1739 PS 7 -1B410 PS B -18411 PS 9 -1961* PS 10 -21313 PS 11 -20414 PS 12 -225IS PS 13 -249.14 PS 14 -263PP5 15 -272
PS 16 -28719 PS 17 -2B620 PS 18 -31421 PS 19 -3222£f P4 2 -32323 P6 3 -32924 P6 4 -35825 P6 5 -36226 P6 6 -37327 P6 7 -3862B P6 B -38729 PA 9 -38730 PA 10 -38431 PA 11 -40938 PA 12 -43833 P6 13 -43034 P7 2 -48135 P7 3 -4B434 P7 4 -4BA37 P7 3 -518SB P7 A -54839 P7 7 -6124* P7 B -75341 P7 9 -79842 PB 2 -285
————— SEARCH ————— ——— X BAT X ———— CPREO BEL DELTA PEAKS PIT PEAKB H/E TOP231 231 1 956 .130 23J413493 49354BB107131172183183 '.19A2132042252492A32722B72863143223233293583623733863873873844094384504B24B34875195496137538002BS 285
79 4131 995 . 55 493
5094A26484 172SB 1B456
. ... .,•. S3•.."••••"''•.• 101
7A 204..,„„. 9A
.,.-. 4M*1l8i, AS„..*.„.,..- »*
, , 63 2726272 28697
.1174312765751307B9775127A3 .173SB5883 ' 4BS16492 511112106104
i 992 ! Oi$29&:
CHRO *••»•»»•«« 3*DELTA PEAKS
OreP8 3 -514 .513 514 -1 1 976 . 100 3144 -697 698 699 i 1 993 . 176 699
aUANTITATION REPORT FILE: OBB40213A1B
[3ATA: G8840213A1B, TI32/AS/84 10:43:00BAILIE: 10 ML H20 + 3 UL 199901.18983 ON 018SUBMITTED BY: 018 ANALYST: 633
LAMOUNT-AREA t REF. AMNT/<REF. AREA>» REBP. FACT)r/REBP. FAC. FROM LIBRARY ENTRY
NO NAME .r.1 t BROMOCHLOROMETHANE (XB)S 221 CHLOROMETHANE3 220 BROMOMETHANE4 231 VINYL CHLORIDES 209 CHLOROETHANEA 222 METHYLENE CHLORIDE7 252 ACETONE (2-PROPANONE)8 201 ACROLE1N9 , 202 ACRYLONXTRXLE18 i238 TRXCHLOROFLUOROMETHANE11 284 CARBON DXBULFXDE12 21A 11-OXCHLOROETHYLENE13 214 11-OICHLOROETHANE14., 22A TRAN8-1,2-OICHLOROETHYLENE15 211 CHLOROFORM1A 215 I 2-OXCHLOROETHANE17 2S3 2-BUTANONE18 227 111-TRICHLOROETHANE!__. 20A CARSON TETRACHLORXDE2(9 « 2-BROMO-l-CHLOROPROPANE21 257 VINYL ACETATE22 212 BROMODICHLOROMETHANE23 217 1 2-DICHLOROPROPANE24 250 TRANS-l 3-OXCHLOROPROPENE ''—25 229 TRICHLOROETHYLENE26 203 BENZENE27 228 112-TRICHLOROETHANE28 218 CIB-1.3-OXCHLOROPROPENE29 208 DXBROMOCHLOROMETHANESB 210 2-CHLOROETHYL VINYL ETHER31 203 BROMOFORM32 256 4-METHYL-2-PENTANONE33 * DICHLOROBUTANE34 2SS 2-HEXANONE35 223 112, 2-TETRACHLOROETHANE36 224 TETRACHLOROETHENE37 225 TOLUENE3B 207 CHLOROBENZENE »..39 219 ETHYLBENZENE ........ ... '" r ... . . . . . .'• ..40 251 BTYRENE41 239 0-XYLENE42 0 D4-1,2-OXCHLOROETHANE43 0 , DB-TOLUENE44 0 BROMOFLUOROBENIENE 014294
M/E SCAN TXME,VREF RRT HETH AREA(HCHT) AMOUNT XTOT
NO M/E SCAN TIME REF RRT METH AREA(HCHT> AMOUNT XTOT1 130 231 11:45 1 1000 A BV 86306. 10.000 UC/KG 15,96r*\ NOT FOUND':J NOT FOUND4 NOT FOUND5 NOT FOUND6 64 172 8:45 1 0.745 ABB 14620. 1640 UC/KC 2,627 58 184 9:21 1 0.797 ABB 1033, 1948 UC/KC 3,11B NOT FOUND9 NOT FOUND
10 NOT, FOUND - "•"••" ••" ••' "•"• "' '(;11 74 204 10:22 1 0.883 ABB 393. 0.026 UC/KC 0.0412 NOT FOUND13 NOT FOUND14 NOT FOUND15 83 272 13:50 1 1177 ABB 2645. 0.194 UC/KC 0,3114 NOT FOUND17 72 2B6 14:32 1 i. 238 A 88 2563, 2.641 UC/KC 4.2218 NOT FOUND19 NOT FOUND20 79 413 21: M 20 1000 A BB 35329. 10.000 UC/KC 15.9621 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND '"r" '•—:•" ' ''25 NOT FOUND24 NOT FOUND27 NOT FOUNDJNOT FOUND
NOT FOUNDSB NOT FOUND31 NOT FOUND38 NOT FOUNDS3 55 493 25:04 33 1000 A BV 82071 10.000 UC/KC IB, 9634 NOT FOUND35 83 483 24:33 1 2.091 AtBB 347. 0.023 UC/KC 0,0436 NOT FOUND37 92 318 26:20 1 2.242 AtBB 542. 0,041 UC/KC 0.0730 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND42 AS 285 14:29 1 1234 A BV 71864. 7.323 UC/KC. 116943 IM 514 26:08 1 2,223 ABB 1S42A5. 8.7B9 UC/KG, 14,0344 176 699 35:32 1 3.026 ABB 236378. 10.023 UC/KC 16, 00
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R, FAC RFAC(L) RATIO1 Hi 46 1 00 1 008 1 00 10. M 10, M . 1 000 1 M0 1M2 2:54 0.246 40. M V"" •' 0.449 •3 4:34 0.388 v 40. M * 2.093 .4 3:32 0.478 40. M'•'''•'•";.""'.2,1W3 6:46 0.573 40. M 0.3956 8:48 0.99 0.746 100 164 40, M 0,042 1.033 0.047 9:24 0.99 0.797 100 195 299.98 0. 000 0.061 0. Bl8 9:24 0.797 399.98 tf. 335P18:01 0.649 399.96 0.176
10: S3 0,926 40, M 1.976
, . v v'i
11 11 10:22 1,0(1 0.879 1,00 0.03 40.00 0.002 Z, 681 0. M11:26 0.970 40.00 0.87612:42 1.078 40. M 0.363
IV 13:22 1134 40. M 0.64913 13:80 100 1172 IM 0.19 40. M 0.008 1696 0.0016 14:33 1,237 40.00 0.875
. 17 14:32 100 1233 IM 2.64 299,98 0. Ml 0.113 0.01I IB 16:01 1358 40. M 1114
19 14:25 1392 40. M 134920 21:03 1M IBM 100 10. M 10. M 1M0 1M0 IM21 16:25 1.392 .48,09 9,89328 16:43 1418 40. M 0.17723 18: i5 1,347 40.00 0.23824 18:27 1.545 40. M 1.29525 19:01 1412 40. M 1.38424 19:37 1.444 '" 40. M 194627 19:40 1648 40. M 10282B 19:43 1472 40. M 0.67329 19:34 1489 40.00 151530 20:30 1747 40. M 0.41631 22:14 1BBB 40. M 156732 22:56 1.944 60,09 0.30833 25:07 1M 10M 1M 10.00 10. M 10M 1000 10034 24:27 & 073 60,00 0.97033 24:39 108 & 991 109 0.02 40. M 0.001 1774 0.0036 24:45 2.099 40. M 144837 24423 109 a 237 1,09 0.04 40. M 8. M2 1537 0. MSB 27:54 2.346 40. M fc 497{*_, .31:10 a 642 . 40. M 1121Jftr 38:26 3.259 40. M Z. 38341 40:43 3.453 40. M 1.46342 14:32 100 1233 1.00 7,32 10, M 0.829 1133 0.7343 26:11 100 a 220 IM 6,79 10. M 1767 2.034 0.6644 35:32 1.00 3,013 1.00 10,03 10. M Z. 739 2,732 1,00
Q i 014296
o
O 014297
, U.I. ENVIRONtNTAl. PROTECTION AGENCY - CLP imp 11 MintgnMnt Oft let' P.O. tm 111, Alwandrla, Vlrglnli 22313 - 703/JJ7-J4W
O ORMNISS ANALYSIS DATA SHEET
Lrtcrntory NIMI CO-BUHV-JI_____________ CiM Nwe*rLH> InpU ID Not ^HHUalfe__________ QC Htport No..IwpltMitrlKi lellii _____________ Contrict No.t.Dati Itolmi Autlwriito iiyi - Dft* Smelt Rictlvtat
- toT ua-
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CmdKTMTIONi (__) WOIUM HIOH (clrda) tOMDrmATIONi ION WDIUM HUM lelrel* en*)BATt KTIWCTlO,f1«FAI«Ol f - 3-- BATlDATE MMimOl J"l»"ftH. PATl AKALTZtDlmam NOIITUKI __________________ pwawr noiituKtAssociated iimples iqs'&g, ~uq. ____ Associated samplesHylllply Dtttetlon llnlta by I ftHor|"f Multiply Dtttctlofi Unlti by 1 QerQ ____
(Clwek Ion for Aptroorlat* Factor) _ (Ctnck Ion tor Approrlatt Factor)M>l CAW . opUujA.8
lelrelt onilllDrln__________4.rll
iroyMK-VKM.giiiij»iH-:a.vc-
UkJJ-iiHQlDin-aM-Mtip."" te»ie»nm
DIOKIH5
CONCCNTRATIONl LOW KOIUM HIM (Orel*)BMI AHALYttCl •wicoit nHimifci ^Associated iimples:______ yg/g
or yg/Vj(elrclt ont)
July, 19!!
VOLATILE LOW SOLIDQ ORGANICS ANALYSIS DATA SHEET - Page 3
Lib Nine! Held CompuChem
Ub Simple I.D. *.__£_____ __ SS D Ds __ B1«nl!
A. SURROGATE SPIKE RESULTS
COMPOUND
(IB-Toluene
dM,2-D1:nl3roethine
Bromofluorobenzene
FRACTIONVOA
VOA
VOA .
"}•
CONC(ug/kg )
°i.<n"ML.
10. f r"
'••
•••'.•.;
(Surrogates only)Spine
Added (ug/kg )
10
10
' 10
••'V.VA"
-K*>»*»*,''.''
(Recovery
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im
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.
03DD
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0 ^ ' «
* CH
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it*-* ' ,__.O( _
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,ll*«k t
Cut
Z/
OC Sue It
iisn
SwellNtlght (g)
/ ff.it
Afl
0.3S"
da
Datt SerMnt
lurrogftt No. Idwdult
tt-fltl———
:.-., taount NMMII) Counttr I.W Lot______________
^ J-S-89/53"
•Jf l»T
" v' COMPUCHEM NO. IQQleA DATE _____ 1 of 2COMPOUND LIST NO. ____ "~""~~""""
———— IDENTIFIER VOLAT1LES - LOH LEVEL SOLID"> —————————————————"•-'' • • (IUANT.
COMPOUND REPORT CORRECTION RESULTS DETECTIONCOUNTER NUMBER COMPOUNDS VALUE K FACTOR • (ugftgl LIMIKuaAfl)2. 221 CHLOROMETHANE ............3. 220 BROHOMETHANE .............4. 231 VINYL CHLORIDE ...........5. 209 CHLOROETHANE..............6. 222 METHYLENE CHLORIDE .......7. 252 ACETONE ..................6. 201 MROLEIN .................9. 202 ACRYLOHITRILE ............10. 230 TRICHLOROFLUOROMETHANE ...11. 254 CARBON DISULFIDE .........12. 216 1,1-DICHLOROETHYLENE .....' 13. 214 1,1-DICHLOROETHANE .......14. 226 TRANS-1,2.DICHLOROETHYLENE'15. Ul ..CHLOROFORM ...............
*)16. 215 ''"i' lCKLOROETHANE .......*17. 253 2-BUTANONE ...............IB. 227 1,1,1-TRICHLOROETHANE ....19. 206 CARBON TETRACHLORIDE .....21. 257 VINYL ACETATE ............22. 212 BROMODICHLORONETHANE .....23. 217 1,2-DICHLOROPROPANE ......24. 250 TRANS-1,3>DICHLOROPROPENE.25. 229 TRICHLOROETHYLENE ........26. 203 BENZENE ..................27. 228 1,1,2-TRICHLOROETHANE ....28. 218 CIS>1,3, DICHLOROPROPENE..29. 208 DIBROMOCHLOROKETHANE .....30. 210 CHLOROETHYLV1NYL ETHER....31. 205 BROMOFORM ................32. ' 256 4 €THn.2.PENTANONE .....34. 255 2-H.XANOHE ...............35. 223 1,1,2,2'TETRACHLOROETHANE.
PLEASE COMPLETE CORRECYlON FACTOR CALCULATIONS ON SECOND SHEET OF THE
COMPUCHEM NO. iQQbA DATE Z of 2COMPOUND LIST NO. -
———— IDENTIFIER VOLAT1LES - LOH LEVEL SOLID
Q • QUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS________ VALUE x FACTOR • (uo/kal LlHlTtug/kg36. 224 TETRACHLOROETHENE37. 225 TOLUENE38. 207 CKLOROBENZENE39. 219 CTHYLBENZENE40. 251 STYRENE41. 239 0-XYLENE
QUANT.COMPOUND SURROGATE REPORT MOUNT •-* t RECOVERYNUMBER COMPOUNOS______ VALUE SPIKED RECOVERY HNDOH258 D4-1,2,DICHLOROETHANE (SURR) 1.HL 10.0 7l" (50-150)*233 OB-TOLUENE ISURR).......... JLH •••••J__2.' ^ (81-1201247 BROMOFLUOROBENZENE (SURR).. . /L\ M 10.0 )&/ (57-137)*
*A*»1sory Llilts^ % Recoviry • Quint. Report Value
Moum spueo *
CORRECTION FACTOR CALCULATION: Instrument Code 238|0 g '. _____
Ver Hi. of unple used " Dilution Fietor » DV "•<•"*
10 fl
014303O . JRT 11/83
s————,————._.___———,_ _ _.. ___?-J1 _ ^»B-
•2 " ' "8
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PROCEDURE: RK DIAGNOSTIC REPORT 2/86/84 11:30! 42DATA FILE: CH01996BA18REFERENCE: V23S
vsaa INITIALIZATION OPTION: s PROCESSING OPTIONI aV23BS1
•C —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - LIST NAMES - > .,,.PROC USED P088 RMS PROC USED POSS RMB STANDARD/UNKNOWN ?/|
U S i 0 . 44 6 1 SB V23BS1/V23BU1
44 COMPOUNDS PROCESSED, 6 FOUND;.,•.• •• . ..V..'.:-W' ••.»-.««!• is:..
< COMPOUND X ———————— SEARCH ———————— X SAT X ———— CHRO ————— :NO LIB ENTRY REF PRED 8EL DELTA PEAKS FIT PEAKS M/E TOP DELTA PEAK T1 PS 1 -238 230 230 . 1-960 . - 130 230 . 1.S P6 1 -4.1 412 , , . . .79 4123 FT 1 -491 492 492 . ... 996 , 53 492 . i4 PS 2 -S3 . 92 . . , . 50
' H PS -.a -87 B6 . , ....... - . .94 . .A PS 4 -105 104 . . . . . 62 ....? P S S -130 1 2 9 . . . . . 6 4 . . .B PS 6 -171 170 . . . . 84 171'» PS 7 -182 1B1 . . . . . ... ,98 18310 PS 6 -182 1B1 . . . . '3614. PS 9 -194 193 . . . . 53IE PS 10 -211 211 . ......nxrifp.Mi" ••••-. 101 ...13 PS 11 -202 201 , . . 76 203 i14 PS 12 -223 223 . . . 9615 PS 13 -248. , . 248 . . . . . . . 65 . . .Mfc PS 14 -261' 861 , . . " 96 .W PS IS -270 270 . . ..• '."• . 83 270 . A1 9 P S 1 6 -28S 2 6 3 . . . . . 6 2 . .1? PS 17 -284 284 2B4 . 1 937 72 2842 f t P S 1 8 -313 3 1 3 , , . . . 9 7 3 1 321 PS 19 -320 320 . . . . 11722 P6 2 -321 321 4323 F6 3 -327 327 . . , . 1272 4 P 6 4 -357 3 3 7 6 5 , .2B P6 3 -361 361 , , . . , 7S2 C « P 6 6 -372 3 7 3 . . . . . 1 3 0 3 7 22 7 F 6 7 -3B4 3 8 3 . . . . 7 8 3 8 52 0 F 6 B -385 3 8 6 . . . . . 9 7 3 B 729 F6 9 -3B6 3B7 , . . . 7530 F6 10 -383 384 , . . . • :127 383 . i31 F6 11 -408 409 . . . ,63 412"X: F- 12 -436 437 . . . ... 173 43T33 F'6 13 -44B 449 , , . . , SB 449 . .34 P7 2 -479 4BC , , . . , 5 8 4 6 0 .M) F7 3 -483 4B4 , . , . ..,.,„, B3 4B3 .36 F7 4 -465 486 , . . ..,.•.•«.», ••~.4_4 • 485 '. *37 P7 3 -S16 B17 , ." . • •„,. ,.•'.:,•'.*, 92 .,917'.'. . I3B P7 6 -946- 548 . . ' . ' ' .;/ " 112 ,'',948 . .3? P7 7 -609 611 . , . . ,"• 106 610 . i40 P7 8 -748 731 104 732 . :4 1 F 7 9 -791 7 9 4 . , . . . -106 7 9 3 . Z4R PE 2 -284 284 2B4 . 1 986 63 284_f_ F'6 3 -512 513 S13 . 1 979 108W re 4 -691 1694 694 , 1 991 , 176
3UANTXTATXON REPORT FJ.LC: CM8J.V96BAJ.B
DAIiy GH01996BA18, TI83TV84 10i 58: (103AMH.E: 10 ML SMPLE #19968 + S HI. 109111,10936 ON *IBSUBMITTED;BY: #13 ANALYST: 633
AMOUNT-AREA t REF, AMNT/(REF, AREA)* REBP, FACT)FAC. FROM LIBRARY ENTRY
NO NAME1 « BROttOCHLOROMETHANE (IS)& 221 CHLOROMETHANEM 589 BRvnOnCTHnNE •VF"* .4 231 VINYL CHLORIDES 209 CHLOROETHANE6 222 METHYLENE CHLORIDEV 392 ACETONE (2-PROPANONE)0 201 ACROLEXN9 202 ACRYLONITRILE
Itt 230 TRICHLOROFLUOROMETHANE1J, 2S4 CARBON DI8ULFIDE1!? 216 1,1-DXCHLOROETHYLENE13 214 1,1-DXCHLOROETHANE14 £26 TRAN8-1,2-DXCHLOROETHYLENE1& 211 CHUOTOWW1 •'-"'-16 215 1.2-OXCHLOROETHANE,1V £53 2-BUTANONE.IB 227 1,1,1-TRICHLOROETHANE. £06 CARBON TETRACHLORXDE">r""'-a-BROMO-l-CHLORQPROPANE'
£fl 257 VINYL ACETATEas 212 BROMODICHLOROMETHANEaS 21V 1,2-DICHLOROPROPANE-4 250 TRANB-1,3-DICHLOROPROPENK2'.', 229 TRICHLOROETHYLENE?.<< 203 BENZENE2V 228 1,1, 2-TRICHLOROETHANESI* SI 8 CIS-1, 3-DICHLOROPROPENE:•"/ 206 DIBROMOCHLOROMETHANE3d SIC b-r,HLOROETHYL VINYL ETMF.R3.L E85 BROMOFORM3 256 4-METHYL-2-PENTANONEar« * OICHLOROBUTANE3't 255 S-HEXANONEiV; 223 1< 1, 2, S-TETRACHLOROETHANK'J(, 224 TETRACHLOROETHEiME3? 225 TOLUENE3& £07 CHLOROBENZENE3V 219 ETHYLBENZENE '.,._;>40 231 8TYRENE "...''.4J. 239 0-XYLENE * .4ft #""' 'D4-1,2-DICHLOROETHANE4t. » D8-TOLUENE44 * BROMOFLUOROBENZENE
O ^/E SCAN TIME REF RRT METH AREA(H6HT) FWOUNr XTOT
10 ' I U'01430
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT 54TOT1 130 230 11: 41 1 1. 000 A BB 91414. 10. 000 UG/KG 14, 17
*-N NOT FOUND ;'••J NOT FOUND
ii NOT FOUNDP NOT FOUND6 84 171 8:42 1 0.743 ABB 9069. 0. 953 UC/KG 1.35? 58 183 9: IB 1 • 0. 796 A BB 761. 1. 06S UC/KG 1, 510 NOT FOUND9 NOT FOUND
10 NOT 'FOUND ' '•?*•*•• '1J, 76 203 10:19 1 0,883 ABB 629. 0. 029 UG/KG 0,0419 NOT FOUND13 NOT FOUND14 NOT FOUNDIK 83 270 13: 43 1 1, 174 A BE) 3479, 0, 218 UG/KG 0. 3116 NOT FOUND17 72 '" 284 14: 26 1 1. 239 A BB 4B92, 4, 998 UG/KC 7. 02Id 97 313 19: 99 1 1, 361 A BB 496. 0. 049 UG/KC 0. 06If NOT FOUNDW> 79 412 20:97 20 1,000 ABB 37928. 10, 000 UG/KC 14. 17?.}, NOT FOUND221 NOT FOUND23 NOT FOUND34 NOT FOWB "• •« •»'• "'•£K 130 372 IB: 59 1 1. 617 A BB ,3068, 0. 234 UC/KG 0, 3326 78 38S 19:34 1 1,674 ABB 903, 0, 049 UC/KG 0,6727 97 387 19: 40 1 1. 683 A BB . 741. 0. 074 UG/KC 0, 11 •ML NOT FOUND'V 127 383 19: 28 1 1. 665 A BB . 696, ' 0. 046 UC/KG 0, 07'dP 63 41? 28:37 1 1,791 A BE! 625, 0, 123 UC/KC 0,173J. 173 43V 22: 13 1 1, 900 A BB 2653, 0. 172 UC/KC 0, 24M. 5B 449 22:49 1 1.938 ABB 2548. 0. 942 UG/KG 1.33:<•' 35 492 23: 01 33 1. 000 A BB 89740. 10. 000 UG/KC 14. 1734 SB 480 24: 24 1 2. 0Q7 A BB 9396. 2. 366 UG/KG 3, 353S 83 4B3 24: 33 1 2. 106 A BV 7509. 0. 471 UC/KC 0, 6736 164 485 24: 39 1 2. 10V A 8B 2338. 0. 171 UC/KC 0. 24m 92 51V 26:17 1 2. 24U ABB 3314. 0. 252 UC/KC 0,363f) 112 548 27:31 1 2,383 ABB P1C6, 0. 333 UC/KG 0. 483V 106 610 31:00 1 2.652 ABB 2863. 0, 304 UC/KC 0,434C> 104 752 38:14 1 3,270 A»BV 6978. 0. 369 UO/KC 0,354J 106 793 40: 23 1 3, 437 AtBV 4462. 0. 377 UC/KC 0. 5343 65 284 14:26 1 1, 235 ABB . 73164, 7. 465 UC/KG 10, 574H 100 513 26: OS 1 2. 230 A BB 151602, 9, 466 UC/KC. 13, 4144 176 69B 35: 20 1 3. 022 A BB 192793, 10. 103 UG/KG 14. 32
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R, FAC R, FAC(L) RATIOJ. 11: 3H 1. 00 1. 000 1, 00 10. 00 10. 00 -• 000 1. 000 1. 003 2:4E 0.231 . • 40. 00" "*" .'.iP ;• 0.306 .:) 4:19 . 0.371 H;40.' 00 ' 1.342.<> 5:17 •••454 • 40.00 1,236S '6:30 0.959 40.00 0,259ft 8:38 1.01 0,742 1,00 8,95 40,00 0,025 1,041 0.02f 9:12 1,01 0.790 1,01 1.07 299,99 0.000- 0,078 0.00H 9:ja 0.790 399,99 0.081* 9:49 0.843 399.99 0.184
.0:400.843 399.9 .14 niJOA-.0.917 40.00 1,592 U14J07
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L> R, FAC R. FAC(L) RATIOil, 10:13 1,01 0,678 1,01 0.03 40.00 0.002 2,386 0,00\ 11:17 0.969 j 40,00 0. B84
... 12:33 1079 40, 00 0, 37114 13:16 1140 40, 00 0,689J15 13:4B 1,00 1179 1,00 0.22 40.00 0.010 1,744 0.0116 14:39 ' 1 243 40. 00 0, 9291? 14: £6 1 00 1, 240 1. 00 4.96 299, 99 0. 002 0, 108 0, 021« 15:55 1 00 1 367 1, 00 0. OS 40, 00 0. 001 1, 193 0,00IV 16:16 1397 40,00 1,68520 20:97 .100 1000 1,00 10.00 10,00 1(300 1,000 10021 16:19 1402 40,00 0,9632L> 16:37 1428 40,00 0,188,aa 18:09 1999 40.00 0,24624 18:21 1576 40,00 1,3492L', 18:55 1, 00 1624 1, 00 0. 23 40, 00 0. 008 1, 43526 19:31 1 0(1 1677 1. 00 0.03 40. 00 0. 002 2, 003PY 19:37 • 1 00 1 686 1 00 0. 07 40, 00 0. 002 1, 08929 19:37 1686 40,00 0,703
, M 19: £8 1 00 1672 1.00 0,09 40! 00 0.002 l! 6541 30 SO: 44 1 01 1 762 1, 01 0, 18 40,00 0, 002 0,997
Q
.0100.00
.0031 22:13 1.00 1908 1.00 0,17 40,00 0,007 1689 0. 00'M 22:49 1, 0H 1,961 1,00 0,94 60.00 0.009 0,296 0.02•33 S3:01 100 1,000 1.00 10,00 10,00 1.000 1,000 1.0031 24:24 -. 100 2.096 1.00. 2.37 60.00 0.010 0,290 0.04315 24:36 10(1 2.114 0.99 0,47 40,00 0,021 1,745 0.0136 £4:37 1,00 2.118 1.00 0,17 40,00 0,006 1,494 0.00yi 26:17 100 a 298 100 0.23 40.00 0,009 1,438 0.01527:48 1 00 a 389 1.00 0,34 40. 00 0. 022 2, 622 0. 01
31:00 i. Mi a 664 1.00 0.30 • 40.00 0.008 1,039 0.0140i 38:11 1 0ft 3,279 1. 00 0, 37 40, 00 0, 019 2,067 0, 0141 40:22 100 3.467 1.00 0,38 40,00 0,012 1,296 0. 014fc! 14: 'd'J 1 00 1 236 1, 00 7, 47 10, 00 0. 800 1, 072 0. 7540 26: OS 1 00 2. 240 1. 00 9. 47 10. 00 1 658 1. 752 0. 9544 35:1Y 1 00 3, 031 1 00 10, 11 10.00 2. 109 2.0B7 1 01
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' OHWIISS»AUSIS DATA SHEET
lHWittry NMI 'enmiiCM- CM NwMr _Lit lMpl* ID Not,_____SlPVt-ll________ «CMeort No..
|Tl Ip li Httrlxi tent____.__________ ContrietNo.i b^-ot »Diti RtltMi AirttMrii«a «ri ________________ Dit* imp It Rtnlvidi
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eOWEKTMTIONl ( _pW)IUM NI9H (elrclt) OONCnrfflATIONl UN WDIUH HI8H (clrcl* «n«)DATE nTMCTO/MEPAICDi ^ *.'<>"'(f M™ K™«TIB/IW«BI| ,________MTEMMLTHDl A.lQ'ftH DATEMMLTZIDl ______________WCEMT MOItnMCi _____________________ flUCUfl MDIITUKlAssocl.tid Miples (Q&bO-_______ Assoclited simplasMultiply DtttctlM llnlti ty 1 ]_(- Q _____ NiltlMv Dtttctlon Ililti ky I QorQ ____
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CAW or ugAg(elrcli eni)•t iil£_U
UN WDIUH HIBH (etreit)DATE EXTftACTED/nKr'MDiDATE WM.T2EDIPtKENT mnUK
July, 1989
VOLATILE LOW SOLIDMGANICS ANALYSIS DATA SHEET - P«ge 3
,>Lib Hint; Mild CoBDuCh-mUb Simple I.D. W>.dJt>\d\ QSS ~]OS [S&link
A. SURROGATE SPIKE RESULTS
COMPOUND
dB-Tolutne
d4-l,Z-D1eftl9roithine
Iropifluorobenzine
FRACTIONVOA
VOA
VOA
CONC (us/kg )
fo,t$*.(911,05-
•
. .. ,
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10
10
10
tRieoviry
107
<%*-no
V*,!'
.1 IN OJ
S ^
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1 313
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8s
COHPUCHEH NO. ____/__/ DATE » 1 of 2COMPOUND 11ST NO. """ ™———— 1DENT1F1ER YQLAT1LES .. LOV LEVEL SOLID
QUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS VALUE K FACTOR • (ufl/ka) LlMITJ.Q/kg.
2. 221 CHWRONETHANE ............ ___ FT I ___ 2.S220 IROHOMETHANE ......231 VINYL CHLORIDE ....209 ' ''CHLOROETHANE.......122 KTHVLENE CHLORIDE252 . ACETONE ...........201 ACROLEIN ..........202 ACRYLONITRILE .....
10. 230 TRICKLOROfLUOMHETHWIE ...11. 254 CARBON DISULFIDE .........12. 216 I,I.DICHLORO_THYLENE .....13. 214 1,1-OICHLOROETHANE .......14. 226 TRANS.1,2-OICHLOROETHTLEUE15. 211 CHLOROFORM ............... ___ .IS. US W-OICHLOROETHANE ....... g___,. ..»
253 .2-BUTANONE ............... __,____«;,,..18. 227 l.l.l.TRICHLOROETHANE .... ___19. 206 CARBON TETRACHLORIDE ..... ___21. 257 VINYL ACETATE ............ ___22. 212 BROMODICHLOROMETHANE .....23. 217 1,2-DICHLOROPROPANE ......24. 250 TRANS-1.3-DICHLOROPROPENE.25. 229 TR1CHLOROETHYLENE ........26. 203 BENZENE ..................27. 228 1,1,.-TR1CHLOROETHANE ....28. 218 CIS-1,3, DICHLOROPROPENE..29. 208 DIBROMOCKLOROMETHANE .....30. 210 CAOROETHYLVINYL ETHER....31. 205 IRONOFORM ................32. 256 44ETHYL-2-PENTANONE .....34. : 255 MEXANONE ...............35. 223 1,1,2,2-TETRACHLOROETHANE.
2.52.52.5
(fi 2.55050502.5
2.52.52.52.52.51002.5
2.52.52.52.52.52.5
2.52.52.55050
QlEASE COMPLETE CORRECTION FACTOR CALCULATIONS ON SECOND SHEET OF THE COMPOUND LISTIII01431500~.fi 3
COHPUCHEM NO. JOItt DATE ______ 2 of 2COMPOUND LIST NO. ____ -
———— IDENTIFIER VOLATILE5 - LOH LEVEL SOLID
0 QUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS________ VALUE K FACTOR • (uo/ko) LlMlT(.g/kg36. 224 TETRACHLOROETHENE......... ___37. 225 TOLUENE................... ___38. 207 CHLOROBENZENE............. ___39. 219 ETHYLBENZENE ............. ___40. ••• 251 STYRENE...................___41. 239 0-XYLENE.................. ___
COMPOUND SURROGATE REPORT MOUNT 1 * I RECOVERYNUMBER COMPOUNDS VALUE SPIKED RECOVERY MIHDOH258 D4.1,2,DICHLOROETHANE (SURR) 3.19 10.0 <&-, (50-150)*233 Oj-TOLUENE (SURR).......... VfA 10.0 ' lt>~> (81-120)247 BROMOFLUOROBENZENE (SURR).. |l.0fl- 10.0 Hi) (57-137)*
•Advisory Unitst * Rtcowy • Quint. Report Viluemount spueo * »"•• .........
CORRECTION FACTOR CALCULATION: Instrument Code 23810 j____
Her Ht. of simple used x Dilution Fietor * *n MW FKtqp
10 g9
O , JRT 11/83
"*'** t;.
'ROCEDURE: RK DIAGNOSTIC REPORT ./10/B4 3:06:493ATA FILE: GH080141C1B*E«RENCE: V23B' -...E-THOD: V23B INITIALIZATION OPTION: 2 PROCESSING OPTION: 3REPORT: V23B81
. < —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - L.X8T NAMES - >PROC USED P03B RM8 PROC USED P08S RMB STANDARD/UNKNOWN
3 3 J, 24 44 6 1 36 V238Sl/V233Ui
44 COMPOVJN03 PROCESSED, 6 FOUND
< COMPOUNDNO LIB 'ENTRYX PS'3 P6fl PT4 PSS PSk PS7 PSB PS9 PS10 PSU. PS12 PS13 PS14 PS
PSPS
17 PS18 PS19 PS20 PS21 PS22 P623 P624 P625 P626 P627 P623 P629 P630 P631 P633 P633 P634 P735 P736 P737 P738 P739 P740 P741 P7
44 PB 4 -696
U
QUANTITATION REPORT FILE:
DATA: CH020141C16, TI02A10/84 2:16:00sOlE: BOIL BLANK 20141 + 10 ML H20 + S UL (10983+18990)SUBMITTED BY: IB ANALYST: 714
AMOUNT-AREA t REF, AUNT/(REF. AREA)* RESP, FACT)RE8P. FAC. FROM LIBRARY ENTRY
NO NAME' 1 * BROMOCHLOROMETHANE (IS)2 221 CHLOROMETHANE3 220 BROMOMETHANE4 231 VINYL. CHLORIDEa 209 CHLOROETHANE6 222 METHYLENE CHLORIDE7 252 ACETONE (2-PROPANONE)fl 201 ACROLEIN9 202 iACRYLONZTRILE10 230 TRICHLOROFLUOROMETHANE14 2S4 CARBON DISULFIOE18 216 1,1-DICHLOROETHYLENE13 214 1,1-DICHLOROCTHANE14 226 TRANB-li 2-DICHLOROETHVLENE15 211 CHLOROFORM
1 16 215 1, 2-OICHLOROETHANE17 233 2-BUTANONE| 18 227 1.1,1-TRICHLOROETHANEi 19 206 CARBON TETRACHLORIDE! ft • 2-flROMO-l-CHLOROPROPANESSf 257 VINYL ACETATE2& 212 BROMODICHLOROMETHANE23 217 J.2-OICHLOROPROPANE
! 24 250 TRANB-1, 3-OICHLOROPROPENE. 25 229 TRICHLOROETHYLENE26 203 BENZENE27 228 1,1,2-TRICHLOROETHANE2B 21B CIB-1,3-DICHLOROPROPENE29 208 OIBROMOCHLOROMETHANE3d 210 2-CHLOROETHYL VINYL ETHER31 205 BROMOFORM3B 256 4-METHYL-2-PENTANONE33 * DICHLOROBUTANE34 2SS 2-HEXANONE35 223 1, Ii ?i 2-TETRACHLOROETHANfc136 224 TETRACHLOROETHENE3V 225 TOLUENE38 207 CHLOROBENZENE39 219 ETHYLBENZENE40 251 8TYRENE41 239 0-XYLENE48 * D4-1. B-DXChLOROETHANE43 « DB-TOLUENE44 « BROMOFLUOROBENZENE
M/E SCAN TIME REF RRT METH AREA<HOHT> AMOUNT XTOf .
014319
NO M/E SCAN TIME REF RRT KETH AREA(HGHT) AMOUNT XTOT1 130 231 11:43 1 1,000 A BV 6B649. 10. 000 UG/KC 14, 39
NOT FOUNDNOT FOUNDNOT FOUND
S NOT FOUNDb 84 173 B: 'IB 1 0,749 A BB 9066. 1, 440 UG/KC 2, 107 NOT FOUND8 NOT FOUND9 NOT FOUND10 101 213 10:50 1 0.922 ABB 2830, 0. 348 UG/KG 0.5111 NOT FOUND19 NOT FOUND13 NOT FOUND14 NOT FOUND15 83 272 13: SO 1 1.177 A BB 3611. 0.321 UC/KG 0, 4716 NOT FOUND17 72 286 14:32 1 1.23B A 68 2487. 3,049 UO/KC 4.4318 NOT FOUND19 NOT FOUND M|20 79 **T*21:0e 20 1.000 ABB SSUTrV 10.000 UG/KG 14.3921 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND26 78 386 19:37 1 1.671 A BB 980. 0. 076 UG/KC 0. 1127 NOT FOUND28 NOT FOUND..j£| NOT FOUND2Sr NOT FOUND • ""'31 173 438 22:16 1 1.896 A BB 1834. 0. 143 UG/KC 0. 213B 58 450... 22:32 1 1.948 ABB 929_(fej4 0. 406 UG/KC 0.5933 55 499W25:04 33 1,000 A BV «99Tr""' 10.000 UG/KC 14.5934 58 481* 24:27 1 2,082 AW 63S5. 0.915 UC/KC 1.34311 83 484 24:36 1 2.095 A BB 4589. 0, 352 UC/KG 0.5136 164 486 24:42 1 2.104 A*6B 1074, 0. 100 UG/KC 0, 1337 92 519 26:23 1 2. 247 A BB 2114. 0, 225 UC/KG 0, 333D 112 550 27:57 1 2.361 A BB 5446, 0, 307 UG/KC 0, 433? 106 614 31:13 1 2.658 A*BB 1627. 0.234 UG/KG 0.3440 104 754 38:20 1 3.264 AtflV 6905. 0.342 UG/KC 0.5041 106 799 40:37 1 3.439 A*BB 4964. 0.393 UC/KG 0.3743 63 285 14:29 1 1.234 A BB 64112, B. 194 UG/KG 11,9643 100 814 26:08 1 2.225 A 88 ,124999. 10.684 UC/KG 15.5944 176 697 35:26 1 3.017 ABB 212152. 11.017 UC/KG'16.07
NO RET(L) RATIO RRT<L) RATIO AUNT AMNT(L) R. FAC R.FAC(L) RATIO1 11:41 1.00 1,080 1.00 10.00 10.00 1.000 1.000 1.002 2:45 0.23S 40.00 0.426» 4:28 0.383 40.00 . ..... 1.832 ; ...4 5:26 ••' 0.465 40.00 '" •'-"v 1771S 6:40 0.570 40.00 •>'•' 0.291'6 8:45 1,01 0.748 1.00 1,44 40.00 0.033 0.917 0.047 9:18 0,796 299,98 0,0910 9:18 0,796 399.98 ' 0,073» 9:55 0.848 399.98 0.G 10:47 1,00 0,922 1,00 0,39 40.00 0.010 1,
fr it
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R. FAC R, FAC<L> RATIO11 10:19 0. BBS 40,00 3,1371ZL 11:23 0. 974 40, 00 0.741: " 12:36 1. 078 40, 00 0.31314' 13:19 1.139 40,00 0.591153 13:47 1.00 1.178 1.00 0,32 40.00 0,013 1.63B 0.0116 14:32 1.243 40,00 0,92517 14:89 1.00 1.239 1. 00 3,03 299, 98 0. 881 0, 119 0. 01IS 13:38 1.363 40,00 1,11619 16:19 1,396 40.00 1,64230 20:97 1,W 1,000 1.00 .10,00 10.00 ,*t, 000 1,000 JL 0021 16:22 i, 400 40,00 ' 1,13022 16:40 1,426 40.00 0.19723 18:12 1,557 40.00 .0.22124 18:21 1,370 "" 40,00 1.29325 18:55 1.617 .40.80 141726 19:34 1, 00 i. A7» i. 08 0,08 40.00 0.004 1.873 0.0027 19:37 1.678 40.00 1.1192B 19:40 1,683 40.00 0.69929 19:28 1, MS 40.00 1,77030 20:47 1.778 40,80 0.48031 22:13 1.00 1.900 1.00 0,14 40.00 0.007 1.884 0,0032 22:49 1,80 1,952 1.00 0.41 60.80 0.002 0.333 0.0133 25:01 10* 1.000 1.00 10.00 10.00 1000 1,000 1,0034 24:24 1.80 £ 087 i. 00 0.92 68.00 0.019 1,011 0.0235 24:36 100 2.104 i. 00 0,35 40.00 0.017 1.898 0.0136 24:39 1,00 & 109 1.00 0.10 40.80 0.004 1.338 0.0037 26:80 1.00 1252 1.00 0,23 40.00 0.008 1,367 0.0136 27:48 1.81 2. 078 1. M 0.31 40.00 0.028 2.581 0.01O 31:04 tO« & 457 1.00 0,23 40.80 0.006 1.011 0,014Sr 38:14 1,00 3.270 1.00 0.34 ' 48.00 0,025 2.943 0,0141 40:31 1.00 3.465 1.00 0,39 40,8* 0.018 1,836 -0,0148 14:26 1.00 1.235 1.00 8.19 10.00 0.934 1.140 0.8243 26:05 1.00 2.230 1.00 10,68 10.80 1.821 1.704 1,0744 35:23 1.00 3,026 1.00 11.02 10,80 3.090 2,805 1,10
014321
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014325
V.f. WYIIIOWOITr. MOTKTIOH WtNCT - CU« !•*)• Hwij-wit 011lc*P.O. ft* lit, Almmdrli, Virgin)* 22313 • 705/5J7-24W
IMPLE NUW»
OMAN IDS ANALYSIS DATA IHECT
C«t Nirtw —— ,3.33?Lit M-l* 10 NPI fiPSIO ___________ «c towrt No.1-jU Mitrlni telld ______ ; ________ Centric* No.i left ~tit-fa-L. a—.Oiti ItolHM fcrtHwiMiiyi - tat« IMP I* MK«|VMI
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014326
VOLATILE LOW SOLIDQ ORGANICS ANALYSIS DATA SHEET • Pigc 3
Lib Hint; Hiid ComuChHnLib SiffiPlt I.P. Ho. Si OS \O QSS QOS
A. SURROGATE SPIKE RESULTS
COMPOUND
dB-Tolutne
d4-l,2-D1cni5rotthine
Bronofluorobtnzini
0
FRACTION
VOA
VOA
VOA
CONC(ug/kg-)
Sf.te
f.feell.O!
••
., ;•
(-urrojjitts only)501 ktAddid(ug/kg )
10
10
10
1Rnovcry
9ft6bM«
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o
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U14329SdMdul* Rit«rtne«_
COMPUCHEM NO. aftg.P DATE _____ 1 of 2IDENTIFIER VOLATILES ~ LOH LEVEL SOLID
QUANT.„..„... REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS VALUE H FACTOR • (uo/kfll UMlTdifl/kyl2. 221 CHtOROMETHANE3. 220 IROHOMETHANE4. m VINYL CHLORIDES. 209 CHLOROETHANEi. 222 METHYLENE CHLORIDE .......7. 252 ACETONE ..................B, 201 ACROLE1N .................9. 202 ACRYLONITRILE ............10. 230 TRICHLOROFLUOROMETHANE ...11. 254 CARBON DISULFIDE .........12. 216 1,1-DICHLOROETHYLENE .....13. 214 1,1-DlCHLOROETHANE .......14. 226 TRAHS-LZ-DICHLOMETHTLENE,15. 211 CHLOROFORM16. 215 1,2'DICHLOROETHANE .......17. 253 2-IUTANONEIB. 227 1,1,1-TRICHLOROETHANE ....19. 206 CARBON TETRACHLORIDE .....21. 257 VINYL ACETATE22. 212 BROMODICHLOROMETHANE .....23. 217 1,2-DICHLOROPROPANE ......24. 250 TRANS>1,3-DICHLOROPROPENE.25. 229 TRICHLOROETHYLENE26. 203 BENZENE27. 228 1,1,2-lRICHLOROETHANE ....28. 218 CIS-1,3, OICKLOROPROPENE..29. 208 DIBROHOCHLOROMETHANE .....30. ,..210 CHLOROETHYLVINYL ETHER....31. " 205 MOMOFORM32. 256 4-METHT1.2-PENTANONE .....34. 255 2-HEXANONE ............... ___ I ___ 5035. 223 1,1,2,2-TETRACHLOROETHANE. ___ ^ ___ 2.5
OPLEASE COMPLETE CORRECTION FACTOR CALCULATIONS ON SECOND SHEET OF IHE CQKROMND LIST!11
2.5,2.52.52.52.55050502.552.52.52.52.52.51002.52.552.52.52.52.52.52.552.52.52.550
COMPUCHEM NO. e3&S,D DATE _____ 2 of 2COMPOUND LIST NO. ____ ——————^ ———— IDENTIFIER VOLATILES •• LOH LEVEL SOLID
OUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS________ VALUE n FACTOR • (uo kg) LlMIT(ug/kg36. 224 TETRACHLOROETHENE37. 225 TOLUENE38. 207 CHLOROBENZENE39. 219 ETHYLKNZENE40. 251 STYRENE41. 239 0-XYLENE
QUANT.COMPOUND SURROGATE REPORT /WOUNT 1 * S RECOVERYNUMBER COMPOUNDS______ VALUE SPIKED RECOVERY HINDOH25B D4-1,2,DICKLOROETHANE (SURR) «MO 10.0 gV (50-160)*233 De-TOLUENE (SURR).......... q. 10.0 W (81-120)247 BROMOFLUOROBENZENE (SURR).. H.Ol 10.0 ilD (57-137)*
•Advisory Unitst f Rtcoviry • Quint. Report Vilue
/wount .pi itea
CORRECTION FACTOR CALCULATION: Instrument Code 23810 g _________
Her Ht. of 'simple used * Dilution Fictor " Dry Nilght Fictor »
10 g
O , 014331' JRT 11/B3
o
SJ*_t§If,
j«»$B
M
HI
8B \<r\ £r£ o>
1 t, XI
PROCEDURE! RK DIAGNOSTIC REPORT 2/13/04 14: 37: 29DATA FILE! GH0SW510A18REFERENCE: V23flO-THOO: VS3B ZNXTXALXXATXON OPTION: 2 PROCEBBING OPTION: 3'"REPORT: V23B81
< —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - UST NAMES - >PROC USED POB8 "MIS PROC USED POBB RUB STANDARD/UNKNOWN
3 3 1 0 44 6 1 49 VZ3B-1/V.3BU1
COMPOUND X ———————— SEARCH ———————— X BAT X ———— CHRO ————— >0 LIB ENTRY REF PRED BEL DELTA PEAKS PIT PEAKS M/E TOP DELTA PEAKS1 P9 1 -831 238 B32 i 9S1 130 231 -1 12 P* 1 -413 414 414 . 1 7883 P7 1 -493 494 494 . 1 9934 PS t -S3 93S pa 3 -i9 896 PS 4 -108 1087 PS S -132 132B PS 6 -173 1739 PS 7 -184 18410 PS 8 -184 184U PS 9 -19* 196IS n 10 -213 21313 PS 11 -204 20414 PS 12 -883 22S13 P3 13 -849 8493 P3 14 -843 8.3-7 PS 19 -272 273IB PS 1* -887 28619 PS 17 -886 88730 PS 18 -314 31331 PS 19 -322 323E2 P6 2 -323 32433 P6 3 -329 33034 P6 4 -3SB 39923 P6 S -362 36336 P6 6 -373 37437 P6 7 -366 38728 P6 8 -387 38829 P6 9 -387 38830 P6 10 -384 38331 P6 11 -409 41032 P6 12 -438 43933 P6 13 -450 4S134 P7 2 -481 48235 P7 3 -4B4 48336 J»7 4 -486 46737 P7 S -418 51938 P7 6 -548 94939 P7 7 -612 61440 P7 8 -793 7SS41 P7 9 -798 80038 PB 2 -883 886 885 -1 1 986•ii PB 3 -514 \S13 SIS 1 97844 P8 4 -697 699 699 . 1 986
79 414S3 4949094686484 17398 18956S31017696639683 272'6272 286971174312765751307897751876317358S8 48883 48316492 82011210610410663 883100 SIS
™ Ma01&33
QUANTITATION REPORT FILE: GH020310A1B
DATA: GH020510A1B, TX0/13/84 14:02:00'oAMPLE: 10 ML X8AMPLE 020510 + 5 UL 10990lil09B3 ON 018SUBMITTED BY: MB , ANALYST: 633
AMOUNT-AREA * REF. AMNT/JREF. AREA)* RESP. FACT)REBP. FAC. FROM LIBRARY ENTRY
NO NAME1 « BROMOCHUOROMETHANE (IB)S 221 CHLOROMETHANE9 880 BROMOMETHANE •? ' . '4 831 VINYL CHLORIDE9 809 CHLOROETHANE* 888 METHYLENE CHLORIDE7 838 ACETONE <2-PROPANONE) ;••».•.8 801 ACROLETN9 808 ACRYLONTmiLE10 830 TRICHLOROFLUOROMETHANE11 834 CARBON DIBUUFIDE12 216 1.1-OICHLOROETHYLENE13 814 L1-DICHLOROETHANE14 826 TRAN8-1,8-DXCHLOROETHYLENE19 811 CHLOROFORM16 819 JL, 2-DICHLOROETHANE17 893 8-BUTANONE18 227 1/1.1-TRICHUOROETHANE x>
806 CARBON TETRACHLORIDE« 2-BROMO-l-CHLOROPROPANE . .,
81 837 VINYL ACETATE '22 812 BROMODICHLOROMETHANE83 817 Ii 8-OICHLOROPROPANE84 830 TRANB-1.3-DXCHUOROPROPENE25 889 TRICHLOROETHYLENE86 203 BENZENE27 22B 1, i, 2-TRICHLOROETHANE28 218 CIS-1,3-DICHLOROPROPENE29 808 DIBROMOCHLOROMETHANE30 810 2-CHLOROETHYL VINYL ETHER31 203 BROMOFORM3£ 836 4-METHYL-2-PENTANONE .... .33 « DICHLOROBUTANE34 833 8-HEXANONE i ,.35 883 i, 1,8,8-TETRACHLOROETHANE ,36 824 TETRACHLOROETKENE37 823 TOLUENESB 807 CHLOROBENZENE39 .819 ETHYLBENZENE . T.."40 231 BTYRENE41 839 0-XYLENE48 #"' 04-1.2-DICHLOROETHANE43 tt DB-TOLUENE44 « BROMOFLUOROBENZENE
O M/E SCAN TIME. REF RRT METH AREA(HCHT) AMOUNT. REF RRT METH AREA(HCHT) AMOUNT XTOI *n*A
NO M/E SCAN TIME REF RRT METH AREA(HGHT) AMOUNT XTOT1 130 231 11:45 1 1.000 A BB 80271. 10.000 UG/KG 19,03
NOT FOUNDNOT FOUND
4 NOT FOUND5 NOT P6 84 /tjTg) 6:48 i 0.749 ABB 11691. ST460 UC/KC 2.7 98 M£3 9:24 1 0.801 A BB 988. 1.337 UG/KG 2, Ol'B NOT FOUND9 NOT FOUND10 NOT FOUND11 NOT FOUNDIS NOT FOUND13 NOT FOUND14 NOT FOUND15 83 ,872 13:90 1 i. 177 A BB 8993. 0.833 UG/KG 0.3316 NOT FOUND17 78 886 14:38 1 1.238 ABB 2839. 3.942 UG/KG S. 38IB NOT FOUND19 NOT FOUNCwJ I fMjLt20 79 4*4**2i: 03 28 1.000 A BB •OCgV-7 10.000 UG/KG 19.0321 NOT FOUND28 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUNDm NOT FOUNDO NOT FOUND30 NOT FOUND31 NOT FOUND38 NOT FOUNDagf KO&fi33 SS -UH 23:07 33 1.008 A BV TWtt! 10.000 UG/KG 19,0334 98 482 24:30 1 2.087 AftBV 3130. 0.443 UG/KG 0,6735 83 489 24:39 1 2.108 A BB 678. 0.051 UG/KG 0.0836 NOT FOUND37 92 920 26:26 1 2.231 A*BB 680. 0.093 UG/KG 0,0838 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND42 69 283 14:89 1 1.234 A BB 69011 B. 603 UC/KC 1ft 9343 100 919 26:11 1 2.229 A BB 140142, 9. B16 UG/KG 14.7944 176 698 39:29 13.022 A BB 811020. 11.013 UG/KG 16.93
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R. FAC R, FAC(L) RATIOi 11:48 100 1000 1,00 10.00 10,00 1000 1000 1.002 . 8:31 0.841 40.00 0.3763 4; 34;. 0.388 40.00 till4 3:89 0.466 40. H 1,707S 6:46 0.573 40,00 0.3476 8:91 0.99 0.790 1,00 1.46 40,00 0, 036 0.994 0.047 9:24 100 0.797 1,00 1.34 299.98 0, 000 0,055 0.00B 9:84 0.797 399,98 0,056
10:01 0.849 399.98 0.161 M,10:53 0.9E2 40,00 tTPt433>)
NO RET(L) RATIO RRT(L) RATIO AUNT AMNT(L) R, FAC R. FAC(L) RATIO11 1«:89 0.884 40,00 2,368
/—\2 11:29 0,974 40.00 0,825."-5 18:42 1076 40.00 0.33214 13:89 1,138 40.00 0.60915 13:53 100 1.177 100 0,84 40.00 0.009 1.586 0.0116 14:38 1:241 40.00 0.81717 14:33 1.00 1,837 1.00 3,54 899.98 0.001 0.100 0.01IB 16:04 1.368 40.00 106919 16:88 1.397 40,00 1.49380 81:06 1.00 1.000 1,00 10.00 10. H 1000 1.000 10081 16:88 1397 40,00 0.84882 16:46 1488 40.00 0.17083 18:18 1992 40.00 0.88384 18:30 19*9 .40.00 1,19285 19:04 1*16 ,44.00 , 133026 19:40 1668 ' 40.00 185487 19:43 1672 40.00 0.97888 19:46 1677 40,00 0.68889 19:34 1659 40.00 144830 20:94 1772 40.00 0.39631 88:19 1898 40. M . 1.46838 22:59 1948 60.00 , 0.28933 29:07 100 1000 1,00 10,00 10.00 1000 1000 10034 84:30 100 8.078 1.00 ' 0.44 60.00 0,006 0,880 0.0139 84:48 100 ft 099 100 0,03 40.88 0.008 1667 0.0036 24:48 ft 103 40.00 1.41837 26:86 100 ft 241 100 0.03 40. M 0.008 1437 0.00
27:57 ft 371 40.00 ft 91631:16 8.651 , . 40.00 104438:89 3.863 40. H 8,10140:46 3.437 40.00 1.86314:33 0.99 1837 1.00 B, 60 10. H 0.860 0.999 0.8626:14 100 8.824 1,00 9.88 10.00 1746 1.779 0.9833:32 100 3.013 1,00 11.01 10.00 ft 629 ft 387 1.10
O 014336
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ORBWICS NIALTSIS DATA MET•2-3.33-1|.*w«t«rf KtM! ff id C-" ^ CtitllM*ri_.
Jalld Oontrtrl No.iBit* talmt Mtwrlitd lyi __________ Ott» H*U UmlwdiAssociated u«p10i:JHSi3_____
__KmnuTikt ccmum .0»miw HIM uircit «wiBATI
MUCOff MOIITMl•••". •"»>..-.'•
MtlplT OMKtlon llnltt tr 1 Qtr II |
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SEMI-VOLATILE LOU SOLIDORGANIC* ANALYSIS DATA SHEET - Plgl 3
Lib MiMi Htld COBPUCtllff.
Lib Swplt I.D. Mo. flS/ST Q SS E OS 0ll.nk
A. SURROGATE SMtt KSULTS
COMPOUNDl-Flwrophinol
1,4,6-Trlbronophinol
D.M
DS-NUrobinnni
DU Mtrplwnyl
2-Fluoroblphinyl
FUCTIONSEHIVOA
SEHIVOA
snow**SEHIVOA
SEHIVOA
SEHIVOA
••
CONC (ue/kd
3qoo3360*33£83150
; Q3CO
1360
isurraiiusMdid (ug/kd
5000
5000
5000
5000 """'"
5000
5000
p
•
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76<_<,(,.
43'^
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014341
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19
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0:4343
' • COHPUCHEH MO. CfS DATE •• I of 3* 'COMPOUND UST NO. ___ ——— —————
——— IDENTIFIER StHl-VOLATlLES - LOM LEVEL SOLIDjL QUANTQ COMPOUND REPORT CORRECTION RESULTS DET. LIMIT
COUNTER NUMBER COHPOUNDS_____441 MITROSODIHETHYLAMINE610 PHENOL473 ANILINE411 IIS(2-CHLOROETHYL)ETHER601421 1,)41CKLOMKNZCNE422 1.44ICH.OR06ENZENE474 KRYL
10 420 1.2-DICHLOROKH2ENE11 62012 41213 62214 44215 4)616 44016 4)819 60620 603 2,421 41022 62523 60224 44625 43926 47527 43428 10829 477M 435II 11132 12624 41615 47926 42517 402N 428 2,6-DINITROTOLU-NEPLEASE COMPLETE CORRECTION FACTOR CALCULAT!
lISU-CHLOROISOPROPYDnNER
twruuritn NU. u-s imu ______ * m •>«ST NO. ——— IDENTIFIER SEMMOHTILES ^ LOH LEVEL SOLID
QUANT.REPORT CORRECTION RESULTS DET LIMIT(uu/kg) (ug/Kol
100.1050100102010101010020102010102010101010104010201010101020202020
„„..„„__ _ ——014$cileulntlons end wrrogitii en tack)
V ** f
COMPUCKEMNO. _____ DATE _____ 3 of 3y COMPOUND LIST NO. ___ ————— —————<> ———— IDENTIFIER SEH1-VOLAT1LE5 - LOU LEVEL SOLID
QUANT.QUANT. REPORT
COMPOUND SURROGATE REPORT MOUNT * tt ACCEPTABLE•UMBER COMPOUNDS VALUE SPIKED X RECOVERY RAUBE
119 2-FUIOROPHENOL *?7 //y" '" ' ""112 DB-PHENOL447 DS-NITROBENZEME Sf_____ _448 2-FUMROBIPICNYL H 3/ ^W»128 TRIRROMOPKENOL V*—— 125 f471 DIO-PTRENE bl 7_y 125496 DM-TIRPHENYL tl ** 1281
*^ (32-124)f8 -TZ? I HA )
Rtcovtry • Quint. Rtport Vilu*QtiininUpori NMiim >piufl * •>uu*
CORRECTION FACTOR CALCULATION:
Flnil txtrietlon voluM(iil) 50 iin ror MIO, o.wti for w * mt Miint Extricua 10 *^ D.< (*1) _ 60g
i.u mo o.s mi
OUANT. REPORT
250 altaunt MiTogiu woia mi j
250 ul
AMOUNT SPIKED CONVERSION FACTOR. ,H..
Flnil Extract Vol. M)* ui ror Kid, b.bni TOT M
DryWlutlon HHghtFactor * Factor n 40 •
x 40
Wlrtlcfn* Patter •
2> TBTl« i.o and.o.i' :r* (
'•For Advisory Purposts Only
ii/Bi 01434e|
'mi
MsctuMo-5 cnunais
fi
RESPOISE FACTOR CAtOWTIOM
0.30$
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0143<
005R-7J
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003R72
SlhT
•0 ••$8+is
f-flCEDURB! RK DIAGNOSTIC REPORT 8/08/84 B: 30:14UifA FILE: OJ019B37C19REFERRNCE: FBCC7
METHOD: FBCC7 INITIALIZATION OPTION: 8 PROCESSING OPTION: 3REPORT: FBCC7BI
< —— STANDARDS ——— >< •—— FLUB UNKNOWNS —— X - LIST NAdES - >PROC USED P08B Rttt PROC USED FOBS RUB STANDARD/UNKNOWN
6 4 I 41 94 61 41 FBCC7SI/FBCC7U16 6 1 41 34 U 1 98 FBCC7B8/F8CC7U2
C COMPOUND X ———————— BEARCH ——'————— X BAT X ———— CHRO ————— >NO LIB ENTRY REF PRED BEL DELTA PEAKS FIT PEAKS fl/E TOP DELTA PEAKS1 Cl8 C83 C34 C49 C96 C6
-8034
7 Cl 8 -368 366B Cl 3 -73V 737t Cl 4 -736 73410 Cl 9 -74B 74611 Cl 6 -791 74Vfl2 Cl 7 -778 770i Cl 8 -781 77914 Cl 9 -B09 B0719 Cl 10 -811 80916 Cl 11 -838 83017 Cl 18 -839 83318 Cl 13 -896 89419 Cl 14 -859 89780 Cl 19 -860 B9B81 Cl 16 -878 87688 02 8 -919 91783 C8 3 -931 98984 C8 4 -943 94189 C8 9 -960 99886 C8 6 -983 9B187 C8 7 -971 96988 C2 B -989 98389 C8 9 -994 99830 C8 10 -1012 101031 C8 11 -1087 108938 C8 18 -1097 109933» C8 13 -1114 111834 C8 14 -1194 119839 C8 19 -1170 116636 C8 16 -1176 117437 C3 8 -1198 119638 C3 3 -1887 1889
C3 4 -1266 1864C3 9 -1271 '.1269
41 C3 6 -1276 127448 C3 7 -1293 129143 C3 8 -1304 130844 C3 9 -1317 131949 C3 10 -1333 1331
9979BO996978799
-2329 2327 8387 . 1 898
130 777136 9891*4 1897IBS 1999840 8038 -1864 83277 4 . . .
TO ! ! !9 3 . . .1861 4 6 . . .146 . . .1 0 6 . . .1 4 6 . . .1 0 8 . , ,1 8 1 . . .1 0 8 . . .iao1 1 7 . . .1 8 3 . , ,8 2 . . .1 3 9 . . .1 8 8 . . .93 . . ,1 0 9 . .1681 8 0 . . .188 . .187 . . .8 8 9 . . .107 ." '" .119 ' . .837 .1 9 6 . . .1 9 6 . . ,1 6 8 . . .IS : 014350;us ; 0;0;5,R7'41 3 8 , . ,
109
47 C3 18 -1344 134848 C3 13 -1391 13B949 C3 14 -1396 139490 C3 19 -1393 139191 C3 16 -1408 1400
C3 17 -1419 1413C3 IB -1419 1417 , .
94 C3 19 -1424 148899 C4 8 -14BO 147896 C4 3 -1903 190197 C4 4 -1936 1934.96 C4 9 -1961 1999 , .99 C4 * -1968 196660 C4 7 -1678 167661 04 B -1778 177068 C9 8 -1B18 181063 C9 3 -180? 1B0764 C9 4 -1949 194369 C9 966 C9 6 -8031 8089 . . .67 C9 7 -2062 806068 C9 B -8039 803769 C9 9 -2192 819070 C6 8 -2897 889671 C6 3 -8897 889678 C6 4 -2336 833973 C6 9 -8799 879474 C* 6 -877B 877779 C6 7 -8877 287676 C7 8 -990 9B8 9B9 1 1 9977 7 C 7 3 -737 7 3 9 . . . .
C7 4 -879 873 B73 , 1 994C7 9 -1184 1182 1188 , 1 999
SO C7 6 -1439 1437 143B 1 ' 1 986B l C 7 7 -1809 1807 . . . .82 C7 8 -1846 1844 1849 1 1 996
I.*'
o
169•149804 . • .1 6 6 . . .138 .198 .1 6 9 . . .7 7 . . .8488 8 4 . . .8 6 6 . . .178 . . .1 7 8 . . .149 1676 . 1808808IM 1807 . 11 4 9 . . .8 9 8 . . .888 . . .14988B149 '.898 , . .8 9 8 . . .8 9 8 . . .8 7 6 . . .§78 , . .8 7 6 . . .118 98999 73988 873178 1188330 1437 -1818 1807844 1849
014351\
, t* OOr.R7j
/YNTITfVTION REPORT FILE: 6J019B37C19"w'DATA: OJ019837C19. TI08/08/64 7:86:00•AMPLE: 1UL 19837 + 9UL IS (10999)•UBM1TTED BY: 19 . ANALYST: 794
AMOUNT-AREA • REF. AMNT/ (REF. AREA)* REBF. FACT) ,REBP. FAC, FROM LIBRARY ENTRY "*"""'
NO NAME • ••'-• • ••••••••- •I «D4-1,4-DICHLOROBENZENE (IS)8 441 N-NITR080DIMETHYAM1NE3 610 PHENOL
473 ANILINE411 IIB(8-CHLOROETHYL)ETHER601 8-CHLOROPHENOL481 I, 3-DICHLOROBENZENE488 1.4-DICHLOROBENZENE474 BENZYL ALCOHOL
10 480 1.8-DICHLOROBENZENE11 680 8-WETHYLPHENOL •1 8 4 1 8 BI8(8-CHLDROISCPROPYL>ETKER • •13 688 4-WETHYLPHENOL14 448 N-NITROSO-DI-N-PROPYLAMINE19 436 HEXACHLOROETHANE6 440 NITROBENZENE --.•~ «460 DB-NAPHTHALENE (IS)IB 438 IBOPHRONE19 606 2-NITROPHENQU80 603 81 4-DIMETHYLPHENOL81 410 BIB(8-CHLOROETHOXY)METHANE88 689 BENZOIC ACID83 608 8,4-DICHLOROPHENDL24 446 1.8,4-TRICHLOROBENZENE89 439 NAPHTHALENE86 479 4-CHLOROANILINE87 434 HEXACHLOROBUTADIENE88 60S P-CHLORO-M-CRESOL89 477 8-HETHYLNAPHTHALENE30 439 HEXACHLOROCYCLOPENTADIENE31 611 8.4,6-TRICHLOROPHENOL38 686 2,4, 9-TRICHUWCPHENQL33 «D10-ACENAPHTHENE (IB)34 416 2-CHLORONAPHTHALENE39 479 3-NITROANILINE ,.,„.,..„ .,;...,36. 4a»'DIMETHYLPHTHALATE ' .... rt37. 408 ACENAPHTHYLENE •38 428 2, 6-DINITROTOLUET«39 476 2-NITROANILINE40 401 ACENAPHTHENE41 609 8, 4-DINITROPHENOL48 607 4-NITROPHENOL
MS 476 DIBENZOFURAMW4 427 2i4-»INITROTOLUENE nr..49 424 DIETHYLPHTHALATE 1 1! I . • .46 417 4-CHLOROPHENYL PKENYL ETHER
O>47 438 FLUORENE48 4BO 4-NITROANILINE49 604 4.6-DINITRO-O-CREBOL90 443 DIPHENYLAMINE (N-NITROSO)91 430 1,2-DIPHENYLHYDRAZINE (AZOBENZENE)92 »467 D10-FHENANTHRENE (IB)93 414 4-IROMPHENYL PHENYL ETHER „ .94 433 HEXACHLOROBENZENE ""99 409 PENTACHLOROPHENOL96 444 PHENANTHRENE "97 403 ANTHRACENE9B 486 DI-N-BUTYLFHTHALATE .*•99 431 FLUORANTHENE «,40 «499 D18-CHRY8ENE (IB)41 449 FYRENE48 404 BENZIDENE43 419 BUTYLBENZYLPHTNALATE44 483 3,a'-DICHLOROIENZIDINE49 409 BENZO(A)ANTHRACENEM 413 B18(8-ETHYLHEXYL>PHTHALATE47 418 CHRY8ENE48 489 DI-N-OCTYLPHTHALATE49 «D18-BENZO(A)FYRENE (IB)70 407 IENZD<8)FLUORANTHENE1 409 BENZO(K)FLUORANTHENE
406 BENZO(A)PYRENE437 INDENO(l,a«3-C.D>PYRENE
74 419 DIBENZO(Ai WANTHRACENE79 408 BENZO(0,HrI)PERYLENE76 619 8-FLUOROPHENOL (SURROGATE)77 D9-PHENOL (SURROGATE)70 447 D9-NITROBENZENE (SURROGATE)79 448 B-FLUOROBIPHENYL (BURROOATE)80 TRIBROMOPHENQL (SURROGATE)Bl D10-PYRENE (SURROGATE)88 D14-TERPHENYL (SURROGATE)
NO n/E SCAN TIME REF RRT METH AREA(HGHT) AMOUNT XTOT1 190 777 9:43 1 1.000 ABB 87008. 40.000 NO 9.07a NOT FOUND •3 NOT FOUND4 NOT FOUND9 NOT FOUND6 NOT FOUND7 NOT FOUNDB. NOT FOUND '9 NOT POUND10 NOT POUND11 NOT FOUND18 NOT FOUND13 NOT FOUNDJL4 NOT FOUND0 NOT FOUND16 NOT FOUND17 136 989 18:82 17 1.000 ABB 68819. 40.000 NO 9.07IB NOT FOUND
M/E SCAN TIME REF RRT METH AREA(HGHT) AMOUNT XTOT19 NOT FOUND80 NOT FOUND81 NOT FOUND22 NOT FOUND83 NOT FOUND84 NOT FOUND89 NOT POUND86 NOT FOUND87 NOT FOUND88 NOT POUND89 NOT FOUND30 NOT FOUND ft31 NOT FOUND38 NOT FOUND33 1*4 1897 16: 13 33 1. 000 A BB 33039. 40. 000 NO 9. 0734 NOT POUND39 NOT FOUND36 NOT FOUND37 NOT FOUND38 NOT FOUND39 NOT FOUND .„, . .,,... ,.:..,„ . . .:.40 NOT FOUND41 NOT FOUND48 NOT POUND43 NOT POUND
NOT FOUND ""»••NOT FOUND
46 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND90 NOT FOUND91 NOT FOUND98 1BB 1999 19:26 92 1.000 ABB 93979. 40. 000 NO 9.0793 NOT FOUND94 NOT FOUND99 NOT FOUND96 NOT FOUND97 NOT FOUND98 149 1676 80: 97 98 1, 078 A BB 407. 0. 877 NO • 0. 0499 NOT FOUND : *,• >. • • ' ' *40 840 8032 29:24 60 1.000 ABB ' 34692. 40. 000 NO 9.0761 NOT FOUND62 1B4 1807 iM:39 60 0, BB9 ABB 70S. 77. 996 NO • 9. 84 -//,63 NOT FOUND - '»'••< ~> • '64. NOT FOUND69 NOT FOUND46 NOT FOUND67 NOT FOUND68 NOT FOUND69 864 8387 89:09 69 1.000 ABB 87689. 40. 000 NO 9.07.;» NOT FOUND „. .--•m NOT FOUND , 01435472 NOT FOUND '73 NOT FOUND «, |l74 NOT FOUND ,
„.01nRT
79 NOT FOUND76 112 9B977 99 73978 82 87379 172 1162BO 330 143781 818 180782 844 1849
NO RET(L) RA1 :44 1.8 :363 :144 :189 :816 9:837 9:398 9:469 10:0710 10:0811 10:34-.."»'18 10: 8613 10: 4814 10:44 -JIB 10:"49" ' "$ft 10:9817 18:83 1.IB 11:8919 11:3880 11:4781 18: 0022 18: 1783 18: 0884 18: 1989 18: 8986 12:3987 18: 9088 13: 4389 13: 9930 14: 8931 14: 3738 14: 4833 16: 14 1.34 14: 9639 19:8036» 19:4937 19:9338 19:9739 16: 1040 16:1841 16: 8B.i"2 16: 40Ma 16: 3944 16: 4B49 17:8346 17:87
7:82 1 0.7969:11 17 0.74310: 99 17 0, 86314:46 17 1.19917:98 33 1,10688:39 60 0,88983:04 93 1.186
TIO RRT(L) RATIO00 1,000 1.00
0.4780.9490.9490.9600,964.0.9911,0031.0391,0411.0681.0731.0991. 103 ,1.1041.127
00 1.000 1.000.9870.9390.9920.9690.9980.9600.9941,0031,0811,0361,1071. 1841,1641.1811.187
00 1, 000 1. 000. 9880.9490.9790.9760.9880.9991,0041.0141.0861.0891,0391,0711.079
A BV 98364. 96.A BV 69994. B3.A BB 49983. 94.A BB 36760. 33.A BB 18698. 83.A BV ,.,,,,76769.-:-.. .41.A BB 96719. 97.
AUNT AMNT(L) R. FAC40.00 40.00 1.000
90. 0090.0090.0090.0090,0090.0090.0090,0090,0090.0090.0090.0090.0090.0090.00
40,00 •' 40.00 1.00090.0090.0090.0090.00890. 0090.0090,0090,00890. 0090.0090.0090.0090,0090.00390. 00
40, 00 4o! 00 1. 000' ,flfK«M •890.0090. 0090.0090.00890.00
• 90.00890.00189.0090.0090.0090.0090.00
970 NG376 NO319 NG984 NO984 NG986 NO081 NO
R.FAC(L)1.0000.6331.3121.1801.0870.794O.B640.9080.9640.7900.7960.8930.8600.1600.4390.4491.0000.9870.8230.3990,9760.0870.3040.3361.1320,8080.1B40.4990.3060.1380.8760,1761.0001.8030.4431.4140.7980.8930,0701,1180.1330.8091.4830, 4761.9690,908
18.3010.986.894.8610.997.867.83
RATIO1.00
:!•• •
(
1.00
* •'
1.00
...
014355
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RET(L) RATIO RRT(L) RATIO AUNT AMNT(L) R. FAC R.FAC(L) RATIO47 17:8948 17:3149 17:4190 17:4491 17:4698 19:88 1.00
078 90.00 1. 148079 290.00 0.049089 890.00 0.199092 90.00 0.398096 90.00 1.B71000 1.00 40.00 40.00 1.000 1.000 1.00
93 18:90 0.991 90.00 0,19894 18:47 0.969 90.00 0.84799 19:18 0.987 90.00 0.18196 19:31 1.003 90.00 1.19997 19:36 1.007 "90.00 0.94898 20:9B 1.00 1.078 1.00 0.88 30.00 0.009 1.489- 0.0199 83:09 1.136 / • ' 90.00 1.18940 89:89 1.00 1.000 1.00 40.00 40.00 1.000 1.000 1.0041 88:39 0.891 90.00 1.40048 88:37 1.00 0.889 1.00 77.60 90.00 0.016 0.010 1.9943 84:19 0.996 90.00 1.07744 86:09 1.004 90.00 0,036 '49 89:83 0.999 90.00 1.41446 89:46 1.014 90.00 1.44947 89:89 1.008 90.00 1.03048 87:84 1.076 90.00 8,67169 89:07 1,00 1.000 1.00 40,00 40.00 1.000 1,000 1.0070 8B:13 0.969 100.00 . 1.00071 88:13 0.969 100.00 ,1.000
89:12 1.003 90.00 0.93934:86 1.183 ' 90.00 0.394
74 34:43 1.193 90.00 0,40779 39:96 1.839 90.00 0,86376 7:8877 9:1378 10:9679 14:4680 17:9981 82:3782 33:04
00 0.79700 0.74400 0.86300 1. 19900 1. 10800 0.68900 1. 186
00 96,97 90.00 1.993 0.80000 83.38 90.00 0.846 0.90900 94,32 90.00 0.637 0.96600 33,96 90.00 0.473 0.70400 83.92 90.00 0.307 0. 16400 61,99 90,00 1.772 1,43000 97.02 90.00 0.841 0.737
. .,..!•*--vs.
94670967672414
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u.s. WVIMIWNTAI. PROTECTION AGENCT-CLP smpit Mmgmint otti»NO. lo« III, Mtxmdrll, VA 2291} • 7»/»MM90
CRMNICS ANALYSIS DMA SHEET
l*oritcr» Hwm _t»Lib SWIl IP N8.I >CltJ>l^ __________ « rtoport Na.i >3fe/
lend Oontrtet No.i ufe-eOitt IteltH* AgtliorlMd ly: ___________ OUt Swfil* RictlvfdiAssocUted simples :
______ KMinLATIlC Uwww. . „,• /«=». ' " ''"'"'""
CWttHTHATICN: POCOIIM HIIH (tlrct* MM)
DATE MMLQIDl«RdHT»ISW«i
-:*•
U.K. b. I ]")•• lB|"|«r|yj_ (IP(Clnek ten 1or
tn(clrcU em) (clrcli ent)
y, 1MJ
nSEMI-VOLATILE LCM SOLID
ORGAN]CS ANALYSIS DATA SHEET - Pige 3
Lib HIM: Htid CompuChtmLib Simpli 1,0. No.j£lj<MjL D SS D "S
A. SURROGATE SPIKE RESULTS
COMPOUND
2-Fluorophenol
2,4,6-Trlbromophinol
.;':.Whwol
DS-N1trobinstni
Oi4 P-Ttrphinyl
2-Fluoroblphcnyl
• ',>
FRACTIONSEHIVOA
SEM1VOA
SEMIVOA.,,
SEHIVOA
SEKIVOA
SEHIVOA
CONC (uo/kd
3a «sASto1 3,0
MO.,
•cSi)-o
ai^o
fc.
' !,'l-. \,;,r»X"
isurrogiMJ omyiSpiKi
Addtd (ug/kd
5000
5000
i-8000
:»:4000
5000'
5000
•
.»!f..
fttcovery
(o4
51. a.3S.4
3a.S43.X
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6
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, ' COMPUCHEM NO. _____ DATE _____ 1 of 3•'' COMPOUND LIST NO. __ ——— —"———— IDENTIFIER SEH1-VOLAT1LES - LOV LEVEL SOLIDWANT.
35 47996 42537 402 KENAPHTHYLtNE38 428 2J6.DINITMTOIU.NEPLEASE COMPLETE CORRECTION FACTOR CALCULATIONS ON THIRD KIT OF
„
40 401 ACENAPHTHENE41 COS 2,4-DINITRQPHENOL42 607 4-N1TROPHENOL43 476 DIKNZOFURAN .....44 427 2,4-DINITROTOLUENE45 424 OIETHTLPHTHALATE46 417 4-CHLOROPHENYL PHENYL ETHER.......47 432 FLUORENE
COMPOUND LIST NO. ~"———— ——————. • ———— IDENTIFIER SEMMOLATILE5 - UK LEVEL SOLID
QUANT.COMPOUND REPORT CORRECTION RESULTS DET LIMIT
s COUNTER NtlHBER COMPOUNDS_____ VALUE K FACTOR K • (UB/kg) ' "'
39 478 2-NITROAN1LINE ................... ____ I .o *l flD*- 100-10501001020101010
•100201020101020
' 101010101040102010101010202020202020
48 480 4-NITMMNlLINE49 604 4,6.DINITRO-0*CRCSOLSO 443 DIPHENYLAM1NE (N-NITROSO)51 430 1,2-DIPHENYLHYDRAZINE (AZOBENZENE)S3 414 4-BROMOPHENYL PHENYL ETHER54 433 KEXACHLOR08ENZENE .........
PENTACHLOROPKENOL56 444 PHENANTHREHE57 403 ANTHRACENE ..58 426 DI-N-BUTYLPHTHALATE59 431 FLUORANTHENE .............61 445 PYRENE ...................62 404 BENZIDINE ................63 415 BUTYLBENZYLPHTHALATE .....64 423 3,3'-DICHLOROBEr!ZIDINE ...65 405 BENZO(A)ANTHRACENE ......66 413 BIS(2-ETHYLKEXYL)PHTHALATE67 418 CHRYSENE .................68 429 OI-N-OCTYLPHTHALATE70 407 BENZO(B)FLUORANTHENE71 409 KNZO(K)FLUOMNTKENE72... 406 BENZO(A)PYRENE ........n 437 nDENO(l,2l3.C,D)PYRENE74 419 DIBENZO(A,H)ANTHRACENE75 408 KNZO(G,H,I)PERYLENE
uleulitlons indtsurrojitij on tack)014363
J ** 005RR7
COMPUCHEM NO. tyfit'l BATE ______ 3 of 3COMPOUND LIST NO. ____ * '"' ' '—————
'' ———— IDENTIFIER 5EMI-VOLATILE5 - LOH LEVEL SOLID
O QUANT.QUANT. REPORT
COMPOUND SURROGATE REPORT MOUNT Iff ACCEPTABLENUMBER COMPOUNDS VALUE SPIKED x RECOVERY RANEE
(26-116)(10-104)
619 2-FLUOROPHENOL TV 125112 BS-PHENOL S1 MS447 DS-NITROBENZCNE VI iw448 2-FLUOROBIPHENYL628 TRIBROMOPKENOL
125US
471 Dio-PtRENE 5~? 125416 OM-TERPHENYL . eq rts
(32-124)*( DA )(34.«6)«
Rieovtry • Omnt. Rtport Vilue M/N"i. mpon Mwuni sputa * '"Oi
CORRECTION FACTOR CALCULATION;Ory
Flnil txtnetlen voluBe(inl) 50 9 _______ Dilution NilghtMI ror AGIO, u.sni ror BN « Kit mignt Extriettd (g) * Fietor * Fietor * 40 •
1 ." <Bll 50i.i.u ina u.s ni IgT x _I x _f x 40 .
QUANT. REPORT AMOUNT SPIKED CONVERSION FACTOR!
250 ill_____ Flnil Entnet Vol. (nl) DllBtlqhMwunt surrofiu AOMO mil * un ror Mia, g.sm tor w * FKtor
250 ul_____mi, x 1.0 ind.o.Mi
•For Mvfiory Purposes Only
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PROCEDURE: RH DIAGNOSTIC REPORT 8/03/04 If:28! 09DATA FILE: OH019819B19REFERENCE: F8CC7
METHOD: FBCC7 INITIALIZATION OPTION: S PROCE8SIN9 OfTION: 3\REPORT: FBCC751O'
< —— STANDARDS ——— >< —— PLUS UNKNOWNS —— X - LIST NAMES - >PROC USED POBS RMB PROC USED PQBB RMB STANDARD/UNKNOWN
6 6 1 124 94 6 1 124 F8CC7B1/FBCC7UI6 6 1 124 34 11 1 188 FBCC788/FBCC7U8
< COMPOUND X ———————— SEARCH ———————— X BAT X • ——— CHRO - ———— ?NO LSI ENTRY REF PRED SO. DELTA PEAKS FIT PEAKS • M/E TOP DELTA PEAKSi er2 C83 ca4 C49 C9'6 CA
-813 810 810-1028 1089 1089-1341 1337 1337-1604 * 1600 1600-8089 8080 8088 8-8418 2413 8411 -1
996 . 190 BIO180 . 134 1029996 . 164 1337WO . 4M 1600048 . 840 8081 -1916 . 864 8411
7 C l 8 -399 3 9 7 . . . . . 7 4 . .8 Cl 3 -771 768 , . , , 949 Cl 4 -769 766 ... .'• 9310 Cl 9 -780 777 . . . 93U Cl 6 -786 783 . . . ~ . 128'» Cl 7 -807 804 . . ."" . '.'•"" 14613 Cl 8 -816 813 . . . . 1461 4 C l 9 -843 8 4 0 . . . . . 1 0 8 . .19 Cl 10 -846 .843 . . . . . 146 .
.Cl 11 -866 863 . .... ... aa-wws........-.;,,;;,.,*»Cl 12 -869 866 , . . • , . . 131
IB Cl 13 -890 887 . . . 10819 Cl 14 -892 BB9 . . 13020 Cl 19 -896 893 . . . . 11721 Cl 16 -914 911 ... -...• . 183 .28 C2 2 -994 991 . . . . 88 94883 C8 3 -966 969 , . . . 13924 C8 4 -979 976 . . . 1822 9 C 2 9 -999 9 9 2 . . . . . 9 3 . .2 6 C 2 6 -1019 1016 . . . . . 1 0 9 . .27 C2 7 -1009 1006 . . . . 1622 8 C 2 B -1022 1019 . . . . . 1 8 0 . .2 9 C 2 9 -1033 1029 . . . . . 1 2 8 . .30 C8 10-1092 1049 . . . . v ... 127; .31 C2 11-1064 1061 . . .. ,v. T 28938 02 12 -1139 1132 . . . 1073 3 C 2 1 3 -1193 1190 . . . . . 1 1 9 . .34 C2 14 -1193 1190 . . . . 83739 C8 19-1809 1806 . . . .,,„#.. ..,,,,. 19636 C8 • 16-1816 1813 . . . . ,• . IV* > *' .37 C3 2-1238 1839 . . •.•..:." •,vS:v-". 162 ..38 C3 3 -1269 1269 . . . . ," '"'; 13839 C3 4 -1309 1301 . . . "', . 1634 0 C 3 9 -1313 1309 . . . . . 1 9 2 . .41 C3 6 -1317 1313 . . . . . ' 16942 C3 7 -1339 1339 . , . . . 138 n< .,_.
C 3 B -1347 ,1343 . . . . . 1 9 4 014367C3 9-1361 '1397 . . . . . 184
4 9 C 3 1 0 -13BB 1384 . . . . . 1 0 946 C3 11 -1379 1371 . . . . • 168 .47 C3 IS -13B6 1382 . . , 169 .48 C3 13 -1431 1437 . , . , . 149 143849 C3 14 -143B 1434 . . !_...„..• !?04 _..
C3 16 -1477 1473C3 17 -1499 1499C3 IB -1462 149BC3 19 -1467 1463C4 2 -1929 1922C4 3 -1949 1946C4 4 -19B9 1982C4 9 -1608 1604C4 6 -1616 1612C4 7 -1722 1718C4 B -1823 1819C9 .2 -1863 1899C9 3 . .CS 4 -1992 19BBC9 9 . .C9 6 -2082 .4078C9 7 -2109 2101C9 8 -2090 2086C9 9 -2249 2240C6 2 -2329 2324C6 3 -2339 2330C6 4 -8426 2481C6 9 -2908 2896C6 6 -2921 2919C6 7 -3041 3039C7 2 -688 680 680C7 3 -769 767
yo9 909C7 9 -1883 1820 1220
996
991C7 4 -1484 1481 1483 2 1 992C7 7 -1860 1896C7 B -1894 1890 1891 1 1 991
1 3 8 . . .*1981 6 9 . . .778 4 8 . .8 8 4 . . .8 6 6 . . .1 7 8 . . .1 7 8 . . .149 1719 . 12 0 2 . . .2 0 2 . .184149 . ' .2 9 2 . . .2281 4 9 . .2 2 8 . . .1 4 9 . .3922 9 2 . .2 9 2 . . .2 7 6 . . .2 7 8 . . . .2 7 6 . . .112 62099 76882 909172 1220330 1482 -1212 1899244 1891
'*$".."'
W , 014368
1 QUANTITATIDN REPORT FILE: CH019819B19
DATA: OH019819B19, TI02/02/84 17:47.00AMPLE: 1UL 198i91/31/B4)ON«19»v: 19 ANALYST: 799AMOUNT-AREA * REF, AMNT/< REF. AREA) f REBP.FACT)RESP, FAC. FROM LIBRARY ENTRY
NO NAME1 *D4-1< 4-DICHLOROBENZENE (IB)2 441 N-NITMOBODIMETHYAMINE3 610 PHENOL4 473 ANILINE9 411 l-Btf-CHLCttOGTHYL, ETHER6 Ml 2-CHLOROPHENOL7 481.1,3-DICHLOROBENZENEB 422 1,4-DICHLOROBENZENEf 474 BENZYL ALCOHOL10 420 1,2-DICHLOROlENZENE11 420 2-METHYLPHENOL12 412 BIB(2-CHLOROIBOPROPYL)ETHER13 622 4-METHYLPHENQL14 442 N-NXTROBO-DI-N-PROPYLAMXNE19 436 HEXMHLOROETHANE14 440 NITROBENZENE .:•••17 «460 DB-NAPHTHALENE (IB)18 438 IBOPHRONE19 406 8-NITROPHENOL20 403 2. 4-DIMETHYLPHENOL
410 •IB(2-CHLOROETHOXY)METHANE429 BENZOIC ACID
23 402 2i 4-DXCHLOROPHENOL34 444 1,2.4-TRICHLOROBENZENE29 439 NAPHTHALENE24 479 4-CHLOROANXLINE27 434 HEXACHLOROBUTADIENE28 408 P-CHLORO-M-CRESOL29 477 2-METHYLNAPHTHALENE30 439 HEXACHLOROCYCLOPENTADIENE31 411 2i4i6-TRICHLOROPHENOL32 626 2,4, 9-TRICHLOROPHENOL33 «D10-ACENAPHTHENE (IB)34 416 2-CHLORONAPHTHALENE39 479 3-NITROANILINE36 429 D1METHYLPHTHALATE37 402 ACENAPHTHYLENE38 428 2.6-DINITRQTOLUENE •3f 478 a-MTROANILXNE " "40 401 ACENAPHTHENE ' • ' '41 409 2,4-DINITROPHENOL42 407 4-NITROPHENOL43 ~476 DIBENZQFURAN44 427 2, 4-DINITROTOLUENE49 424 DIETHYLPHTHALATE46 417 4-CHLOROPHENYL PHENYL ETHER
NO NAME47 432 FLUDRENE
480 4-NITROANILINE404 4,4-DINITRO-O-CRESQL
90 443 DIPHENYLAMINE (N-NXTROBO)91 430 1.2-DIPHENYLHYDRAZINE (AZOBENZENE)92 «447 D10-PHENANTHRENE (IB)93 414 4-BROMDPHENYL PHENYL ETHER94 433 HEXACHLOROBENZENE99 409 PENTACHLOROPHENOL94 444 PHENANTHRENE97 403 ANTHRACENE98 424 DX-N-BUTYLPHTHALATE99 431 FLUORANTHENE40 *499 D12-CHRYBENE (IB) ' •41 449 PYRENE43 404 BENZIDENE .... .43 419 BUTYLBENZYLPHTHALATE44 483 3.3'-DICHLOROBENZXDINE49 409 BENZO(A>ANTHRACENE44 413 BIB(8-ETHYLHEXYL)PHTHALATE47 418 CHRY8ENE68 429 DX-N-OCTYLPHTHALATE69 «D12-BENZO(A)PYRENE (IB)70 407 BENZO(B)FLUORANTHENE71 409 BENZO(K)FLUORANTHENE72 404 BENZO(A)PYRENE73 437 XNOENO(1.2i3-C.D>PYRENE'4 419 DXBfMZO(A,H>ANTHRACENE
400 BENZO<flrH,I>PERYLENE >>--.-'4 419 2-FLUOROPHENOL (SURROGATE)77 D9-PHENOL (BURROBATE)78 447 D9-NITROBENZENE (BURROOATE)79 448 2-FLUOROBXPHENYL (BURROOATE)80 TRIBROMOPHENOL (SURROGATE)81 D10-PYRENE (BURROOATE)82 D14-TERPHENYL (SURRDOATE)
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 190 BID 10:07 1 1.000 A BV 97649. 40.000 NO 6.292 NOT FOUND3 NOT FOUND4 NOT FOUND9 NOT FOUND6 NOT FOUND7 NOT FOUNDB NOT FOUND9 NOT FOUND ,.••.. •10 NOT FOUND „. :11 MOT FOUND ..12 NOT FOUND •13 NOT FOUND ' „., ,14 NOT FOUND19 NOT FOUND16 NOT FOUND
136 1029 12:49 17 1.000 A BV 120949. 40.000 NO 6.29B2 948 11:91 17 0.929 A»W 1799. 0,708 NO 0.11
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT19 NOT FOUND20 NOT FOUND
NOT FOUNDNOT FOUND
23 NOT FOUND24 NOT FOUND29 NOT FOUND i24 NOT FOUND27 NOT FOUND28 NOT FOUND39 NOT FOUND ''' •30 NOT FOUND •3 1 N O T FOUND . . .32 NOT FOUND • "ffm*.. '• •••#••33 144 1337 14:43 33 1.000 A BV 49982. 40. 000 NO 4.2934 NOT FOUND •'-39 NOT' FOUND - . . - . . ' -.%•„,;34 NOT FOUND .•"•••"" " '37 NOT FOUND38 NOT FOUND39 NOT FOUND40 NOT FOUND41 NOT FOUND42 NOT FOUND43 NOT FOUND -44 NOT FOUND49 149 1428 17: 91 33 1. 048 A BB 1921. 0. 939 NO 0. OB44 NOT FOUND-17 NOT FOUNDMB NOT FOUND "•'49 NOT FOUND90. NOT FOUND91 NOT FOUND92 IBS 1600 20:00 98 1.000 A BV 116916. 40. 000 NO 6.2993 NOT FOUND94 NOT FOUND99 NOT FOUND96 NOT FOUND97 NOT FOUND98 149 1719 21:29 92 1.074 ABB 466. 0. 100 NO 0.0299 NOT FOUND60 240 20B1 26: 01 60 1. 000 A BV 88874. 40. 000 NC 6. 2961 NOT FOUND42 NOT FOUND63 NOT FOUND64 NOT FOUND69 NOT FOUND66 NOT FOUND67 NOT FOUND "" '48 NOT FOUND " * .-.49 244 2411 30:08 49 1.000 A BV 43B02. 40. 000 NB •' 4.2970 HOT FOUND71 NOT FOUND72 NOT FOUND • «_ .«««73 NOT FOUND 014371
NOT FOUND
»»
79 NOT FOUND112 620 7:49 1 0.769 A BV 68773. 80.386 NO 12.9799 76B 9:36 17 0.749 A BV 96037. 47. B71 NO 7.48
78 82 909 11:23 17 0.887 A UV 61494. 40.769 NO 6.3779 172 1220 19:19 17 1.190 A BV 109904. 93.912 N0 8.4380 330 1482 18:31 33 1. 108 A BV 18726. . 43.998 NO 10.00Bl 212 1899 23:11 60 0.891 A BV 169219. 97.269 NO 8.9982 244 1891 23:38 93 1.182 AW 118319. 94.327 NO 8.49
«2
1 10:10 1. 00 1.000 1. 00 40. 00 v '40; OOT**t; 000 1, 0002 4:99 0.491 90.00 0.9023 9:38 0.948 90,00 1.0334 9:37 0,946 90.00 0,7019 9:49 0.999 .90.00 1.0946 •9:4»,;._ . ,.0.9*7 ,a;;;,':|0.'00"'•'•'.•;.' ' 0.7647 10:08. 0.993 90.00 0.843B 10:12 1.004 90,00 0.9289 10:33 1.037 90.00 0.39410 10:34 1.041 90.00 0.04111 10:4912 10:9813 11:0714 11:0919 11:1216 11:2917 13:91 1.00
069 90.00 0.714069 90.00 0.3B3099 90.00 0.769097 90.00 0. 162102 90.00 0.401124 90,00 0,413000 1.00 40.00 40.00 1.000 1.000 1.00
11:99 0.99 0.928 1.00 0.71 90,00 0.012 0.040 0.0113:06 0,948 90.00 0.30613:14 0.992 • ,90.00 0.329
21 13:36 0.968 90.00 0,49932 12:44 0.991 290.00 0.14833 13:37 0.982 90.00 0.28924 13:46 0.994 90.00 0.33439 13:94 .004 90.00 1. 10826 13:09 .023 290.00 0,20627 13: IB . 039 90,00 0, 1B12B 14:11 .104 90,00 0.41829 14:29 . 122 90.00 0.34630 14:99 . 161 90,00 0,09931 19:07 . 176 90.00 0.31332 19:12 ,183 290.00 0.16633 16:46 1.00 1.000 1.00 40.00 40.00 1.000 1.00034 19:28 0.923 90,00 1.16039 19:92 0.946 290.00 0.37736 16:19 0.973 90.00 1.39137 16:39 0.979 90,00 1.27138 16:28 0.982 .,,:'; 90.0ft 0,39339 16:44, ,0,999 - .290,,00'v;-,'",".'' 0,08940 14:90 '.".'#.'004 ... 90,00'Vv.T 1.10041 17:01 1.019 .,,.;.' 390.00 0.04442 17:3143 17:1144 17:19
17:93 1.0017:98
, 039 129,00 0.049029 90.00 1.693034 90,00 0.449067 1.00 0,93 90.00 0.017 1,6340,72 90.00 0,47B
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L) R.FAC R.FAC(L> RATIO47 17:9848 18:28
18:14•iiO 18:1491 18:2092 20:03 1.00
072 90.00 1.242101 290.00 0.013088 290.00 0.129090 90.00 0.934094 90.00 1.939000 1.00 40.00 40.00 1.000 1.000 1.00
93 19:04 0.991 90.00 0.18494 19:22 0.966 90.00 0.22999 19:49 0.98B 90.00 0, 10996 20:06 1.002 90.00 .... 1.10297 20:13 ..•-"'•'i; 007 ' •"*'**' •••jttSWi'OO"..5 '•<-•»••••• 0.990 "•' '98 21:31 1.00 1.074 1.00 0.10 90.00 0.003 1.601 0.0099 23:47 1.137 u#tBO, 00 ..-, 1.10040 24:04 1.00 1.000 1.00 40.00 -40.00 1.000 1.000 1.0041 33:17 0.894 90.00 1.97043 28:41 0.899' .90.00 0.01043 84:94 0;999' :.*?::. ' *0;0<f.,-,;.'., .. 0.94444 24:34 1.001 ' 90.00 0.03949 24:01 0.999 90.00
010 90.00002 90.00077 90.00 2.399000 1.00 40.00 40.00 1.000
339327187
66 26:1967 24:0748 28:0449 30:13 1.0070 29:0771 29:1172 30:1973 34:1474 34:31
38:01 1.298 90,00 "".' 0.289
963 90.00966 90.00 0,921003 90.00 0.989200 90.00 . 0.488208.. 90.00 "'.MBfew..'.' 0.376
000 1,00174
7:4477 9:3778 11:2379 19:1780 18:33
00 0.76900 0.74800 0.88600 i. 19000 1.107
81 23:19 1.00 0.89282 23:40 1.00 1.181
00 BO, 39- 90.00 0.994 0.994, 1.6100 47.87 90.00 0.371 0.387 i 0.9600 40.76 90.00 0.406 0.499 0.8200 93.91 90.00 0.724 0.672 1. OB00 63.96 .90.00 . ..0.219 0. 168 1.2800 97.27 90.00 1.649 1,437 1.1900 94.33 90.00 0. B12 0.747 1.09
^ ,r.Mr 014373^ ^
014374
U.i. CNVIROH.NTAL PROTECTION AOCNCY * CU> Si~l« Minigvntnt OfllctP.O. to III, Almifltfrli, Vlrglnli 23313 - 703/557-MW
OR8ANICS ANN.YIII DATA MEET
Ittgritory MIMILib lMpl* ID HoIwpli NUrlm _lollil
IAH-E NUMBER
tOUTILES
«I«NTRATION| UM MEDIUM HI8M (elrell. COHCEHTMTIOHt C5<OtUM HI9H Iclrcll OM)DATE «THACTB/H*PA-»| ____________ OATI DCfflACTID/fMPWOlDAn«NALTZIDl ____________________ OATIWAlTBDlKWWI »iitu«iAssoditid iimpUs___________ Assoclittd iimpl8S_j2SSfi»-HultlHr Dtt«etlon limn by I OOT Q ____ Hiltlply Dtttetloci Ililti by \ 'fi.jr
(CM* ta for Afproprliti fietv) ICOtck tai for Mw rl"* rietor)•I/I
cr «|A|(elrelt ON)•In
C] PESTICIDE LOH SOLIDORGAN1CS ANALYSIS DATA SHEET • Pigi 3
ESS QDS gjnink
. SURR06ME SMtf KSULTS
COKPOUNP'PESTICIDB -|,5 I K
COHPUCHEH MO.10EHT1FIER PtSTlClDES (LOV .OTL.SOL10)
1 COHPOUH) LIST - NO. ___CMfUCHEMCOMPOUND
COUHTER H1IHBER COHPOUHO NAPE RESULT DETECTION LIH1T (tn/fca)1. 0701 ALDRIN ••••-•••••••••«•••• 4.0I. 070Z ALPHA-IHC ~———........ \ 4*0I. 0703 KTA4HC •——————— . \ 4.0 '4. 0704 fim-BHC-~.«.~.-~ | 4.0S. 0705 CELTA-BHC ~.............. 4.0I. 0706 caORONK ~~»~-~~~- .'"•:•: ,.. ,4.07. 0707 4,4'.WT ———-——— 4.0I. 0708 4,4'-ME———————— 4.0I. 0709 4,4'-HDD —•———i— 4.010. 0710 D1ELMIN————-——— 4.0U. 0711 . ALPHA-EJIDOSU.FAN •—•—. 4.012. 0712 KTA-CNDOSULFMI——— " 4.0U. 0713 ENOOSULFM SULFATE ——- fa 4.014. 0714 " "• MWN ———i——^iJ»*" fJfA 4.0IS. 0715 BMW ALDEHYDE———— V 4.0It. 0716 HEPTACHLOR ~-...-....~. 4.017. 0717 HEPTACHLOR EPOUDE —18. 0716 PCB.1242 <————-—19. 0719 PCM254 —.........20. 0720 PC8.1221 —————21. 0721 PC8-1232.————•
4.04.04.04.04.0
22. 0722 PC8.1248—— • ————— ! 4.0H. 0723 PCW2W ———————— 4.0M. 0724 KM01I. ———————— M25. 0725 TOXMHENE ———— « —— 4.0
'••''": OUAKT.CWfOUW NMOBATE , I RECOVCRf REPORT COMECTIOM ,..x• IMKR cotouiBS nrnat TALUE FACTOR IIESULT0738 OIIUTYL CHUKWATE (41-121)* ___, ''"___ L. JJH 3&
-'7 4378ts
AMPLITUDE x.2S uV-xtcond* (EnUrgud x 16*19)
014379
Report i 1964.00 Channel i 0 BLANKO«npX«i PP 19819R T.nj*rt«n1 *t l<M4i2!? ON FF.B 15, 19H4E8TD Mtthod. EP«0 8i-q. 8F.Q03 8ub«q/8<inpi 1/33 Bt) • 7381-wirtth HV/Min Dolay Hin-Ar Bunch
,250 .300 3.00 )0fl
Actual pun tlti-i 35.217 niniitu* '-i"«M"»
RT ITM Factor APM ,,', UG/rU.
142949. 8V 14294B.620
.17,1917,81 .iOOOOF+OIIB. 32 .lOOOOF+flt
, , .5.54 20,35 .lOOOOE+O)5.8? 5>1.3B . 10000F+DI!;9i74 ft:tt -. miffitU6.27 23. OS ' .lOOOOF+Oi6.AR 84,51 .100nOE+Blh.7R 24. P9 .lOnOOFtfll7.10 26.0? .lOOOOF^Ol7,?? 26.52 ,10fl(inF+n)
*•'* »•;« iisiiB.8B 32,58 .10000F.+019,0? 33,35 ,lOnOOF.+01.9 26 33 98 lOOflflF^O)9.62 35.30 ,10000E>019.79 35,93 .IOOOOF+01
10.65 39,10 .lOOOPP.+m.«:?l 4i,tB2 :i°o°oflo»i11.34 41.62 .10000F+0111,12 3,30 .IQBOOR+O!
i24 59.63 .10000
toi M. „ .....,„ AIJ)..M
Kit IBKKBO.42, 10000F.+01 , ,82.54 47403e-n«i 24941,88 ,118 PP'DDT «4.AA«C14JJO
.lOOOOF.+Ol BBO; BB §80.250 '......... ..«. «~ 14R0.813 ,I060,68fl ;,, *»
Total AP»« • 411146, Total UR/HL • 1060.688data filfi P0333 R«H d«t« fllei R0333
014381
»*
o
014382
Repopt. 5333.00 Channel c 1 BLANKOanpliH CP 19819R Tnjwtml at 8.09.59 ON PER 14, 1984E8TRMfthod.PAr.K01 8-q. 8EQ12 Subnq/Sanp. 1/44 Bt) . 44Bl-Hirlth NV/Hih r>»lay Hln-Ar Bunch
,500 .300 Q.Oft 1000 Auto
Actual pun ti«»> 85.008 nlnutts, F.nrJtd not
RT ITH Factop Ap-a w" ^ AREA X Nan*
.30 0. fl , lOnOOF+01, 3632690. B83632690.SOO,42 «.I 0 .lOOOOE+Ql 3875443. BB3875443.500
.10000F+01, 116623, BB, 116623.500•«.»»£•»•«» .36277, BB 3.6?76,ft2S
,1,1IO(IOE+01
OnOF.+Ol 4768. BB 4768,663IOOE+01 3361. BB 3361,313Kl M:,&M$.l"",10000F*Ot '3091.BB 3091,375
.lOOOOF+fll 602082, BB 60|082,500
O.dO '.lOOOOF+01 1872. BB 1871'.750Total Ap«a • 21552068. Total AREA X - 1871.750Ppoc-«flfCl data fHe. P1244 Raw data file. R1244
014383
U.S. IrttlMMCNTAL PROTECTION MENCY - CU> Swpl* KiMJwwit Oltle*P.O. to ai«, Al-imfrlt, Vlrglnli J75I5 - 70S/M7.MW
(MGWIC5 ANALYSIS DATA SHEET.2 77 TLtboritory H«»l Ca*>vtom_____________ Cut Nwoir *--?. _3
L«h i»l« IB Hoi lCl'fe3T PC Moat Mo. \3lol .e.Implt Mttrlw Celld ____ ' ftmtrnt No.i toe -01 • blfa*-»Otti talim AntlMrlnd B»i _____________ Oiti Iwpli taMlxai ________
VM.ATIUS
GaWENTIIATIONl \SM «OIUM HIOH IctlxU) OOHdHTRATIONi (g) KDIUM HJ* (clrclf pnt)DATE OniACIID/PTWrWEOj ______________ DATt KmACIW/WWAKOlDATE ANALRIOl ____________________ OATl MMLYKDl _____PBWHT WltTUKl -__________ - , mCOff »IITI«| __Associated samples_____\___________ Associated samples.Multiply DttKtlon Unit* by I Qor P ______ Kiltlply Dtttctlon llnlti by I,
(CMck tai for Approorlit* Foctor) (Bwcti ton for AMraprlit* r'l•g/l HI/IWl CAW or yg/Vg m CAM or yg/Kg
(elrelo ont) (clrelo oni)•crel.ln
OIOXINi ,
' OONONTMTIWl UM KOIIW HI9H (clrcl*)
PIMHT MltTUfciAisoclitid unplts: •;____ yB/.ff«i. ..M .. _«___p_^_^__ .irryor Kg/kg——•—————————————T lelroloont)J,J,7,l-lrtrKhl(irBdlti*nie-IIM) I7IMM P-tflOTlr, Q.I6U
July, 1965
014384
PESTICIDE LOW SOLIDORGANIC! ANALYSIS PATA SHEET • Page 3
OLab Him s_ Head CompuCheir.Lab Sample 1.0. No.)QS37 _] SS p OS
A. SURROGATE SPIKE RESULTS
COMPOUND '
DlbutjfcMoroendite •
,
- |.....
i 1;.
FRACTION
PESTICIDE
CON: (ua/kt3.1ST"
• ^ • • • •
(Sjrro;itti orl>)Spike
Added (us'U
25
»., ,
.... •»
• •• > -,,
Rt:overy
V
01438500.,7<. 0 6\v *•
•WMPUCHEM NO.______ DATEIDENTIFIER PESTICIDES (LOH LEVEL-SOLID)
.O COMPOUND LIST - NO. ___COMPUCHEMCOMPOUND
COUNTER NUMBER COMPOUND NAME RESULT DETECTION LIMIT (ug/kg)nLORIN •••••«-•»*••->•"•-»
0702 ALPHA-BHC —————0703 BETA'BHC -———-•—0704 GAfflA-BHC ——————•0705 DELTA-BHC ~~-————
4.04.0
C. 0706 CHLORDAKE —-7. 0707 4,4'-DDT ——••——— .06. 0708 4,4'4DE —9. 0709 4,4'-ODD —•10. 0710 DIELDRIN —•11. 0711 ALPHA-ENDOSUFAN —— —12. 0712 BETA-ENDOSULFAN ——— — -13. 0713 ENDOSULFAN SULFATE — —14. 0714""" ENDRIN ————— •• ———15. 0715 ENDRIN ALDEHYDE -»-- ——16. 0716 HEPTACHLOR ——.-.—-.17. 0717 HEPTACHLOR EPOXIDE ———18. 0718 PCB-1242 —..-.-.. ———19. 0719 PCB-1254 ——-———.20. 0720 PCB-122I —..--—-.-—21. 0721 PCB'1232 ~.-..--~.~.—22. 0722 PCB-1246 —-———•—23. 0723 PCB-1260 — —————— .024. 0724 PCB'1016 —-.-.--.--.—25. 0725 TOXAPHENE ~...—.—..— »
- • IHIWT.., ''"•"COMPOUND SURROGATE I RECOVERY UPOUT COMECT10N --'«»T- AMOUHT %TlUMBER COMPOUNDS OTNDOM VALUE FACTOR RESULT SPIKED RECOVERY
.»0738 OIBUTYL CHLOREHDATE (41-121)* ___ ___ j££ /Otff £~
uonpuGhtn Nunher- 1VB31/' UAai.* -4HO tvt\* H
J VoluriB or weight extracted" ,i)b hi Ugr-.isFinali tKtract Volune- SSplit'. 4
• Dilution Kactor» 1Dry Witight Mctor= i
The Calculation Equation in,... ' ' '
Sinpl* Art*St.nd«rd Are* * btd Cone * Dilution * Split I \-inm ViO~"™ •""*~|*|'»"'~» Hr-mmi «.«»««.• UMIH.* ,, H.«r««nH«M>*«HH«>-i-i-ii--<Hi-i. i •••--••••
Volune or Weight / Dry Wiight K-ctor
D«t« (-or Compound KNUOSUl.t'ANS«nple Area • /.UUStandard Arta • 1*00Standard ConevntrAtion « ,(iyConcentration of tNDO.UUAN _ULHATHI;AP) is t.yoyuv ug/kg
Data For Co-pound -NBOSULI'AN SULPATE(l'ACK)Sample AfM « b.VStandard Arta • 14Standard Concentration « .(MConcentration O'C KNUUSUkKAN SULFAlt.O'MIC.)-., ^ 6.74.H6 ug/kq
f!OF.7|;P)
\> <14388
RMPLITUDE x.26 uV-«»cont.x CEnUrg*cl 'if 14.41)* 0) l» <"
2.2
oatIXW"•
i ?
513
"0 £
014389
Report i 6577.00 Channel i 5PP 19837 Injected at 33. .03 ON FfIB fl, J9B4
""E8TD Method i EPAB 8*q. 8F.RS6 8uh«in/8<inp . tAfl BH . 10
p"nrh
Actual run tine. ,30.006 ninuteng(s> ni«*ffdlot on ban«>lini>Reading (B) ni««ftdRndnd no
XT XTH Factor Arm AREA % N«n<>
5.34 19. B. .lOOnnF+flt 6A4736. 8B ,5. 50 20.43 .10000I-.+01 807717. 8H 207717.8505.61 ?O.BS ,100001-tOl 194093, BH 194091,9705.7621.3B ,100nOF+01 S4687J . 8H 546871 .SO 05.91 21.94 .lOOOOE+m. 4V6176, RH 496175,810
RKTA(5913. 8V *6Wt3.*QO
iaiSlS' fili i51_§3''r*fl.._... ..... ;i0660E+6i 344211.' 8V 344211 !L.12.66 47.02 .27143E-07 104835, BV .003 ALORIN
I !!:27» ft-.D :UWI£U IB91; «$ imil:t» PP'DDT26,5298.49 .1QOOOF.+QJ 4B422?! 8V 4B4225.SOO26,92100.00 .110961--05 155753. RV .173 *)>BC
Total Arffl • 1337340B. Total ARFA X « J55758.940Prnress»rt data film P5610 Ran data film RS610
rWUTU.E x.2S uV-ftconds (£nUrq«d x 26.00)
SI
00)
5 MQ »
roz)l1.3!7
0.M
•TO2.1t>- r-n ..... 2.52
J 3: - ••'•*..> *-63\- V.!.':, '• ..."- S> 5.51£.1 »44
IS. 63
18.92
-1.P.2
'" "«3R! «|««-.;
°l*39t
\ »*V, nosTtg
/•"•s. Neport. 32VH.OO Channel.. S
SAMple. UV IVUW Injected at ;i.4(li3«;! UN IT« 14, 1VII4
6I3TD Method. PACKOi.' lien,. -t;t)2;< Uubvq/Uanp. 1X16 Rtl. 16
Ul'width MV/hln Delay Man-fV tinnrh.QUO .JOl) 0,00 ao Auto
Sup-Unit Dv'T ID-U1 HefK'IW XKTW itbiJ't Ifi.nNO 0.1)0 I) .-0 -.0 100,1)0 NU
Actuai run tine. ,017 Minutes
«l (I'h Me tor Art* UU/rtL
IIH.4!> S.ll) ,lUUI)Ui£l01 »4 44'/, SB 1M.4447,410.64 3,02 , lOllOdK.iUl it'/641, W 16V641.iyil.76 J.57 ,10110lit:'Ilit 14'/M. SO i4763.yi6.U'/ 4,09 .lHOUdLMIll l(li!£!6, til! lUiJ!:ii.7S(l
1.1V S.SO pi ,10BOOE*Ol u'/Uia. SB 78112.000i.;<o 6,12 .iouooti-ioi 6vi. SB tvo.vs;-;i.'jll 7,00 ,WJ'j'je-OS yUV/'J. 90 ,096 ALPHA Dili:£.)„ 10,11 .lOOOOK'lO) UV4V. iiH IIVUl.'J622,'JU 11.07 ,1000HIMOt 1.VD6. 8B 1)3706.»6£.'2,'/U K'.'.V4 .JOOOOlMUl • a/_. 2H A.06?,•4.4'i 16, U7 .IDUDOIil'MIl ' 410..JU 409,'/Ob3.6V I1/.3V .KIOOOE'llll 2V_. '8l«" SV .ai;'.4,6.i 1M.U4 ,10l)00n>l)l ia/;(. 36 1274, IIllfl6.!;t aii.vb .i07(.w-(i!,: tc/a!<. sb .onv6.4<) 30.36 ,101)1)III;till Hl'JV. -tt6,11(1 /.K.u;'1 JOOOOPKil 210V, SBn,,j'> w,.o ..ooooKMii ivy., sn 1754,uoo
11... 63 Vit.64 ,17bOLJl>OV; liUU1/. f!W .010 K'NlllllillU AN liLII I A'llIH.Vi.' »'/,16 ,10llOlli:M)l L"j6,i. SU 2S6,(,00021,i'.1100.00 .J7110K-06 6M»B. 8B • ' '.OOJ *ll»ll;
•
I'ntfll Area * 6a444V, • Total IJB/hl. « 6552:>!4ft
data file. P23H. rJaw data
00-71
014393
U.S. DNIMNCKTM. PIWTICTIW MCNCY - OP S«*l* Mtntpmt Oltlc*P.O. IOM lit, Alonoriflrli, Vlrglnlt 22313 * 705/557-24M
IAM.EMMER
ORMNICS MALYSIS DATA SHEET
CM Hu*r g______Lri> *•*>!• ID Not tl'ttSI 3"_______ QC Rtport Ho. J^fc/-a.e.< RtiiIwpli Mttrlm ,to'i_ _____ .. Coirtroet Ho.i faQ'-to \, —1Drti itoltMt AutWIitd Ifi ____________ Ditt Ii ilt R*ctl«Mi
VOLATILE5 KSTICIKS
eOWENTMTICNl ( KOIUM HI OH lelreU) OONCENTIIATIONl W> (CDIUM HIM (circle oiw)DATE em«TO/r-pAiW! __________ DATE Exrf»cTED/f«p/«Di .________BATE NMinOl _____________________ BATE ANAimDl __________________PDICENr WltTMEl __________________ PEWOff MOISTURE! __Associated simples____________ Associated samplesMultiply Btttetlon Unlit bf I er__^_ Hiltlply Dttoetlor. ll.lti ky 1 ^ ———
(ClwckloKfor Afproprlitirietar) (CMcK Ion lor Aftrofrltt* Foctor)«B/I MJ/I
f CAW or ug/kg ffl CAW or ugAgCelreU oot) (clrclo on«)CMHI '"
CONCEHTHATIONl (L > HDIUM. HIBH Iclrelt)DATE EirmACTEO/PiSPMEDlDAHKMCNTHDIV __Associated samples:.
———7-——— fcirSrrwt)2,5,7,Mttr«cMcrMlb«fiicr
HMB» IT4fr<l-t B-dla»ln _______C.I6U
July, 1«8!
014394
51?
«? C
-\
•
K
00
EDURE'. RK DIAGNOSTIC REPORT B/2-/B4 U-.34-.08)TA FILE; TJf>19B37A03REFERENCE'. TC
METHOD'. TC INITIALIZATION OPTION'. 2 PROCESSING OPTION: 3REPORT-. TC8
< —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - LIST NAMES - >PROC USED POBS RT1S PROC USED POSS RMB 8TANDARD/UNKNO>»M
2 2 4 19 7 B i B? TCB/TCU
7 COMPOUNDS PROCESSED, B FOUND
vvnnNO LIBa TC2 TC3 TC4 TC5 TC6 TC7 TC
mm* fENTRY
1234S67
REP-6SS-633-633-633-652-652-63S
PRED661642642642661661661
— BBIBEL661642642642
(.
661
wwi —— —— —DELTA PEAKS
2211
( t
, t
1
— — ."; BWI f\ — —PIT PEAKS M/EB31 332996996996
f
(
921
329322297326322257
-— vrww •' — • •• — .TOP DELTA PEAKS660 -11642 1642642662656
,
1122,
014397
MEAD COMPUCHEM<*>MNTITATION REPORT FILE'. TJ019B37A05
DATA'. TJ019B37A05, TI02/29/04 11:08:00SAMPLE: 2UL OF TCDD SAMPLE 19637 ON QUA «0SSUBMITTED BY: 05 ANALYST-. 643
AMOUNT-AREA<HCHT) * REF. AMNT/<REF. AREA<HCHT># RE8P. FACT)REBP. FAC. FROM LIBRARY ENTRY
NO NAME1 *13C12-2, 3,7, B-TCDD(INTERNAL STANDARD)2 1,2,3.4-TCDD3 1,2.3.4-TCDD4 1, 2. 3.4-TCDDS 2, 3, 7, B-TCDD6 2, 3,7. B-TCDD7 2, 3,7, B-TCDD
NO M/E SCAN TIME REF RRT METH AREA<HOHT) AMOUNT XTOTi 332 660 15; oe i 1000 A BV 1902220. 200.000 PC/UL 26.6i2 320 642 14.36 1 0,973 A BV 2373230. 174.179 P6/UL 23. IB3 322 642 14.35 1 ft 973 A BV 3124500. 178, 907 PC/UL 23. Bl4 257 642 14.35 1 ft 973 A VV 10B3940. 186. 004 PC/UL 24. 755 320 662 15:03 1 i, 003 A«VV S4294. 5,593 PC/UL 0.746 322 65B 14:57 1 ft 997 A«W B4376, 6, B54 PC/UL 0.91
tfjfc 7 NOT FOUNDW
NO RET(L) RATIO RRT<L> RATIO AMNT AMNT<L> R.FAC R.FAC(L) RATIO1 14-. 57 1,00 1, BOO 1,00 200.00 200.00 1,000 1000 1, 002 14-. 29 1,01 8. 96B 1,00 174.16 200.00 1.24B 1433 0, B73 14-. 29 1.01 0. 96B 1 00 178. 91 200.00 1.643 1, B36 0, 694 14i 29 1.01 0. 96B X 00 166.00 200.00 0.570 0.613 0,935 14:57 1.01 i, 000 1,00 5.59 200.00 0.029 1,021 0.036 14:57 1.00 1.000 100 6,85 200.00 0.044 1294 0.037 14; 57 1, 008 200.00 0.513
014398
TCDD 069 DxAONDrrxctin*' FXUBNAMB TJ019B37A05
DXAONOBTXC..__,__ VALUB PABB/FAXL
320/322 ttATZo:SUMRDBATB (0. 60 - 0. 94) 0. 76 PABBAWALVTB <0. 67 - 0. 67) 0. 64 FAIL
ANM.VTB BLUTM MZTHZN 3Of XNTBRNM. BTANOArTD:
SURROOATK BBPAWATKI AT LBABT 5BCANB FKDM ANAkVTB: PABB
014399> ». 00 >3
TCDD Low LBVBU SOLIDQU.BNAMB: TJ019B37A05 CoMi»uCHBM No. ————— DATB 02/29/64SAMPLB: 2UL OF TCDD SAMPLE 19637 ON OMA «05
EPA SAMPLE; ————, CABB NUMBBR: _™——
COMPOUND COMPOUND QUANT REPORT » CORRECTION • RIBIM.T DBTBCTZON LIMITNo, VALUE FACTOR (UO/HO) (UB/MB)
469 237B-TCDD 5.59 0.0060 BDL 0,230 (0,160)
ButmooATB (12.3.4-TCDD) RMCOVMV • (AMT MI ABU-BO / AMT B-ZHBO) * 100X
RBCOVBRV • 69, 7X
CORRECTION FACTOR:• (EXTRACT VOL. (M.) / 0, 1 ML) ft (50 O / AMT BHTRACTBO) ft 0, OOB
su FACTOR • 0, 0080
NOTB: TME 0.160 DETECTION LIMIT ZB THI OPTIMAL (100% RBCOVBRV) DBTBCTZON LIMIT.THB 0, 230 DETECTION LIMIT ZB THE RBCDVBRV-CORRBCTBDi ANAi.yBZB-B-BCXPZC
DBTBCTZON LIMIT.
014400
005.7 94'
s,8 , ____f
SI &
I
'
i i
U.S. ENVIimCNTM. PmTECTION AflENCT - W Smplt M«Aig«Nnt Olfle*r.0. to Ita, Almmcrlo, Virginia 2J3IJ - 70V99KI4M
IMf_E MMCft
Lrtoritory MMI eaauMyi Cm Hmfetr
ORMNICS MM.YSIS DATA SrKT
333Lob *•*!• ID Not iqfelgf__________ gc Mport No...taplo Mrtrlm tell*.____________ ControetNo.i_jjiiOiti tolfNt AutMrliod lyi ______________ Dit* Swplo Noctlvtdi
VOATILES "."•• ' PHTICIBH«DIUM HIM uireii) eoMOEHmATiONi dSSbtPiiiH HI«H ceireit omi
_ DATE KTMCTtO/mi«/«Dl ______________________» PAW MMLTKDl •
WCDIT MF.INKI - PKNINT WISTIMIl _ ^Associated samples________"••••'• Associated samplesMultiply DttMtloo ll-lti by 1 QorQ _____ Hiltl»ly DttwtlM Ililtt bf I QorQ ____
(Ctaok kK tor Aoprofrlito foctor) ICfto* fcw for«|/l
fPI CAW ort|A|IctrcU ono)
Associate «JDlts;|ClS6<a
t,3.7,t-tftricMorodl»Mio»MM) IT4fH)l-6 tt-diailn 0.1611
Ally, 1M5
014402
MSMilCS ANALYSIS DATA SHEET CASE*.QC REPORT*.
1* MUBUBBttH—— . Associate H.i.l..
A. SUMOEMC.fflKE RESULTS
014403
19 v £.s;
\
M M I U M I M r* v V .
MH>W
\
8fi- - . . . - _ _ _
\r\
|-<
L
\ 1 I
11 .404
t»
PROCEDURE: RK DIAGNOSTIC REPORT 2/13/84 7:43:20DATA FILE: TR19B19C05
^METHOD-! TC INITIALIZATION OPTION: 2 PROCE88INC OPTION: 3REPORT: TC8
< ——• STANDARDS——— X —— PLUS UNKNOWNS —— X - UBT NAMES - >PROC USED POSS RtIB PROC USED POBB RUB STANDARD/UNKNOWN
8 2 J, 0 771 45 TCS/TCU
7 COMPOUNDS PROCEBSED, 7 FOUND ''"'' -" ' " "
< COMPOUND X ———————— SEARCH ———————— X SAT X -——• CHRO ———— >NO US ENTRY REF FRED SEL DELTA PEAKS FIT PEAKS H/E TOP DELTA PEAKSA T6 1 -704 704 704 1 Ml 338 704 . 1I TC 2 -681 M4 684 . 13 TC 3 -681 684 684 . .-..-A 9084 TC 4 -681 664 684 1 908B TC 9 -704 704 783 -1 1 '6886 TC 6 -704 784 783-1 1 6887 TC 7 -784 784 784 1 822
1321 684 . . 1257 684 . 1318 783 . 1328 786 3 3857 782 -2 1
••
-SUANTITiHMD CONPUCHEM
•ATXON REPORT FILE: TR1W9C05
DATA-. TR19B19C05. TI02/19/84 7:21:00SAMPLE: BULB TCDD SAMPLE 198198 2-2-84 ON ONA005SUBMITTED BY: 05 • ANALYST: 619
AMOUNT-AREA<HOHT? * REF. AMNT/IREF. AREA(H6HT)* RE8P. FACT)REBP. FAC, FROM LIBRARY ENTRY
,«.,Xvi4)i:».,i',.
NO NAME1 »13Cll-2.3.7, B-TCDD(INTERNAL STANDARD)2 JUB.3.4-TCDO3 l»i.3.4-TCOO4 1..2.3* 4-TC80 •B ;8.»7.B-TCOO . ...•.•••• ••".?;.... •• ' •••-6 2.3.7.B-TCDO7 1.3.7,0-TCOO
NO M/E SCAN TIME REF RRT METH ARSA<HCHT> AMOUNT XTOT1 338 704 15:51 1 1880 W 4986820. 280. OH PC/UL 16.772 328 684 15:24 1 0,9723 322 684 19:24 1 8,9724 287 684 15:24 1 8.971S 328 783 15:49 1 8,999
BV 3864268. 93.261 PC/UL 7.82BV 3874988. . 98,009 PC/UL 7.93W 9999998. 846; 781 PC/UL 45. 85W 146240. 6.382 PC/UL 8. S3
6 382 786 15:53 1 1883 A«W 398498, 12.899 PC/ML J. 887 2S7 782 15:4B 1 8.997 AW 3291190. 24ft 284 Pfi/UL 28.48
NO RET<L> RATIO RRT<L> RATIO AMNT. AMNT(L) R FAC R FAC4L) RATIOA 19:41 181 1000 188 288.88 288.80 X 880 18H 1.002 15:12 1.01 0.968 180 93.26 288. H 8.668 1433 8.473 15:12 181 0.968 188 98.01 888,88 ft 845 1877 8.454 15:12 181 0.968 188 946.78 888.80 2.093 8,766 K 739 19:43 181 1.001 180 6.38 28ft 88 8.832 1812 8.836 19:43 101 1.001 100 12,90 200,00 0.078 1212 0.067 19:43 1.01 1.001 100 243.28 280.80 0.709 8,983 1.22
014407
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1 CROWICS ANALYSIS DATA
libcritcry HI-»I CerouCimn Cm Nunbr. _ _Lib .**>!• ID Noi ~ f?2-gy OC Rtport Ho. /?f/-<ffi'
talia________________ Contrict No.! 96-Ol-Dita Itolint AtrthcriiK Ky:._____________ DWo Impli Rtcdvtd:
KCTICIDES
COWENTHATIONl (Ullp KDIW HIM (clrclt) CONXNTMTIONt UK WDIUH +U6H Ulrelt Oftt)PAH omwcno/fKPAKDi ,___/ "j-f-JTr BATtBATE MW-Dl /-Sf-J'Vr- DAH MMLTZIDlPBCENT MOISTURti _______________l__,-~ PDOKT Winiffil __Associated samples ftfed —I1f6 2>___ Associated samplss_Nultlily Dtttctlm Multi by I or|£| ft"li> Hiltlply Dttoetlon Ililti by I U*U ___
(Chock Sex for Apprcorlrtt Fietor) (CMck •« for Approprlito Fcctcr)—" ug/l
PPf CAW or ugA,gIclrelt oni)i.eu
4I>'J« I-HP-H
DIOXINS.
.... COHCErmwTIONl LOW KBIW HUH (elrclt)DATE IXTHACTED/rWr'A-ai "
Associated samples:______ M^9________________ or up/kg1———'—————~"—'———' lelrelo on)2,S,7,S ttr»qiilerodlboiiie-
1T4M1-t e-aloilF, _____ Q.I6U
July, 19!!
VOLATILE LOW SOLID4* ORMNICS ANALYSIS DATA SHEET • Page 3
Lib Hint; Head CompuChemLib Simple 1.0. No. /&531- njss n OS H BlinkW 1-1 l_l
A. SURROGATE SPIKE RESULTS
COMPOUND
dB-Toluene
d4-l,2-D1cnl3roethane
Bromofluorobenzene
'•'' \
FRACTIONVOA
VOA
VOA
...,
coNciug.'kg )<?-6
_>-3
55'<S-: ,. .
,'
• l.l(Jy t-« *),».*
(iurrogitti only)spike .Added lug/kg )
10
10
10
' ' .&,
.'• --.'..
IRecovery
&£
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5£
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Lot
COMPUCHEM NO. l*,1fP DATE ______ 1 of 2COMPOUND LIST NO. ____
———— IDENTIFIER VOLATILES -• LOH LEVEL SOLID
QUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS VALUE H FACTOR • (uq/kq) LlMlTlm/lia!
2. 221 CHLOROMETHANE ............3. 220 BROMOMETHANE .............4. 231 VINYL CHLORIDE ...........
''If. '••'-• 209 "CHLOROETHANE..............6. 222 HETHYLENE CHLORIDE .......7. 252 ACETONE ..................
,»..•.•• 201 ACROLEIN .................»..;.•&,..202 ' "ttRYLONITMLE ............'10. " 230 TRICHLOROFLUOROMETHANE ...11. 254 CARBON BISULFIDE .........12. 216 1,1-DICHLOROETHYLENE .....13. 214 1,1-DICHLOROETHANE .......14. 226 TRANS-1.2-DICHLOROETHYLENEIS. . 211 CHLOROFORM ...............16. 215 1,2-DICHLOROETHANE .......17. '253 '""'2-BUTM|ONE ...............18. 227 1,1,1-TRICHLOROETHANE ....19. 206 CARBON TETRACHLOR1DE .....21. 257 VINYL ACETATE ............22. 212 BROMODICHLOROMETHANE .....23. 217 1,2-DlCHLOROPROPANE ......24. 250 TRANS-1.3-DICHLOROPROPENE.25. 229 TR1CHLOROETHYLENE ........ Il26. 203 BENZENE .................
,-27. 228 1,1,2-TRICHLOROETHANE ...28. 21B CIS-1,3, DICHLOROPROPENE.29. 208 DIBROMOCHLOROMETHANE ...'.30. 210 CHLOROETHYLV1NYL ETHER...31. 205 BROHOFORM ...............32.'"' 256 ' 4-METHYL-2-PENTANONE ....
.,,34. 255.,' 2-HEXANONE ..............35. 223 1,1,2,2-TETRACHLOROETKANE
PLEASE COMPLETE CORRECTION FACTOR CALCULATIONS ON SECOND SHEET OF THE COMPOUND LIST!!!
014416
COMPUCHEM NO. _____ DATE ••_____ 2 of 2COMPOUND LIST NO. __ ——— —————— IDENTIFIER VOLATILES - LOH LEVEL SOLIDQUANT.COMPOUND REPORT CORRECTION RESULTS DETECTION
COUNTER NUMBER COMPOUNDS________ VALUE x FACTOR • (U9/k9l LlMlT(uo/ko
*
36. 224 TETRACHLOROETHENE37. 225 TOLUENE..........38. 207 CHLOROBENZENE....39. 219 ETHYLBENZENE40. 251 STYRENE41. 239
COMPOUND SURROGATE REPORT MOUNT *. f t RECOVERYNUMBER COMPOUNDS ______ VALUE SPIKED RECOVERY HI NOOK258 D4-1.2.0ICHLOROETHANE (SURR) ..ai 10.0 65 (50-150)233 D8-TOLUENE (SURR).......... 8,30 10.0 V> (81-120)247 BROMOFLUOROBENZENE (SURR).. S,W 10.0 £J (57-137)*
*Adv1sory Limits ' •^ I Recovery • Quint. Report Value
Amount ipuea n 100*
CORRECTION FACTOR CALCULATION: Instrument Code 23B10 9_______
Her HI. of simple used x Dilution Factor " D|py "«<9M Factor
JRT 11/83
014417
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4413
PROCEDURE: RK DIAGNOSTIC REPORT 1/31/83 S3:44:ISDATA FILE: CH01929BB12REFERENCE: V2381 METHOD: VS3B INITIALIZATION OPTION: 2 PROCESSING OPTION: 3
V23BB1
< ~— STANDARDS ——~ X —— PLUS UNKNOWNS —— X - LIST IWIEB - ?PROC USED POBB RMB PROC USED POBB ROB JSTANDARD/UNKNOWN
331 M4. 44 13 1 47 veMBl/VBMUl
< COMPOUND X -———~—— SEARCH •————————• X BAT X -——— CHFW ————— >NO LIB ENTRY REP FRED BEL DELTA fEAKB , PIT PEAKS n/e ~TOP DELTA PEAKS1 Pfl 1 199 C00 E00 . 1 9ST ' , 130 -199 -1 12 F6 1 383 383 382 -1 1 679 . 79 383 1 13 P7 1 443 442 443 1 '._• 983 . S3 463 . 14 PS 2 -37S PS '3 ST 87* FS 4 7» Te7 FS a fa fa• FS 6 -136 136» FS 7 147 147!• FS B -147 147U FS V 162 16211 FS M 177 J.77 17713 FS 11 166 166 16714 FS 12 1V» 190 190IS FS 13 £16 B16 •?
^ 14 FS 14 IM 230Ql7.« IS -841 '841^ IB PS 16 836 2S6
19 FS 17 ES4 2S420 FS IB 8B2 28221 FS 19 290 29022 P6 2 891 29123 F6 3 299 29924 F6 4 327 32723 P6 S 332 33226 P6 6 343 343 34327 P6 7 3S4 334 3S426 P6 8 387 33729 F6 9 -337 3S730 F6 10 -333 333!U F6 11 379 37932 P6 12 409 40933 P6 13 419 41934 F7 8 430 43035 F7 9 -434 43636 F7 4 436 436 . :37 .FT 8 414 •'•4B4 4B436 F7 4 809 309 30939 -F7 7 337 33740 P7 8 660 66041 P7 9 692 69242 PS 8 -234 234 23443 FB 3 4B0 ' 4B0 4B0
£.44 PB 4 621'. 621 621
946264B4 136SB 14836
... 33904 . 101 177924 . 76 167912 .96 190, . .•'..'.'.•»3 .... ....,,, 96
B3 241,• .•. . . 62 236
72 23397117431276575
931 . 130 342 -1982 . 78 394
9773 394
. : . -.. 187 ,.
. .' 63 ' ..173 41038 42838 490
;, . . 83 494' ' ' ' <A4 •'* "*.*,—«»«' 104 . . .—
i • ,948-' . 92 ,4841 939 . 112 309
. 106 399104 699106 691
1 923 , 63 8941 972 . 100 4801 939 . 176 681
QUANTITATIC'N REPORT FILE: CHB19215SB12
DATA: CH01925BB12, TI/""\ 01/31/83 23:08:00..,' -AMPLE: EHP 10CMrU92SB+ieML H20*9UU10936+10941*10933)SPIKE
SUBMITTED BVi 12 ANALYST: 673
AMOUNT-AREA « REF. AUNT/(REF, AREA)* RE8P. FACT)REBP. FAC.. FROM LIBRARY ENTRY
NO NAME1 •••* BWHWCHLOROMETHANE (ZB)2 221 CHUOROMETHANE3 220 BROMOMETHANE ,4 231 VINYL CHLORIDE3 209 CHLOROETHANE6 888 METHYLENE CHLORIDE7 tS8.METONE (8-FROFMWNE) >?B 801'ACROLEZN9 808 ACRVLONXTRXLE10 230 TRICHLOROFLUOROMETHANE11 234 CARBON DXSULFIDEIS 216 1*1-OXCHLOROETHYLENE13 214 1.1-DXCHLOROETHANE14 226 TRAN8-1. 8-DXCHLOROETHYLENE-OS 211 CHLOROFORM16 213 1.2-OXCHLOROETHANE17 233 2-BUTANONEIB 227 i.i,l-TttCHLOROETHANE19 206 CARBON TETRACHLORXDE
ffl 2t * 8-imOflC-l-CHLOROFROPANE ''" 21 237 VINYL ACETATE
28 212 BRONODXCHLOROMETHANE23 217 JU 2-CXCHLOROPROPANE24 230 TRAN8-1,3-OXCHLOROPROPENE25 229 TRZCHLOROETHYLENE26 203 BENZENE27 22B 1.1. 2-TRICHLOROETHANE28 21B CXB-li 3-DICHLOROPROPENE29 20B DXBROMOCHLOR.OKETHANE30 210 2-CHLOROETHYL VINYL ETHER31 209 BROMOFORH32 236 4-METHYL-2-PENTANONE33 * DXCHLOROBUTANE i--34 233 2-HEXANONC39 823 l,l,aa-TETRACHLOROETHANE36 224 TETRACHLOROETHENE37 823 TOLUENE38 807 CHLOROBENZENE39 819 ETHYLBENZBNE ., r,,?'.,':,;;.,":1:,'?;'. ' . '40 , 831 8TYRENE A'41 839 0-XYUNE42 « D4-1/2-DICHLOROETHANE • "•"43 i OB-TOLUENE44 • BROHOFLUOROBENZENE 01.4 20
NO M/E SCAN TIME REF RRT METH AREA(HCHT> AMOUNT XTOT
NO M/E SCAN TIME REF RRT METH AREA(HCHT) AMOUNT XTOT/-> 1 130 199 10.'07 1 1.000 ABB 26917, 10.000 UC/KC 9.01'....'' S NOT FOUND
3 NOT FOUND4 NOT FOUNDB NOT FOUND . '6 84 426 6:55 1 0. -B3 A BV 269236, 60, 982 UC/KC 30,7 SB 148 7.' 31 1 0. 744 A BB 840. 4, 703 UC/KC 2, 36B NOT FOUND9 NOT FOUND „, . . , '10 101 HZ. 9:00 1 0.089 A BB 48342. 8,133 UC/KC 4.09 •*&11 76 167 8:29 1 0,839 A BV B470. 0.763 UC/KC 0.38?12 :,.96 AW 9.39 1 0.9S3 A BB 29909. . 12,386 "UC/KC 6,31 •13 NOT FOWSf ~ ~14 NOT FOUNDIS 83 841 12:13 1 1.211 A 88 <,.'v "8472, 0,444 UC/KC 0,2216 '**48 £36 13:01 1 1, 2B6 A BB " 8103. 2, 742 UC/KC 1,37 wutp17 72 235 12.' 38 1 1,271 A BB 1648. 3.609 UC/KC 2.81 ffIB NOT FOUND19 NOT FOUND20 79 3B3 19:28 20 1,000 A BB 1B030. 10.000 UC/KC 3.0121 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND23 130 332. 17:23 1 1.719 ABB 48572. 11. 178 UC/KC 3,60 •26 76 334 18:00 1 1.779 A BV 100B94. 11,429 UC/KC 3,7327 NOT FODND •• ' ''. .•-.•..• ' ff
O28 ,,73 334 18:00 1 1.779 A BB 1783. 0.706 UC/KC 0,3389" NOT FOUND30 NOT FOUND31 173 410 20:30 1 2,060 AtBB 487. 0.137 UC/KC32 SB 420 21:21 1 2,111 A«_*'. 3044, 2, BS6 UC/KC33 33 463 83:32 33 1,000 A BV 23373, 10,000 UC/KC34 38 430 22:S2 1 2.261 ABB 2067. 2,400 UG/KC35 83 496 23:11 1 2.291 A BB 4047. 0.688 UC/KC36 NOT FOUND37 92 484 '24:36 1 2.432 ABB 65849. 10.910 UC/KC38 112 50? 29:32 1 2, SSB A BV 64220. 9,463 UC/KC39 106 539 28:29 1 2,609 A*BB 1734. 0.330 UC/KG40 104 639 33:30 1 3,312 AtBB 7104, 0.660 UC/KC41 106 691 33:0B 1 3,478 A»VB 3099. 0.472 UC/KC42 63 834 12:39 1 1,276 ABB 84444. B. 897 UC/KC43 100 480 24:24 1 2.418 ABB 97058, B, 293 UC/KC44 176 621 31:34 1 3.121 ABB 31810. S. 843 UC/KC
NO RET(L) RATIO RRT<L) RATIO AMNT AMNT(L) R, FAC R. FAC(L) RATIO1 10:07 1.00 1000 1,00 10.00 . 10.00 1000 1.000 i. 002 1Y33-- ,"*.'41B6 •">•"'''" 40.0ta*rX,V"v""f.74B- "3 8:34 0.2B6 40.00 1.9484 3:33 0.382 40.00 1.1745 4; 41 0,462 40,00 0.6336 6:99 1,00 0.6B3 1,00 60.96 40.00 2, 301 1,6407 7:28 1.01 0,739 1,01 4.70 299.99 9.001 0.066 06 7:2B 0.739 399.99 0.092
,>.* 9 8:14 0,814 399.99 0,160Wlfl 9:00 1,00 0,889 1,00 8,13 40,00 0,373 1.93B 0.20
**
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ORGAN US ANALYSIS DATA HUT
Ittcrittry N—«i CmeiiCium Cm NiiaWrklti .|i-j|l ID Nai ^ ______WH 5 g, K amort No.tmpli Httrlni tefjip Contrict No.!Bit* lltlfMt Auttigruto lyi _______________ Dili imp It tecilvid!
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QUANT.COMPOUNS REPORT CORRECTION
COUNTER JUHBEB- COHPOUKSS____ VALUE x FACTOR •2. 221 CHLOROHETHANE ............ ___ I 'j1 «l ___ 2.5X
2.5
...
3. 220 BROMOMETHANi4. 231 VINYL CHLORIDE5. 209 CHLOROETHANE6. 222 METHYLENE CHLORIDE .......7. 252 ACETONE8, 201 ACROLEIN9, 202 ACRYLONITRILE10. 230 TRICHLOROFLUOROMETHANE11. 254 CARBON DISULF1DE',„...„.12, 216 1.1-DICHLOROETHYLENE .....13. 214 1,1-DICHLOROETHANE .......14. 226 TRANS-1.2-D1CHLOROETHYLENE15, 211 CHLOROFORK16. 215 1,2-DlCHLOROETHANE17. 253 2'BUTANONE18. 227 l.l.l-TRICHLOROETHANEIi. 206 CARBON TETRACHLORIDE21. 257 VINYL ACETATE22. 212 BROMODICHLOROMETHANE23. 217 1,2.DICH.OROPROPAN£ ......24. 250 TRANS-1.3.DICHLOROPROPENE.25. 229 TRICHLOROETHYLENE ........26. 203 BENZENE ..................27. 228 1,1,2-TRICHLOROETHANE ....28. 218 CIS-1,3, DICHLOROPROPENE,,29. 208 . DlfiROMOCHLOROMETHANE .....30. 210 CKLOROETKYLV1NYL ETHER31, 205 IROMOFORK32, 256 4-«nHYL>2>PENTANONE ......,34. 255 2>KEXANONE
...,
2.52.52.55050502.5
_____ 5'_/!_ 2.5
2.52.52.52.51002.5)xC2.552.52.52.52.52.52.552.52.52.5SOSO
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35. 223 1,1,2,2-TETRACHLOROETHANE. ___, ^ ,___ 2.5
PLEASE COMPLETE CORRECTION FACTOR CALCULATIONS ON SECOND SHEET OF THE COMPOUND LIST!11
014444
COWUCHEK NO. . _____ DATECOMPOUND LIST NO. ———— . mnlL-s ..
QUANT.COMPOUND REPORT CORRECTION RESULTS KTKTIOIj
COUNTER JIJM5ER COMPOUNDS ________ VALUE X FACTOR • Jli9/>jl LlKiTlup'ke
36. 224 TETRACHLOROETHENE37. 225 TOLUENE38. 207 CHLOROBENZENE,3>. ' 219 ETHYLBENZENE40. 251 STYRENE41. 239 0-XYLENE
,COMPOUN3 SURROGATE REPORT WOUKT *• t t RECOVERYNUMBER COMPOUNDS ______ VALUE SPIKED RECOVERY H1NDOK258 D4.1,2,DICHLOROETHANE (SURR) 7J.O 10.0 72 (50-150)233 Dj-TOLUEW (SUP,?,).......... ,,7S 10.0 £7 (81-120)247 BROMOFLUOROBENZENE (SURR).. (f.Ut 10.0 tf (57-137)'
'
"Advisory Limits^ * Ricovery • OiiB*t. Report Value
Miount ipueo * *00«
CORRECTION FACTOR CALCULATION: Instrument Code 23610 g ______
Ver Ht. of sinple used " Dilution Factor * "ry Height Fector •
JRT 11/83
O •' 014443
, _ _ _ _ _ _ _ _ _ _ _ _ _ . T,—————
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PROCEDURE: RK DIAGNOSTIC REPORT * 8/31/84 U:17:5:DATA FILE: GR019259A18REFERENCE: V233
_ METHOD: V23B INITIALIZATION OPTION: S PROCESSING OPTION: 3,' ^ REPORT: V23BS1
•c -—— STANDARDS ——— XPRClC USED POSS
3 2 1RM50
44 COMPOUNDS PROCESSED.
< COMPOUND >
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ENTRY1112
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<; ——REF-230-412-492-33-67-106-130-172-183-183-195-212-203-224-248-362-271-286-285-314-381-323-328-358-362-373-3B5-386-387-383-409-437-430-481-4B4-486-SIB-948-611-752-798-284-514-696
PREO22941149153851041281701811611932102012222462602692842833123193213263563603713833643B53814074354484794B24B4516546609750796282SIS.694
—— PLUS UNKNOWNSPROC USED44 12
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|i QUANTITATION REPORT FILE: CR8i'?259AJlB *
DATA: CR019239A1B. TI08/81/84 10:38:00SAMPLE: 10 CM OF SAMPLE #19859 + H UL 1118*11113 + SPIKE ON #18SUBMITTED BY: #16 ANALYST: 633
MOUNT-AREA * REF. AUNT/(REF. AREA)* RESP, FACT)RESP. FAC, FROM LIBRARY ENTRY
NC NAME1 * BROMOCHLOROMETHANE (18)S 821 CHLOROMETHANE3 820 BROtlOMETHANE4 231 VINYL CHLORIDE ' ~B 209 CHLOROETHANE6 282 METHYLENE CHLORIDE7 232 ACETONE (2-PROPANONE)8 801 ACROLEXN9 202 ACRYLONTTRILE10 230 TRICHLOROFLUOROMETHANE11 234 CARBON DI8ULFIDE12 216 1.1-DXCHLOROETHYLENE13 214 1,1-DZCHLOROETHANE14 826 TRANS-1. 8-DICHLOROETHYLENE13 811 CHLOROFORM16 215 t, 2-DZCHLOROETHANE17 253 2-BUTANONEIB 887 1. it 1-TRICHLOROETHANE19 206 CARBON TETRACKLORIDEM t 2-8ROMO-1-CHLOROPROPANE21 857 VINYL ACETATE22 212 BROMODICHLOROMETHANE23 217 1,2-DICHLOKOPROPANE
I 24 250 TRANS-li 3-DICHLOROPROPENt:' 25 829 TRICHLOROETHYLENEi 36 203 BENZENE
27 828 1,1, 2-TRICHLOROETHANE28 818 CIS-1,3-DICHLOROPROPENE89 808 DIBROMOCHLOROMETHANE30 810 2-CHLOROETHYL VINYL ETHER
. 31 80S BROMOFORM' 3? 256 4-METHYL-2-PENTANONE
33 * DICHLOROBUTANE, 34 2SS 2-HEXANONE1 35 223 1.1.2. 2-TETRACHLOROETHANE
36 884 TETRACHLOROETHENE37 885 TOLUENE33 807 CHLOROBENZENE39 819 ETHYLBENZENE ' . • ' .
! 40 231 BTYRENE . "." " '41 839 0-XYLENE . • •48 # D4-1,2-DICHLOROETHANE .'" '43 ^ DB-TOLUENE
I 44 ill BROMOFLUOROBENZENE
| NO fl/E SCAN TIME REF RRT METH AREA(HCHT) AMOUNT
Q \
NO n/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT KTOTI 130 229 11:38 i 1. 000 A BV 65152, IB. 000 UG/KG 4,42P NOT FOUND
, 3 NOT FOUND: 4 NOT FOUND5 NOT FOUNDf> 84 fJTO , 6:38 1 0.742 ABB 672736, , 92.044 UC/KC 40. 65 1-7 38 1,82* 9: 15 i 0, 795 A BB 4195. ' ~9. 326 UG/KC ' 4. 12"6 NOT FOUND9 NOT FOUND «...••- — • ——— ; —— — _10 101 2ttrM0:40 1 0.917 A 8V 194364. . ' 17. 867 UC/K& 7,63 "'U 76 SK 10:16 1 0.882 ABB 13124.. - - .IS 96 /'228s, 11:17 1 0.969 ABB 34911 /"II. 246_UC/KC 4. 97i]"-~13 NOT FOUND ———— r 2- .""" "14 NOT FOUND . , . . ' . ' • - -13 83 869 13:40 1 1.173 ABB : 3763, 0, 354 UO/KC 0.1616 62 265 14: 29 1 1. 245 A BB . 3478. 0. 565 UG/KC 0. 25
i 17 72 283 14:23' 1 1.236 -ABB 2611. . 3, 362 UC/KC 1.4818 NOT FOUND
| 19 NOT FOUND: 20 79 411 20: 54 20 1, 000 A BB 23678. 10. 000 UG/KC 4. 42, 21 NOT FOUNDi 22 NOT FOUND' 23 NOT FOUND
24 NOT FOUNDi SS> 130 S.S3& 18:32 1 1.680 ABB 79825,' 26 76 7384119:31 1 1.677 ABB 118254,, 27 NOT FOOfflTi 28 73 384 19:31 1 1.677 ABB 1993.., .» 0, 442 UG/KC 0,19.I 29 NOT FOUND ' ' .L.x30 NOT FOUND •~i"'W31 173 434 22: 04 1 1, 695 AtBB ,. 616, t. 054 UG/KG 0, OS'• 32 SB 44B 22: 46 1 1. 956 A BB 402, 0. 201 UG/KC 0. 091 33 35 491 24: SB 33 1, 000 A 6V 33B3S, 10, 000 UG/KC 4. 48; 34 SB 479 24: 21 1 2, 092 A BV 3989. 0, 912 UG/KC 0, 40t 35 83 483 24: 30 1 2. 105 A BB 1358, 0, 142 UC/KC 0. 06
36 164 484 24: 36 1 8, 114 A BB 663, 0, 074jyC/ilG_ .AJ37 93 i_5E>26:17 1 8,858 ABB 91813, 10. 94'9 UG/KG 4. 57 "C38 113 CMST' 87: 45 1 8, 364 A BV 109200, Y7TBaO-/KC' 3. My.39 106 £10 31:00 1 8,664 ABB 506, TOTTUC/KG 0.03''
• 40 104 752 38: 14 1 3, 884 A*W 1344. 0. 076 UC/KC 0. 03' 41 106 799 40: 37 1 3, 469 AtBV 1984. 0, 184 UG/KC 0, OSI 48 65 283 14: S3 1 1, 836 A BB 58480. 7. 193 UC/KG 3, IBt 43 100 512 26:02 1 2, 236 ABB 84828. &. 731 UG/KC 3,661 44 176 694 35: 17 1 3. 031 A BB 107636. 6, fM£ UG/Ktf 3. 03
NO RET(L) RATIO RRT(L> RATIO AMNT AMNT(L) R. FAC R, FAC<L> RATIO1 11:38 1,00 1.000 1,00 10,00 10,00 -,000 1.000. 1.002 2: 42 0. 231 40. 00 0. 477 "
! 3 .4:22 0.376 • ,.,40.00 & 052 ...• 4 5:20' ,.0.459 ''40.00 1.697 '' S 4:33, • 0.563 "40.00 .' 0.355', 6 4:36 1,00 0.748 1,00 98.04 40.00 E 381 1.128 2.30
7 9: 12 1, 01 0, 790 1, 01 9. 33 299. 98 0, 002 0, 069 0. 03B 9:13 0.795 399,98 0.1009 9:52 0, 847 399.98 0,20810 10: 44 1, 00 0. 921 1. 00 17, 27 40, 00 0, 746 1. 728 0. 43
_ft 007.773\\- 01444t
NO RET(L) RAT-0 RRT(L) RATIO AMNT AI1NT<L) R. FAC R. FAC(L) RATIO11 10:13 1 00 0,87S 1, 00 0.96 40. 00 0. 055 2. 574 0. 08
._ 18 11:80 1. 00 0,974 i, 00 11, £5 40, 00 0. 811 0. 749 0. 28> 13 12:33 1079 40. 00 C. 330
"' 14 13:16 1 140 40. 00 0, 58715 13:40 1.00 1.175 1,00 0,35 40,00 0.014 1631 0,0116 14:29 1 00 1245 1 00 0,57 40, 00 0, 013 0, 944 0.011Y 14:23 100 1.236 1,00 3,36' 299.98 0.001 0,119 0.01IB 15:58 1.362 40,00 1,18919 16:16 1,397 40.00 1,57380 30:54 1 00 1 000 1 00 10, 00 10. 00 1. 000 1 000 'f 1 0081 16:19 1,403 ... 40.00 1,38582 16:34 1.484 40.00 0,18883 18:06 1335 40, 00 -0, 82484 18:18 1,372 40.00 1.7725 18:58 1,00 1680 100 9.05 40.00 0.306 1,354 0.2326 19:31 1,00 1677 100 10.01 40.00 0.454 1,613 0.2387 19:34 1 Ml . :* 40.00 105628 19:34 100 1661 1 00 0,44 40.00 0.008 0. 694 0.0129 19:25 1668 40,00 1,63830 20:41 1,777 , 40. 00 1 10231 22:07 1,00 1,900 1,00 0,05 40.00 0.008 1,743 0.003S 22:46 1,00 1,956 100 0,20 60,00 0.001 0,306 0.0033 24:58 1,00 1.000 100 10,00 10,00 1000 1,000 10034 24:21 100 a 092 1,00 0, 91 60, 00 0, 010 0,672 0.0235 24:30 100 & 103 1,00 0,14 40.00 0.006 1690 0,0036 24:36 1,00 2,114 1,00 0,07 40.00 0.003 1,377 0,0037 26:17 1,00 2. Z3B 100 10,35 40,00 0.350 1,353 0,2638 87:45 1,00 2.384 1.00 7,08 40.00 0.419 8,386 0.18.
Uj39 31:00 1,00 Z, 664 100 0,08 40.00 0.008 0,968 0.00(rpjl 40 38:07 100 3,275 100 0,08 40,00 0.005 S, 717 0, 00
41 40:85 1,01 3.472 1,01 0,18 40.00 0.008 1,657 0,00i 42 14:23 100 1.236 1,00 7,20 10,00 0.806 1120 0,72
43 26:02 100 2,236 1,00 8,73 10,00 1.308 1,491 0.6744 35:14 100 3,026 100 6,86 10.00 1652 8,408 0, 69
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ORGANIC* WAIYSIS DATA SHEET
L*britor» HIMI _Mti< CamuCtitn Cm NtmM-lLib limit ID Na-r-r- MA0D gc dtpcrt NotSpplt Hrtrlm lifl • _'" Contrict No.iDtta MtiMi Autlwlild-Byi __^___________ Dfti Sm»ll RtetlirtdiAssociated samples; • .
CONCENKIATIONl (gplCDIIIM HIM (clrcDATE EXTRACTEO/FREWKIEOl .___
BATE ANMLTZEOl _____nHCtKT MOISTURE!
Multiply Dtttrtlon llplti by 1 Qcr loQer Jj 4^(ChtcK Ion lor Awroprlitt Ftetor)
SEMI-VOLATILE UN SOLIDORGANICS ANALYSIS DATA SHEET - Pige 3
Lib Mime! Held CompuCheinLib Smpll I.D. No'._/f£££_ SJ SS P DS Q -1"*
. A. SURROGATE SPIKE RESULTS
COHPOUND •
.•Fluorophinol
2|4,6-Tr1brMophino1
D-Phinol
DS'NlfOBinune
Dj4 P-Tirphinyl
2-Fluorob1?henyl
FMCT10MSENIVDA
SEMIVDA
SEHIVOA
SEHIVOA
SEHIVOA
SEMIVOA
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yjoozosvtysv//to
3100
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COHPUCHEM NO. _____ (Mil'. COMPOUND LIST HO. ———— IDENTIFIER SEHUYDLATlLtS - 'LW LEVEL SOLID
QUANT.
COMPLETE CORRECTION FACTOR CALCULATIONS ON THIRD SHEET CF THE ttfOUND LIST! 11
014470
COMPOUND LIST NO. ___1——— IDENTIFIER KMMOLAT1LE5 ~*IOH LEVEL SOLID
QUANT.COMPOUDD REPORT CORRECTION RESULTS DET LIMIT
COUNTER NUHBER COMPOUNDS_____ VALUE K FACTOR »
I 74 419i 75 406 BENZO|G,H,nPERYL-NE ____ ____ ___
014471(Ste eilculitlont in* lurrogitit en tack)
' •' . ' COHPUCHEM NO. ____DATE *____ 3 of 3COMPOUND LIST NO. ___ ™ "
i . .. ——— IDENTIFIER 5EM1-VOLAT1LES - LOU LEVEL SOLID
'"S QUANT.QUANT. REPORT
COMPOUND SURROGATE REPORT AMOUNT t tt ACCEPTABLE•UMBER COMPOUNDS VALUE SPIKED X RECOVERY RAN6E
619 2-FLUOROPHENOL W 125 f ITH H (2C..16)112 D nENOL I.I 115*
""Bs-HTMBEIIZaiE 11 Ittf448 2-FUIOROB1PHENYL llr US tKB TRIBROMOPHENOL % 115471 OH-WRENE tt> m*'4B6 DM-TIRPICNYL T). ' IK 4
f9jg ' (IWW)r / (17-125)(,1 (82-124)*^•f ( « )1,1 (S4-126)*
\ Rtcovtry • Quint. Riport Vilutquini. mpori moum .puto *
"*>.CORRECTION FACTOR CALCULATION;
Drytutnetlon »o1-Be(»H 80 g Dilution
Ul ror Mid, o.»ni for w » tat migni .xtrictta 191 * Fietor « Fietor *1,6 6-i.u mo u.s
f M) 50 qni igi
QUANT. REPORT AMOUNT SPIKED CONVERSION FACTOR;
250 ul _____ Flnil Ertrict »•!. W) _Mount sgrrogitt AOOIQ tui i * . m Tor Mid, o.wi rar H * Fitter. •
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PROCEDURE: RK DIAQNOBTIC REPORT 2/01/8410:11:30DATA FILE: «H019260M9 ' • •REFERENCE: FBCC7
" METHOD: FBCC7 INITIALIZATION OPTION: 2 PROCESSING OPTION: 3REPORT: FBCC7B1
< —— 8TANDARPS ——— >< — PLUS UNKNOWNS —— X - LIST NAMES - >PROC UKD POSS RMS PROC USED 'POSS RM8 STANDARD/UNKNOWN
A 6 1' 93 94 19 1 740 FBCC7B1/FBCC7U1* 4 1 n ••"•_-)• 14- 1 99 F8CC7B2/F«!C7U2
88 COMPOUNDS PROCESSED, 23 FOUND ..„.„, • ,,. i i .•.••i.;v'v.:'"*"!',, " -:**;11' .
< COMPOUND X ———————— SEARCH ———————— X BAT X ———— CHRO ————— ">NO L» ENTRY KEF FRED BEL DELTA'PEAKS • FIT PEAKS M/E TOP DELTA FEAKS1 Cl8 C23 C34 C49 C9* C4
O
-80? ,811 812 1-1029 1027 10S7 . i 983-1337 ,.,1340 1339 -1 ..,.,,» 994-1999 1402 1M2 - . i 983-2080 2084 2084 . 1 799-2409 2414 2419 1 1 944
7 Cl 2 -399 3988 Cl 3 -767 771 769 -2 1 9849 C l 4 -766 7 7 0 . . . .1 0 C l 9 -777 7 8 1 . . . .11 Cl 4 -782 784 789 -1 1 99318 Cl 7 -803 807 . . . .13 Cl B -818 814 819 -1 1 99814 Cl 9 -840 844 ...19 Cl '10 -848 844 . . . .16 Cl 11 -862 864 . . ...17 Cl 12 -869 869 . . • .
' IB Cl 13 -887 .891t 19 Cl 14 -888 892 892 . 1 996
80 Cl 19 -892 896 . . . .< 21 Cl 16 -910 914 . . . ., 82 C2 2 -990 999 . . . .
23 C 2 3 -964 9 6 9 . . . .24 C2 4 -979 960 . . . .2 9 C 8 9 -991 9 9 6 . . . .26 C2 6 -1014 1019 . . . .
1 87 C8 7 -1009 1010 . . . .88 C8 6 -101B 1083 1081 -8 1 999
; 29 C2 9 -102B 1033 . . . .30 C2 10 -1047 1098 . . . " .
' 31 C2 11 -1061 1066 . . . .32 C8 18 -1131 1136 1136 . 1 99833 C8 13 -1149 1194 . . . .
' 34 C8 14 -1189 1194 . . . ., •;.- .i 39 C8 19 -1809 1810 . . . . . ' ...I 36. -8 14-1818 1817 .•-*•; ....V'.'Vn-, 37 C3 8 -1834 1839 . ...-,;-., 38 C3 3 -1864 1869 . . ' .
39 C3 4 -1301 1306 . . . .40 C3 9 -1309 1314 . . . .
i 41 C3 6 -1313 1318 . . . .' 48 C3 7 -1340 1349 . . . .
43 C3 8 -1348 . 1347 1349 -8 1 99144 C3 9 -1396 ' 1368 1367 29 1 44749 C3 10 -1377 1383 . . . .46 C3 11 -1371 1377 . . . .47 C3 12 -1382 13BB 1387 -1 1 9164B C3 13 -1427 143349 C3 14 -1434 1440
190 812134 1027144 1339188 1402240 2084244 84197494 76993 74993 784128 789146146 819108144108121
. .1081PF&.30 B91 -1
11712382 99813912293109162ISO 1081128187889107 1136119237 -...194194 -. ,142138143 1304
194 1349184 n,109 !'168169 1387149 1430ao4 .. .. ,
;
90 C3 19 -1433 143V , . .9 1 C 3 1 6 -1469 1471 . . . .9 2 C 3 1 7 -1494 1460 . . . .93 C3 18 -1498 1464 . . . .9 4 C 3 1 9 -1463 1469 . . . .s 9 9 C 4 2 -1920 1923 . . . .J 9 * C 4 3 -1949 194B . . . .97 C4 4 -1980 1983 1989 2 1 89998 C4 9 -1604 1407 . . . .89 C 4 6 -1411 1419 . . . .40 C4 7 -1718 1722 1721 -1 1 9686 1 C 4 B -1818 1888 . . . .48 C9 8 -1B98 1868 1861 -1 1 9934 3 C9U»cth,3 . . . .M ClT 4 -1987 199149 C9 9 .44 C9 4 -8077 8081 . . . •' .4 7 C 9 7 -8100 8104 . . . .48 CB B -8089 8089 . .49 C9 9 -8238 8848 . . . .70 C4 .-.. 8 -8381 8389 . . . .71 C4 3 -8387 8331 . . . .7 8 C 4 4 -8417 8481 . . . .
. 73 C6 9 -8886 8891 . . . .1 74 C6 4 -8909 8910 . . . .. 79 C4 7 -3084 3089 . . . .
76 C7 8 -618 421 682 1 1 993t J7,. C7 3 -749 748 . . . ." 78 C7 4 -907 910 910 1 9905 79 C7 9 -1219 laaa laaa . i 988i 80 C7 4 -1480 1483 1483 . 1 990
81 C7 7 -1899 1899 . . . .C7 B -1890 1894 1893 -1 1 994
ABB •.138198169 146177 1466248284866 19B417B 160617B 1619149 1721802 1821802 1861,'M4 ,. .149 1991892888 aoeo149 8103a?!8 8088149 8840232 8389898 8338898 8480876878876112 48899 74888 910178 1838330 1483818 1898844 1893
1 111111
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014476
8 005800
1QUANTITATION REPORT FILE: W019260A19
DATA: OH019260A19. TI/-48/01/B4 9:82:00'.' IAMPLE: 1UL §19260 +(9UL 10910 «033) ON «19BUiniTTEO BY: «19 ANALYST: 699
• AMOUNT-AREA « REF. AHNT/(REF. AREA)* RESP, FACT)RESP. FAC. FROM LIBRARY ENTRY
NO NAME1 4D4-1.4-DICHUMOBENZENE <I8>8 441 N-NITROSODIMETHYAMINE3 410 PHENOL
473 ANILINE411 DI8(2-CHLOROETHYL)ETHER401 a-CHLOROPHENOL481 1.3-DICHLOROIENZENE488 1.4-DICHLOROBENZENE474 BENZYL ALCOHOL
10 480 1,2-DICHLOROIENZENE11 480 8-METHYLPHENYL18 418 BXB(a-CHLOR018_PROPYL>ETHER13 488 4-METHYLPHENOL14 448 N-NXTR080-DI-N-PROPYLAMINE
, 19 434 HEXACHLOROETHANE14 440 NITROBENZENE
, 17 *440 DB-frtPHTHALENE (IB)> 18 438 IBOPWONE
19 404 8-NITROPHENOL20 403 8,4-DIHETHYUPHENOL81 410 BIB(2-CHLOROETHOXY)METHANE88 489 BENZOIC ACID
I 83 408 8,4-DICHLOROPHENOL84 444 l,a,4-TRICHLOROBENZENE
< 29 439 NAPHTHALENE •26 479 4-CHLOROANILINE27 434 HEXACHLOROBUTADIENE28 608 P-CHLORO-M-CREBOL29 477 2-METHYLNAPHTHALENE30 439 HEXACHLOROCYCLOPENTADIENE
: 31 611 8.4.6-TRICHLOROPHENOL38 484 8,4, S-TRICHLOROPHENOL
i 33 -D10-ACENAPHTHENE (18)34 414 a-CHLORONAPHTHALENE39 479 3-NITROANILINE36 429 DIMETHYLPHTHALATE37 402 ACENAPHTHVLENE
i 38 488 8,6-DINITROTOLUENEI 39 478 8-NXTROANILINE -n*»\ 4a 401 ACENAPHTHENE
41 409 8,4-DINITROPHENOL48 .407 4-NITROPHENOL43 474 DIRENZOFURAN44 487 a.4-DINITROTOLUENE49 424 DIETHYLPHTHALATE46 417 4-CHLOROPHENYL PHENYL ETHER
& \
NO NAME47 438 FLUORENE48 480 4-NITROANILINE
,'">9 604 4.6-DINITRO-O-CREBDL-SO 443 DIPHENYLAMINE (N-NITROBO)91 430 1.8-DIPHENYLHYDRAZINE (AZOBENZENE)98 «447 D10-PHENANTHRENE (IB)93 414 4-IROMOPHENYL PHENYL ETHER94 433 HEXACHLOROIENZGNE99 409 PENTACHLOROPHENOL94 444 PHENANTHRENE ... M , .87 403 ANTHRACENE • w" '"" .•"«*1-«"1*1 • ' '98 484 DI-N-BUTYLPHTHALATE89 431 FLUORANTHENE40 *499 Dia-CHRYBENE (IB)41 449 PYRENE48 404.BIMZ.DfNE43 419 lUTYLJENZYLPHTHALATE44 423 3,3'-DICHLOROIENZIDINE49 409 IENZO(A)ANTHRACENE44 413 BIB(a-ETHYLHEXYL)PHTHALATE47 418 CHRY8ENE48 489 DI-N-OCTYLPHTHALATE49 »Dia-BENZO(A)PVRENE (IB)70 407 BENZO(B)FLUORANTHENE71 409 BENZO(K)FLUORANTHENE78 404 1ENZO(A)PYRENE73 437 INDENO(1.8i3-C.D>PYRENE74 419 DIBENZO(AiH)ANTHRACENEt79 408 IENZO(0,H, DPERYLENE174 419 2-FLUOROPHENOL (8URROOATE)77 D9-PHENOL (8URR00ATE)78 447 D9-NITROBENZENE (BURROOATE)79 44B a-FLUOROBIPHENVL (BURRDOATE)80 TRIBROMOPHENQL (BURRO-ATE)81 D10-PYRENE (BURROOATE>
. 82 D14-TERPHENYL (BURROOATE,
i NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT1 190 812 10:09 1 1,000 A IV 6*907. 40.000 NO 3.928 NOT FOUND
O
3 94 769/9:37 1 0.947 A 8V 66141. *£5V979 N8 a.aB/«O4 93 769 9:37 1 0.947 A BB 8193. 1.094 NO 0.109 93 784 ,9:4B 1 0.9*6 A*BB 8049. 0.81* NO . 0.076 188 789 • 9:49 1 0.967 A BV 93304. fg-7938 NO . a.77i-Bl7 NOT FOUND _____________B 14* BW^lOill 1 1.004 A BV 71013. (T39.009 NO 3.089 NOT FOUND10 NOT FOUND , „*.IL NOT FOUND18 NOT FOUND13 JNOT FOUND _14 130 891 11:08 1 1.097 A BV 49098. ( 4.711 NO 10.94/gp19 NOT FOUND14 NOT FOUND17 136 1087 18:90 17 1.000 A BV 174818. 40.000 NO 3.92IB ,88 998 11:96 17 0.933 A*BV 1961. 0.494 NO 0.04
_ OH478
NO M/E SCAN TIME REF RRT METH AREA(HOHT) AMOUNT XTOT19 NOT FOUND
/-?0 HOT FOUND_,-l NOT FOUND88 NOT FOUND83 NOT FOUND ^____________^84 180 1031/12:46 17 0.994 ABB 90370. /"S7T004 NO 3.89/g)89 NOT FOUND ' ————————————86 NOT FOUND27 HOT FOUND ____________88 Vff 1134/14:13 17 1.10* A BV ,,44893.*: fS.'odfi NO i. 9-*fc'!)89 NOT FOUND30 NOT FOUND31 NOT FOUND , '*".38 NOT FOUND ' ''"'<33 1*4 1339 14:44 33 1.000 A BB # 91370. 40.000 NO ., 3.9834 NOT FOUND • < > - .39 NOT FOUND ' ': 3383KM'1'34 143 1304 14:18 33 0.974 ABB 1144. 0.333 NO 0,0337 NOT FOUND38 NOT FOUND39 NOT FOUND ______________^40 194 1345 16:49 33 1.004 A BV 83834. {&,.009 NO a noJg>41 NOT FOUND •-»*—
NOT FOUND- *•?•NOT FOUND1*9 13B7-"17:80 33 1.03* ABB 7833.-' 7.323 NO 0.64/«.149 1430 17; 92 33 1,068 A BB 1909. 0.461 NO 0.04NOT FOUND ..,...,,„.••..••„..-.•
\7 NOT FOUND . . •• *".!««K,- •'48 NOT FOUND49 NOT FOUND90 169 1461 18:16 33 1.091 A»BB 447. 0.894 NO 0.0391 77 1466 18:19 33 1.099 A BB 4BO. 0.093 NO 0.0198 188 1602 80:01 93 1.000 A BV 194779. 40.000 NO 3.9393 NOT FOUND94 NOT FOUND99 366 19B4><L9:4B 93 0.9B9 A BV 9139./ 16.479 NO 1. <96 178 1606 20:04 92 1.008 ABB 798. 0.186 NO 0.0897 178 1619 80:11 93 1.008 ABB 796. 0 300 Nfl 0.0898 149 1781 81:31 98 1.074 A W 306398. £30.781 NO 2.'99 808 1631 88:46 93 1.137 ABB 8103. 0.498 NO 0.0460 840 8084 86:03 60 1.000 AW 98384. AO, ana MO y aa61 808 1B61«X83:16 60 0.893 A BV 1349*0. OS. 713 NO62 NOT FOUND63 149 1991 84:93 60 0.999 A BB 639. 0.839 NO 0.0364 NOT FOUND69 828 8080 86:00 60 0.99B A BV 3441. 0.730 NO 0.066* 149 8103 8*: 17 40 1.009 ABB • •;.-. 1914. 0.922 NO 0.0947. 828 8088 86:04 40 1.008 A VB 8097. 0.431 NO ' 0.0*68 149 8840 28:00 *0 1.079 ABB 8891. 0.348 NO 0.0369 864 8419 30:11 69 1.000 A BV 93898. 40.000 NO 3.9870 898 8339 89:04 69 0.963 A*BV 8141. 0.833 NO 0.0771 898 8338 89:09 69 0.966 A*VB 8901. '1.027 NO 0.0978 898 8420 30:19 69 1.008 A BV 8191. 0.896 NO 0.0873 NOT FOUND'4 NOT FOUND i
, V
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NO M/E SCAN TIME REF RRT METH AREA(HQHT) AMOUNT XTOT79 NOT FOUND
~76 112 682 7:46 1 0.766 A BV 130440. 93.978 NO 8.1777 99 760 9:36 17 0.748 A 3V 119323. 61.831 ?« 5.3078 63 910 11:28 17 0.886 A BV 64017. 27.490 NO 8,4279 172 1222 19:16 17 1. 190 A BV 220827. 76.282 NO 6.7080 330 14B3 IB: 32 33 1.108 A BV 23383. , 79.786 NO A. 4*
NO RET(L) RATIO RRT(L) RATIO AMNT AMNT(L),, , R. FAC R.FAC(L) RATIO1 10:07 1.00 1.000 1.00 40.00 40,00- 1.000 1.000 1.00
96 0.4B8 90,00 0.93439 1.00 0.948 1.00 29,98 90.00 0.612 1.177 .0.9234 1.00 0.947 1.00 1.09 90.00 0.020 0.910 0.0243 1.01 0.940 1.01 0.82 90.00 0.019 1.168 0.084* ,,1.00 0.967 1.00 31.93 90,00 0.493 0.788 0.43
i 7 10:02'*' ' 6.993 90.00 0.898B 10:09 1.00 1.004 1.00 39.00 90.00 0.697 0.938 0.709 10:30 1.038 90.00 0.98410 10:31 1.041 90.00 0.83711 10:46 1.066 90,00 0.79412 10:49 1.069 90,00 0.899
; 13 11:09 1.096 90.00 0.809• 14 11:06 1.00 1.098 1.00 124.71 90,00 0.417 0.167 8.49i 19 11:09 1,103 90.00 0.434' 14 11:88 1.189 90.00 0.480jj 17 18:49 1.00 1.000 1.00 40.00 40.00 1.000 1.000 1.00
IB 11:98 1.01 0.987 1.01 0.49 90.00 0.009 0.9B8 0.0119 18:03 0.940 90.00 0.80180 13:11 0.991 • 90.00 0.39881 13:33 0.947 90.00 0.97383 13:40 0.969 • 890,00 0.33683 13:34 0.960 90,00 0.876
, 84 18:43 1.00 0.993 1.00 37.00 90.00 0.831 0.311 0.74>> 89 18:91 1.003 90.00 1.148'! 86 13:09 1.031 890.00 • 0.894
87 13:16 1.039 90,00 0.19986 14:08 1.00 1.103 1.00 83.01 90.00 0.319 0.4BB 0.44
, 89 14:83 1,131 90,00 0.39630 14:93 1.160 90,00 0.06831 19:04 1.176 90,00 0.193
, 33 19:09 1.162 390.00 0.178' 33 16:43 1.00 1.000 1.00 40.00 40,00 1.000 1.000. 1.00
34 19:89 0,933 90,00 1.134.39 19:48 0.949 890.00 . 0.49336 16:16 1.00 0.973 1.00 0,33 90,00 0,010 1.999 0.01
I 37 16:88 0.979 90.00 1.734..' 38 14:89 0.983 90,00 ' , 0.304* 39. 14:49 1.008 -890,00 • 0.084-, 40 14:44. 1.00 1.004 1.00 33.01 90,00 0.734 1.118 0.44
41 14:97 1.014 890,00 0.043I 48 17:13 1.030 139,00 0.114i, 43 17:08 1.039 90,00 1.449I 44 17:16 1.00 1.034 1.00 7,38 90,00 0,069 0.466 0.19> 49 17:90 1.00 1.067 1.00 0.46 90.00 0,017 1. BIO 0.01':.:; 46 17:99 1,073 90.00 0.464V • 014480
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RET(L> RATIO RRT(L> RATIO AMNT AMNT(L) R. FAC R. FAC(L) RATIO17:9918:19<8i 10IB:13IB:1719:9919:0019:1919:4980:03 ;t,<00 1.00380:0881:8888:4384:0083:1383:4184:80.84:3489:9884:1984:0487:9830:0789:0189:0930:13
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00 0.988
072 90.00 1.291096 2-0.00 0.049033 290. CO . 0.130
00 1.00800 1.07400 1.13700 1.00000 0.893
0.89300 0.999
1.00100 0.99900 1.01000 1.00200 1.07600 1.00000 0.9*3-400 0.96600 1.003
00 0.89 90.00 0.004 0.666 0.0100 0.09 90.00 0.004 8.879 0.0000 40.00 40.00 1.000 1.000 1.00
90.00 0, llil90.00 0.193
00 16.47 90.00 0.087 0.081 0.33.00 0.19 90.00 0.004 1.098 0.001.00 0.20 90.00 0.004 0.976 0.001.00 30.76 90.00 1.077 1.749 0. *8IfOO 0.49 90.00 0.011 1.104 0.0100 40.00 40.00 1.000 1.000 1.0000 38.71 90.00 1.094 l.*78 0.*9
.•«.. .. 80.00 ...;•: 0.01000 0,84 80.00 0.009 1.088 0.00
90. 00 0.03900 0.73 90.00 0.080 1.3*0 0.0100 0.93 90.00 0.01* 1.491 0.0100 0.*3 90.00 0.017 1.339 0.0100 0.34 90.00 0.018 2,674 0.0100 40.00 40.00 1.000 1.000 1.0000 0.83 90.00 0.018 1.103 0.0800 1.03 90.00 0.089 1.318 0.0800 0.86 90.00 0.019 1.097 0.08
3*:04 1.19B 90.00 0.49934:19 1.80* 90.00 0.97937:48 1.899 80.00 0.8937:43 1.01 0.764
00 0.74600 0.86900 1.1B900 1.10700 0.69800 1.1B2
00 , 92.98 • 90.00 1.806 0.649 .8600 61.89 90..00 0.946 0.446 .2300 87.49 90.00 0.302 0.990 .9900 76.2B 90.00 1.011 0.6*8 .9300 79.79 -80.00 0.809 0.139 .9800 80.49 90.00 8.336 1.493 .6100 77.43 90.00 1.074 0.693 .99
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OS5WIC5 ANALYSIS DATA SHEET
Libcratory Hainai Mtit) Cmeueimi 6aia HimbwiLib la*la ID Ma.i l«?3fe/ pc daoa-t No.tImpla MalrlKi iaiu Oontract No.iData talaiaa AvtMrliad lyt ___________ Data i«*pla RacalvadiAssodtted simples:___;________
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SEMI-VOLATILE LOH SOLIDORGANIC* ANALYSIS DATA SHEET - Pigt 3
Lib Mi-t! HtidLib Smplt I.D. Mo. /W/ 0 SS H OS Q
A. SUMO-ATE SHKE RESULTS'
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( ' ——— IDENTIFIER SEM1-VOLATILE5 - LOH LEVEL SOLID
O QUANT.QUANT. REPORT
COMPOUND SURROGATE REPORT MOUNT I tt ACCEPTABLENUMBER COMPOUNDS VALUE SPIKED R RECOVERY RAH6E
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CORRECTION FACTOR CALCULATION;
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METHOD: FSCC7 INITIALIZATION OPTION: 2 PROCESSING OPTION: 3REPORT: F8CC7S1
< —— STANDARDS ——— X —— PLUS UNKNOWNS —— X - LIST NAMES - 5PROC USED P088 RM8 PROC USED POSS RMB STANDARD/UNKNOWN
6 6 . 1 97 94 13 1 84 F8CC7B1/PSCC7U16 6 1 97 34 14 1 84 F8CC7B2/F5CC7U2
< COMPOUND XNO LIB ENTRY REF PRED BEL DELTA PEAKS FIT PEAKS IVE TOP DELTA PEAK1 Cla caa ca
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c — —REF-830•1098•1494•1826•2434•2722-331-789-77B-796-796-821-833-873-870—906-907-93B-936-931-996•1009•1029•1048•1066•1102•1077•10921102•113111491246•12971311133213401364•1406146114971473149B19011-241994193B199916291629
PRED83311011497182924378729339793782BOO800829837877•7491091194294093996010131029109210721106108110961106113911931290126113191336134413681410146914611477190S1909192B19981942196316291629
—— BCIBEL83311021497182924372726
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014517
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OUANTITATION REPORT FILE: OJ019361A14
DATA: OJ019261A14, TI02/03/84 9:13:00SAMPLE: 1UL 4U9261J +<9UL 10999 »033) ON #14SUBMITTED BV: «14 ANALYST: 699
AMOUNT-AREA » REF. At1NT/(REF. AREA)* REBP. FACT)REBP. FAC. FROM LIBRARY ENTRY
NO NAME1 «D4-li4-DICHLOROBENZENE (IS)2 *U N-NITROSODINETHYAMINE • *.., , .3 610 PHENOL4 473 ANILINE9 411 BIB<8-CHLOROETHYL)ETHER6 601 8-CHLOROPHENOL7 481 1.3-DICHLOROKNZENE '"•"B 482 1,4-DXCHLOROBENZENE9 '474 BENZYL ALCOHOL10' 420 1.,2-DICHLOROBENZENE11 620 2-METHYLPHENOL12 412 II8(2-CHLQROIBOPROPYL)ETHER13 622 4-RETHYLPHENOL14 442 N-NITROSO-DI-N-PROPYLAMINE19 436 HEXACHLOROETHANE16 440 NITROBENZENE17 M60 DB-NAPHTHALENE (IB)IB 438 I80PHORONE19 606 2-ttXTKOPHENOL20 603 2.4-DINETHYLPHENOU21 410 BIB(8-CHLOROETHOXY>METHANE22 629 BENZOIC ACID23 602 2.4-DICHLOROPHENOL24 446 1.2,4-TRICHLOROBENZENE29 439 NAPHTHALENE26 479 4-CHLOftOANlLINE27 434 HEXACHLOROBUTADIENE28 60S P-CHLORO-M-CRE80L29 477 2-METHYLNAPHTHALENE30 439 HEXACHLOROCYCLOPENTADIENE31 611 2.4i 6-TRICHLOROPHENOL32 626 2. 4. 9-TRICHLOROPHENOL33 «D10-ACENAPHTHENE (IB)34 416 2-CHLORONAPHTHALENE39 479 3-NITROANILINE36 429 DIMETHYLPHTHAUATE37 402 ACENAPHTHYLENE38 428 2.6-DINITROTOLUENE39 478 2-NITROANILINE40 401 ACENAPHTHENE
' 41 609 2,4-DINITROPHENOL42 607 4-NITROPHENOL43 476 DIBENZOFURAN44 427 2.4-DINITROTOLUENE49 424 DIETHYLPHTHALATE46 417 4-CHLOROPHENYL PHENYL ETHER
014518
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NO NAME47 432 FLUORENE48 480 4-NITROANILINE49 604 4.6-DINITRO-O-CREBOL90 443 DIPHENYLAMINE (N-NITROBO)91 430 1.2-DIPHENYLHYDRAZINE (AZOBENZENE)92 M67 D10-PHENANTHRENE (IB)93 414 4-BROMOPHENYL PHENYL ETHER94 433 HEXACHLOROBENZENE99 609 PENTACHLOROPHENOL3fc ^ 4 rHENnPITnREIwS AI' «£' ''97 403 ANTHRACENE '' ' '•''""••' . • "98 426 DI-N-BUTYLPHTHALATE99 431 FLUORANTHENE .. „..,,...60 *499 D12-CHRY8ENE (18)61 .449 PYRENE. ,68 ' 404 BENZIDCNE"63 419 BUTYLBENZYLPHTHALATE64 423 3.3'-DICHLOROBENZIDINE69 409 BENZO(A)ANTHRACENE66 413 BI8(2-ETHYLHEXYL)PHTHALATE67 418 CHRYBENE68 429 DI-N-OCTYLPHTHALATE69 *D12-BENZO(A)PYRENE (IB)70 407 BENZO(B>FLUORANTHENE71 409 BENZO(K>FLUORANTHENE72 406 BENZO(A)PVRENE73 437 -NOENO(1.2,3-C.D>PYRENE74 419 DlBENZO(AiH)ANTHRACENE79 40B BENZO(C,H. DPERYLENE7t> 61* 2-FLUOROPHENOL (BURROOATE)77 D9-PHENOL (SURROGATE)78 447 D9-NITROBENZENE (BURROOATE)79 44B 2-FLUOROBIPHENYL (BURROOATE)80 TRIBROMOPHENOL (SURR08ATE)81 D10-PYRENE (SURROOATE)82 D14-TERPHENYL (8URRQOATE)
NO M/E SCAN TIME REF RRT METH AREA(HSHT) AMOUNT XTOT1 190 833 10:29 1 1.000 A BB 39669, 40.000 NO 2.682 NOT FOUND v3 94 793 •/ 9:98 1 0.992 A BV 36743, (55.69B NC 2.4 NOT FOUND9 93 WO 10:00 1 0.960 iA BB • . 'IIBB. y 300 NQ 0.086 12B BOO •lOi 00 1 0.960 A BB 28694. (57.336 KB 2.
- 7 • NOT FOUND146 836 •'lO: 27 1 1.004 A BB™ 39928. <JtTo07 Nfl 3. 02/S-
9 NOT FOUND ..»>.,».• , ;„-(.,•, . ...10 NOT FOUND . "11 NOT FOUND ' • • • • ....«,.. ....lE;.. "<••;.'18. NOT FOUND • ' . '•''•*'• '"••:13 NOT FOUND ' _.———————————^^14 130 940* 11:49 1 1.128 ABB 21292. .$23.936 NC 14.98/fD19 NOT FOUND16 NOT FOUND17 136 1102 13:46 17 1.000 ABB 79384, 40.000 NC 2.68IB 82 1011 12:38 17 0.917 ABB 374, 0.289 0. M_, 0.02
X
NO M/E SCAN TIME REF RRT METH AREA(HBHT) AMOUNT XTOT19 NOT FOUND20 NOT FOUND21 NOT FOUND122 NOT FOUND23 NOT FOUND
180 1096»/13l42 17 0.999 ABB 26298. 3,432 NO 2.29 126 1109 13:49 17 1.003 ABB 1404, 0.649 NO OTW26 NOT FOUND27 NOT FOUND
^266 1808 22:36 92 0.989 A BB 2924r r2lT639 NO
.
107 1292 19:39 17 1.136 A BV »6930. YS7T963 NO 129 NOT-TOUND '*•• ..»("'T,.. . • •• •«•*• . • •'i*tSj/j'£','.•$&,£ •'30 NOT FOUND31 NOT FOUND , . ,.,;„.,.,,<.St.' NOT FOUND '.•.••w-*> ' •-*>(-•• •33 164 1497 18:43 33 1.000 ABB"*,.,.. 87849. . 40.000 NO 2.6834 NOT FOUND • .(S,;1,- * '" •••.'.39 NOT FOUND - • " ""•"*• v ... , ' '36 163 1464 IB: IB 33 0.978 A BB S94. ' '0:969 NO 0.0437 192 1461 IB: 16 33 0.976 A BB 793, 0.779 NO 0.0938 NOT FOUND39 NOT FOUND
194 1904 18:48 33 1.009 ABB 39818. M.BOO N0_41 NOT FOUND3£> NOT FOUND iff.43 'NOT FOUND* _•;' " '""'• "• •*••«&:Q$> NOT FOUND/*,*49 149 1627 20:20 33 1.087 ABB 1271. 1. 120 NO 0.0846.. NOT FOUND47 NOT FOUND . v... , .48 NOT FOUND . ""™" ' "'49 NOT FOUND90 NOT FOUND <~r91 NOT FOUND92 1BB 1829 22:32 92 1.000 ABB 44097. 40.000 NO 2.6893 NOT FOUND
NOT FOUND
96 178 1834 22:99 92 1.003 ABB 683, 07707 NO 0.0997 178 1843 23:02 92 1.008 ABB 663, 0.610 NO 0.04
-JB 149 2002 28:01 92 1.099 ABB 83978. f49.368 NO 3.31/5?99 202 2106 26: 19 92 1. 191 A BB 832. 0.744 NO OT09
, 60 240 2437 30:28 60 1.000 A BB 22832. 40. OOP NO 2.6BRA 61 202 8196* 26:97 60 0.889 ABB W134. ., lf.2,176 N8 3.90 j$?* 62 NOT FOUND '
63 149 8340 27:13 -0 0.760 A SS 399, Q. 749 V« 0.0964 NOT FOUND69 22B 2433 30:29 60 0.998 A BB 609. 0.734 NO 0,0966 149 24B4 31:03 60 1.019 ABB •* ~"12BB. •.•„„ • 1.984'NO 0.11
. «7 3B8 8441 30:31 60 1.002 ABB '" "*.. 619. :;'..' 0.963 N8 0.0668 149 2618 32:43 60 1.074 ABB 1297.' 0.932 NO 0.0669 264 2729 34:04 69 1,000 ABB ' 21262... >' 40.000 NO 8.6870 292 2666 33:19 69 0.978 A BV 1606. 2.068 NO 0. 1471 292 2671 33:23 69 0.980 A VB 1117. 1.911 NO 0.13
y, 72 292 2730 34:07 69 1.002 ABB 1961. 2.761 NO 0.1873 276 3019 37:44 69 1.108 ABB 1499. 9.966 NO 0.37-*** 74 NOT FOUND
79 276 3096 36:43 69 1.137 A BV 776. 3.263 NO 0.2276 112 606 7:34 1 0,727 A BV 64739. 97. 907 NO 6.93
s~\ 77 99 791 9:93 17 0,716 A BV 92646, 68.763 NO 4.6178 82 996 11:97 17 0,868 A BV 20910. 27.293 NO 1.8379 172 1399 16:96 17 1.230 ABB 120076. 111. 938 NO 7.9080 330 1679 20! 99 33 1. 122 A BB 9890. 87.373 NO 9.8981 212 2192 26:94 60 0.863 ABB 129901. 126, 979 NO 8.4882 244 2209 27:37 92 1,206 A BV 92732. 129,829 NO 8.70
R.FAC R.FAC(L) RATIO1.000 1.000 1.00
:08 0.399 90.00 0.791:92 1.01 0.991 1.00 32.70 90.00 0.741 1.133 0.69:43 " 0.937 90.00 , ... 0.963-.87 1.01 0.999 1.00 , 1.20 90.00 0.023 0.973 0.02:97 1.01 0.999 1.00 37.34 90.00 0.978 0.774 0.79
10:16 0.989 ••;.,. . 90.00 0.82010:29 1.00 004 1.00 48.01 90.00 0.797 0.886 0.9010:99 .092 90.00 0.433
10 10:92 .048 90.00 0.78111 11:19 ,092 90.00 0.96912 11:20 ,093 90.00 0.19613 11:43 .130 90.00 0.64414 11:42 1.00 1.128 1.00 223.94 90.00 0.429 0.096 4.4719 11:38 1.122 iM.OO 0.32916 11:97 1.192 90.00 0.33317 13:43 1.00 1.000 1.00 40.00 40.00 1.000 1.000 1.0018 12:37 1.00 0.919 1.00 0.28 30.00 0.004 0.697 p.'0119 12:49 0,934 "" 90.00 0.17120 13:06 0,994 90.00 0.28321 13:21 0.973 ' 90,00 0.49022 13:46 1,004 290.00 0.12323 13:28 0,981 90.00 0.24124 13:39 1.00 0,999 1.00 43.43 90.00 0.279 0.321 0.8729 13:46 1.0026 14: OR27 14:2226 19:34 1.0029 19:4330 16:2331 16:3932 16:4933 18:40 1.00
004 1.00 0.64 90.00 0.019 1.196 0.01030 249.99 0. 183046 90,00 0.191139 1,00 27.96 90.00 0.179 0,318 0.99149 90.00 0.236194 90.00 0.077213 90,00 0. 184220 249.99 0. 143000 1.00 40.00 40.00 1.000 1.000 1.00
34 17:03 0,913 90.00 '1.92938 17:34 0.941 H49.99 0.'44336 18:16 1.00 0,978 1.00 0.97 90.00 0.016 1.398 0.0137 18:13 1.00 0,979 1.00 0.77 90.00 0.023 1.471 0.0238 18:29 0.986 < 90.00 O."26139 18:4340 18:46 1.0041 19:0342 19:2943 19:1344 19:2949 20:19 t. 0046 20:19
003 . ' 249.99 •.,",'.;*.„. 0.041 ..009 1.00 43.80 90.00 1.029 1/179 0.88020 249.99 0.066040 129,00 0. 103029 90,00 1.768044 90.00 0.393OB6 1.00 1.12 90.00 0,037 1.630 0.02086 90.00 0.924
NO RET(L) RATIO RRT(L) RATIO AUNT AMNT(L) R.FAC R. FAC(L) RATIO47 20:12 11.082 90.00 1.26448 20:33 MOO 24V. 99 0.02349 20:37 1.104 249.99 0.13190 20:43 1. 109 90.00 0.90191 20:49 1.111 90.00 1.79192 22:49 1.00 1.000 1.00 40.00 40.00. 1.000 1.000 1.0093 21:40 • 0.990 90.00 0.18194 21:98 0.963 90.00 0.29099 22:33 1.00 0.986 1.00 21.64 90.00 0.093 0.123 0.4396 82:83 1.00 1.00397' 83:01 1.00 1,00898 84:99 1.00 1.09999 86:17 1.00 1.19260 30:29 1.00 1.00061 86:94 1.00 0,88462 30:01 0,90863 29:13 1.00 0.96064 30:34 1,00969 30:22 1.00 0.99866 31:01 1.00 ,01967 30:29 1,00 .00268 32:41 1.00 .07469 34:01 1.00 .00070 33:18 1.00 0,97971 33:21 1.00 0.98072 34i«9 1.00 .00273 37:40 1.00 . 10774 37:48 ,11179 38:40 1.00 , 13676 7:30 1.01 0.72377 9:90 1.01 0,71778 11:99 1.00 0.66679 16:93 1.00 1.23080 20:97 1.00 1,12281 26:91 1,00 0.8B282 27:34 1.00 1,206
00 0.71 90.00 0.016 1.134 0.0100 0.61-- 90.00 0.012 4.987 0.0100 49.37 90.00 1.918 1.937 0.9900 0.74 90.00 0.019 1.016 0.0100 40.00 40.00 1.000 1.000 1,0000 92. IB ' 90.00 2.072 1.986 1.04
90.00 0.01000 0.79 90.00 0.014 0.931 0.01
90.00 0.02400 0.73 90.00 0.021 1.449 0.01,00 1.98 90.00 0.049 1.429 0.0300 0.96 90.00 0.022 1.127 0.02,00 0.93 90,00 0.044 2.362 0.02,00 40.00 40.00 1.000 1.000 1.0000 2.07 90,00 0.060 1.461 0.0400 1.91 90; 00 0.042 1.100 0.0400 2.76 90.00 0.099 1.064 0.0600 9,97 90.00 0.099 0.493 0.11
90.00 0. 49200 3.26 90.00 0.029 0.447 (i. 0701 97,91 90.00 1.306 0.670 1.9900 68.76 90,00 0.961 0.408 1.3600 27.29 90.00 0.216 0.399 0.9900 111.96 90.00 1.274 0.969 2.2400 87.37 90.00 0.284 0.163 1.7900 126.98 90.00 4.411 1.743 2.9300 129.83 90.00 1,684 0.648 2.60
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OF.8MIICI MW.VIII DATA KH
Laboratory Naaai CgaBiieiy Caaa NmMr _L* fwila ID Hoi " " "iMalt IMrliilData Malaat* Mtarim fti
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COHPUCHEH HO. CW/ DATEIDENTIFIER PESTICIDES (LOH LEVEL-SOLID)
COMPOUND LIST - NO.___
COMPUCKEMCOMPOUND
COUNTER NUMBER COMPOUND NMC RESULT DETECTION LIH1T (ug/fcfl)
! , QUANT. ;.•*•;• •COMPOUND SURROfiATE ' S RECOVERY REPORT CORRECTION ;» <!ffi' NWMT f
j NUMER COHPOUN05 -1N80V VALUE FACTOR RESULT SPIKED RECOVERY
I 0738 DIIUTYL CHLORENDATE (41-121)* ___ ___ /ffi ft? S"0
b «*,„,.«, ' •., »• °14549
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Nunber- lVK6i! CAUL* B333 -PA». UK
or weight txtraettd" ,UbFinal txtrar.t Volunt- UDUiititn Factor- 1Dry Weight
fht Calculation Equation «.... ;,,., - , • . - • ' , . •• ,r•>•••/,'•'';- A?'.iri. '' • . " • - • ...'.'. ' " y'HJ»-- • •» • " 'J
Sanp-t ArtaSlaridard~Arta * Std Cont '» Uilngn I Split « rin«) Voi
.... Uinp.i (feint)* or Wtiqht,./ Drtfiflht ,K«tar.•jr-jr!';!*. .....:,.., •• *»•".. .;,. .
'• •'•.'vMt"" " -•• »B!ita Kor UoHpound BAI1HA BHU•np.i «PM • 6BHOstandard Art* • 14000Standard lionctntratinn • ,4ConctntrMian of -Arthfl IHIC IP Y7.71M ug/kg
Oata ForUonpound HEPTACHLOHCrinple Arta * tifjuu • • . . . . .Standard Arta • itiuOQStandard Concentration • ,4Concentration of HmMiMLUK .• '/0,22-£!
O D a t a |.or Conpound AUDRiNSaHDlt Arta - B1UOinr, • . ........Standard Ar»a « 14000titandard Conctntr-tion » ,4Concentration of ALDK.N •(•••'*"' it 9b ug/kg
uata r'or linnpounflB«npj,e Area • 6^UO nStandard Area •= i.iOOOUtandara Concantration « ,4Conctntrfltun of lU-LDklN is '/6.307V ug/kg
P«t«,l'«r Uonpoond t-NDRINC*nplt Arta « 6y«0 "**!?•"',•,„. ,., . ••' .Utandard Arta • iODOO •• ,, r.Standard Conctntration • .4 ,,., . ..."'" .,Uonctntration of CNUK-N . in 104 ug/kg
ata, For Conpoundr - 6 4
ODT
Standard Concentration • .4 i • • '/ ,„,. .^_ • ..Conctntr.tion of Dt)l < i« 170,667 ug/kg
19
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8 11 32 23 lOOUOEhUl 74206 SH 74206.IKS8,'2i! I5-.6- ,100001:'1(11 63-!i-. 8H 633.3,2.00,43 33,Bi ..OIIOOe+Ql V4U72. UH 93872.125B,'.iK 33.07 , 1UOUUM01 ISlMyii, U[( ISMVM.^.8.6634,41 .lOIIUUtl'Dl J1464. SH 31463.7508,9V 3U.74 JOOOOM01 74!iUO. &H 74MIO..UO9,07 36,04 .lOOOQlM'Ot 107633. Sr 107633.SOO
_ _3V,02 .lOOOOU'lOl10,OU 40,OS .lOUOOErOt
i7 44 3V ' 'linmsc'j.in "f" ;11,47 4S.17 ,1?71S(;-07 _..,..,,
13'Ii!,'4L; 4V.'3ii ,iiiuii6H(ii "3(1661.12.b6 4V,91 ,101)001: 01 1UI>46. SI4 C. *JA Cll .O 4 flflf.flL J./I4 4Lli:l:.f i!l.
. , . ., 74 SD.62 JUOllOt+qi l-';>i<U.. ^,02 51, 74 .IDuOOCtUl 1 7727. U), . .6 'J-,47 ,JUOOOI+(J1 17(1 VW.K, tlf
ALOIUN
1B_4'-,U7S137'
!.,», 13,VI) "5b.b4 ,, .IDUIIOtilll .4140. SI 'J4140.250LJ 14.i!U b6,7tf • ,1(100(It'101 3IIV6, BH KIIVb.7t.il ..W 14 Hll SV l3 lOliuUt+Ul 10166-, SB 101662,-00 fr,
16,lib 6b,77 .lOOOOMul 1311.46. tiH J31U46.SOII r
"' ! W1552
16,72 66,4- .IV,36 6U.9D .KlOOOLHO) 3 171, 13H, 3!J3'/1,bOU17,UV 71.il .10IIOIIH+I11 6-36671. UBM36671.00(1
111,3V 73, OB .^-Ul^t'OV 33041, CH ,002 W"DM>BH y:] B OuOL'rl L'766 SH 6000. 89 ?>. F .19 46 77 33 1UPUOE+»1
1V.63 7U;00 .iOIHMIMUl9. _6 78.90 .lOOOOE+01
.SO, 47 81.31 ,o610t"0720,76 82.47 .iOIIOOK 1-1)1
/.2i,4V.:fl5.a»:p... .iOflOOE+01-21,74 86. 40- .lOOOOI-fOtIi',07 67.69 ,10000r.||il22.31 Ba,66 lOllOOC+Ot,
90,62 JOOOOtMfll
. . , -• -., If:lliU:fi •.illlKSli *
, . . 4i>ac[7ifc. r.n iSSifgg; 60 'wSS.'ysi12.571)1, UV 123901, SOU'/IOlid. BV 710!iU,000IpOOOliMU 107-613. BV 10966U.-00
lOOOOCtOl 344037, SV 344036.7'JOH888B+M Worn, ey saoin.yBiii
6673Vb76. Total AKL'A X - 66611.'JO(II'rocenna-d data file. MVb-J kaw (Jata'-TI'lti KV-i!l
•,1| iblK V •
"I M /i '. V*-'
01.553' t (*)i Ifc,
RtlPLITUDE x.26 uV-*«concJ» (CnUryvd
0
1,014554
Report' 3»Bfl,00 GhanniO i 2 M2333 ssSanp\iti CP 19262 Tnjnct-d M 12i45iR9 ON FFB 3, 19B4earn Method. PACK 02 spq> SEWS 8ub*q/8*«p' 1/45 Rt)> isSi-width MV/Min I)*!*); «in-Ar Bunnh
.500 .300 0,06 20 AutoBup-Unk BvT ID-UJ R«f-RTH XRTW XOU-fNO 0.00 0 ,,.30 <>,0 -Id
Actual run tinm 2S.017 ninuttiEnded not on bantl.nt • , , , , . . .
RT ; ITM Factor Ar-« ..•-. V;"' UC/ML N*n«
.10000F+01 !S«ifl7a, BB 15S872,03fl
.lOOOOHfOl B671SO, BB B67150,000t7R ,SB 3i?aia,37oss mmSB ) 0533,81?!. BB 2750,641
iOT: R :.5i ffl SB.10533, SB ) 0533,81?!2751. BB 2750,641
R., SB ,264 FNPRIN
103B7, SB .010 ENDOBUUFAN (I
._. __,__ .10000F.+01 )2?11. SB 1??11,SOO •."...,B6 B9.37 .10000I-.+01 9697. SB 9697,000SI,11100.00 ,miSF.-06 37570. BB ,006Total Are* => 306S77R. Total UQ/HL - 37570. DOOPror.ti«ed d«t* filtt P2545 Raw dAta film
014555
Ii' . . •i
o N
014558O
U.I. miMMCNTM. PROTECTION MCNCT • CU> hanla Manaaawnt OlflcaP.O. Km III, Ala*tia>la, Virginia »J» - 70J/5J7-J4K)
lAWlCMMER
ORMNICI MMLTtll DATA HCffT
Labcratery Na«iLab hatla ID Hoi
Jsteetlen Delta ky(CMek k* (or Affnjrlete
PESTICIDE IOW SOLIDMSAMCS AM.VS1S DATA MET • Plfli 1
n» liaaes fcl. CoiOuClie-
i.h Uaali l.P. to. -S k? Q$$ EOS QlUnk
; "ewoufe ' •-••Dlbutyl chlonndiU
"1."
- .-,.»
-to.. " '
4.
•fMCT!Mi| COK (us/il •
KST1MM
• '•. .., . t.
fll.nr»••
•
••• .'4l
, &'<fr ,
(S>rrosi*tt»fUI
Udti (uc'kl
15
' ' ' 'W-r
...'*.,
•
'?..•* ;y'.'.;-c ,-".•' ?~p*" k •' If ' ,»
JM:e.i
ft
• •
i '•'•a
}O •? 014553
COMPUCHEM NO.IDENTIFIER PESTICIDES (LOH LEVEL-SOL 10 I
COMPOUND LIST - NO. _ _____
COW1ICHEMCWPII-ND
RESULT DETECTION L1H1T (ug/kg)
., .HUAItT. , .. .CMffOUND SURROGATE I HECOVEKV MfOKT CORKCT10N MAlNT IIMtER COHPOUIPS HIHDOH VALUE FACTOR RESULT SHIED RECOVERY
0738 DIBUTYL CHLORENDATE (41-121)* ___ ___ 3fi 6ft 3*f
\> *Adv1iory Llrtt , 014560,^ ' . . 88
_'-..»•'
O
UoMpuChtn NiM».««r" 1 .6.5 -A__* 2332 I.Hrt* fill
Uolune or weight extracted- , Ob kUogransFinal Lxtrart Volime>> bapiit= 4Dilution Factor" 1Dry Weight Meter* 1
Tht Calculation Equation in." "''"•"• ' •••
Sanplt ArtaStandard Arta * Std Cone *, Dilution'* Split * final VoiConcentration^ - •••— • ——— • - ——— » —— '•— — • — - — — —— ••• — —Uanplt Volunt or Height /Dry Might ractor
• •""" ..'",.. •'•' ...,..• -Data Kor Uonpound GAnhA BIIU ' •>>..>Sanplt Arta • 2700Standard Arta « 14000{standard Concentration • ,4Uonctntration of bANMA WHU is 3ll.8b7l ug/kg
Data hor Co-pound H£PTACHLUI(aawple Arta • UisOOStahdard Arta • 1UOOOStandard Conctntration • .4Concentration of Ht.riACHl.UK IB 7..'/7'/U ug/kg
»•»."'.O p a t a h'or Uonpound ALDR.NSaMplt Arta • 7VOOStandard Arta • 14000
Utandarri Concentration • ,4Conctntratun of ALVK1N if 9J.20&7 ug/kg
l;or Conpound DIELDR.Npound- bt»0Standard Arta • 1-POOStandard Concentration • .4Uonctntration of UltLUlUN i« 67.69S3 ug/kg
Oata hor Conpound ENDR.NSanplt Arta « 6400% „.Standard Arta • 10000 ... ...„.„...,•, >.Standard Uonctntration • .4 ;••<••':. .Uonctntratian of t:Nl)MN i« 102.4 ug/kg
Data for Conpound DOT ' •• '*•fianp-e Ar-a * -Voo • _„ .:£«Standard Arta • 6000 ... „ •,. , "Standard Uenctntration •> ,4 •Uonctntration of OUT U 104 «g/kg
014561
*'
x.2S uv-*tcon.»- (enlarged x 32.22J" " ro *xi w ro o> oS o> is a a~ w (0 <B ID
r» IV IB IB 193., W W « 01
3"
?M
-S?TJ OiPM..
PIMOF>'-I
8.,
_jSf*«' ;a*snf5«M
.*«s1————118.88
iB.'jep—W..I*. tB.89^ ,„ L.19.40Slfa0'——"-"Ti1 ....,. ..... ..—:——rrr-r-j20.93'
—•—26.76 -.•. LimwghX'.. ..,»••»
..p.. ,t*<,-r
; ' '•!!>.
014562
16,7366,04 .1(1000!...!01 S4VU7VU. UH'J4VU7'/U.OO(I^ 17.01.67. IB ,10000(5+01 /,y;<jv'• U.H .,V.32.4'6?5
-?.'lu' '/ft.'6'" ,'_(liMfc>"ul 636illi?V.' t)W6363Ui!V.'0001U.40 7-.67 .1000015+01 77U77. -H 77877.0001(1.US' 74,b9 .illOOIIMOl i!4-'644, b 24.644,00(1tf;»-ii6 :i!!IO M: «iHM.-:blao.il) 77.6U ,101)00(5+01 0, -H 0.000__ . J *| ^J, V £| F ........ . . ............ ............. .....
|JoiV3 B..'66
2b',-lMDI)!oO .'.Ii076 -0'j 24VM>'. 8V ' ''.270 »I)UC-•._.'/6igi.73 .1UOOOM01 31VII!iU..M» 31VOlil*.SOfl•fo.JJ , Are« •,M 60'iJ1676, ' lotal AllU'A X • 3170i>5,.00
data filti P9WU '"' K'VIH data filn
01.563
He-port i V17b,(in Channel' 9 C«!333 (HiUariplei I'H 19263 Injwett.i at liiiUi4U ON r'liW Z, 171)4(•.till) Method i kl'AV Oeqi SttfVS UubRq/Si«Hp i 1/211 BtJ i i!(iai-width rlV/Min U.Uy Min-Ar Bunch
.25(1 3.00(1 3,0(1 3W7
Actual run tinti 30.004 ninutti . . 'Ended nit en haetlint •• .
V '•/.'••*". •' ... ":<n< ITH , factor . . Arta . AM A X
''"''*''•' ' *'i
ii-Bl? •*S!!99.'it!!l • ..........o. 86 ...... ...p. 0003,1- 12,5. .'iOdflOMOl 742'/73.' Oil 74i!77i:.'7-03.47 U.2V .101)0015+111. 49IW43, SH 493S4.J.OOO3,,!i4 '" — .-—--. -.-- -. ----- -----3.S4 13,97 , iqqounm viwv. DH VMIJ/A3.71 14.63 . IpOUUtrUl 1266020. 3H1,;!66B20 00.4,1116,21 .100001M01 3_J41)3, !iH _i'l4(12,!i(IO4,86 16,02 .10000(5+01 076.1.. Oil 096S0.075mm '-ssiHi '«Hiii4.H. 19.13 .lOOOOt+01 77HSOO. -I 778577.750f;fi{ ftflr* lillUKIi. Wgft: _t JoWToo15,i!_.««0.65 •'"•'. JUMBK+fll 6446(10. Gt 6446(10, 1UUS,.Ml 21.24 .10000(5+01 S6SM4, ,SH.S6S614.120.S.4V HI. 69 . lOOOOCiOl '/37W41. mW/iOfAl ,000'J.86 i.'3,12 , lOODO.tOl 71417. UN 91417.2506.111 23,7? .100001.101 '-1S04. OH t>lMJ4.ii'U6,2324,60 .10000ti:il)i 24lUlii. Oil 2401-1,0006,i<6 2b, 11 .iOQOOt+01 K9liH3(l, OH ?9yi!i!0,0(l(lb.Sfi 2!i,7b .1000015+01 631172 SH 631171,'/SO6.611 M6.37 .100QOi:+01 2670 . »I W.70{!4,3706,77 26,7. .101)0011+01 2022i!6. Oil 202226,Iib'07,OS B'/.BS .lOOOOMUi _?£';4A. UH 'J4;:V46,l.ll(l?,«•/ -U.7U ,101100(5+111 274,f»A7, Olli>74306V,0007,63 30.13 .10000HU1 1!»'74. UH l\.i"/'t.Wi-7,96 31.43 .41101D.-D7 0471)4. SH ,003 Olil.frt Bill!- .. f- .......... ........ ... .......... ......B.ii .t',03 . ipoooi.:iin mw<!. BH W'J'AS.KUU 44 33 33 10IIIIOI5+III 06>>70. 0)1 06970,0008,W 33.66 ,iOOOOL.|(li 24U3KI'!. CH 4113 .7.11a.V',1 34,-4 .lOIIOIIKrlU 'J4477. lill -44911.~6£8,116 34,97 .lllOOUt.'401 OUK4;:. SH 00t'4i|.0pi8.97 3..4U .lOOOOE+Ol •.•••44427. -H 343.7,1259,i'0 36 33 , JUOOOLHOl • 1Z1UO, OH li.'HIO,21>(l9,41) 37,32 .lOOOOErOi 194676. UH 193676.1209.W, 3'/.69 . KIUOOH01 W96U4. OH iiWm,O.'/U9,71 30.33 .10000-rOl 462U3. OH 46222.BOO9,'liC 3!/!69 IliiOO'OIHOi9 71 30 33 10000(51.01 -,__, ... .__.---9.V1 3V.14 ,S.'6769t--(l7 Uil^..iiH .000 ..liri'TACHUlK10,0037,00 •- ..lOOOOt+01 0347606. 8HQ44y6l)6,000; .10,60 41.Ob .lOOOOkHOl 10X113.1. Iffl 030.%'
.100UOl5.|.Ui 1600307. OH1600307.UOO., iiiooottoi 7«'/i'/sy. n d'/r/ii'J.noo'
.iOOOOE+Oi 1122439, _H112243V>,000
.iOOOOMUi 1U77II. UH HI'/6V,_'/.
.10000(5+01 \M''>' >l!i A'iJ ' S, , . . .Ii'.-'/ 4V. 63 ,10000^111 i!4),"6. OH 4U!12,74 U0.27 ,10-001- till 23317, -II 2331i;'.,02 -1,4) , lUOOOtVMIl U6U77. CH U6-7
,, -, , . U6-77.0IIO
13,4'j S3, 12 . ,10000-l'Ut 43U7i'J. OH 431371':,, 000
: tt «!i_K-:ttlit.., 73 62,13 .1000llb.+lll li'bA'Sb. -V li.S44S.00016, ,6 6b,39 ,10UO()I;+II1 -4V/.W. IiH -t' JV.'JOO
014565
Report) 3189,00 Channftl < 2 M8333 8R'8a«pX»T. CP 19263 tnjtr.ttd at 13iUi49 ON FER 3, 19H4E8TD Method i PACKO? 8«q> 8Efl?5 Bubnq/Sflnpi 1/46 Rtl>46Si-width HV/Min Delay Hin-Ar Bunch.. — .5»0 .300 P. 00 20 Avto
He/Hi. H«im.
E+01 BM67R, BB BM67B.130E+01 330813. BB 330B12 810rXU 44?.S1. flfi 44351.500
87859.719
,. m, _.__...__, .... ._—r- uMnnrt Bnii21?411, 8B .181 HI-PTARHL.OR
, ...».V.tn;\>-_BB'.
m.18R547. M,. ?Pl'-TO
BO PP'DDT
Total Are* • 5J968540.' Total Wm." • 37503.500 'PrnrM»ed data filti P?S46 Raw data file. RH546
"" . 014566O » . 'I *3
o0. Samplt Preparation PackageThU ooetlon tadudoo Itw QC/FID chromatogram end QC Screen Data Shoot for IhovoktHM fraction of samples auocMed with thia caw. CompuChem scrwns only thevotaWes fraction; all other fractlona ore prepared as "tow17 samples, and diluted Ifnecooury to bring antlyteg within the calibration ranges for quantltatlori,
014567
t.o
' GC SCREEN DATA SHEET
Laboratory Name Head CompuChem' Case Number_______.gg 3*» '
!,
""SampleID Number
/7Y.T
FractionVOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesD1ox1n
6CDetectable*'
Medium LeveliJo
ScreenhitSf
,, Level or*; 6C/NS "'Analysis**t_
B.
•Answer Yes or No. Ol/l'iRfl••Indicated" for medium level GC/NS analysis. . tf * 1JO°Indlcate'L" for low level GC/HS analysis.
RMPLITU-E x.26 uY-*-cong*
•* iii3. *
O 5S
.« «'19
»Hcm •;
«F« 01
s
12.97
16.23••.?*"<" is.76
, jr*( AM.. ,.
v 0 569
) Reporti 3960.00 Channeli 4 M2333 R35J7Banplti VB 19S5B Tnj-cttd at 8i31i03 ON JAN 31, 1984ZERO Method. HEXA04 8*q> 8EQ43 8ub*q/8anpi i/ 1 Btl> 1Sl-uidth HV/Min Dflav Min-Ar Bunch'.50Q .300 0.06 100 AutoBuPrUnk PwTQ IB-Uvl R«f-BIM . XfiTS Hil:
Actual run tinti 21'.017 ninwtt*atonal > l «olt . • . "Endtd not on baitlint
RT *:;.;?Tr1 ,,, Factor , Arta ..... EA X Nam
.10000E+01 110.
.{OOOOE+01 248.'OOOOE+Ol,: flOddE+Oi, OOOOE+OI.10000F.+D1.10000E+01.10000E+01.10000E+01
_ . ....___... 616-li36. HB . "2.145 ,w,v.I I :J|OOOE+0£ 5735373. "Total Area • 78443760. Total AREA X -.,. 5735373.000PractHtd data file. P4301 Raw data filet R4301
014570
i k t«o \
GC SCREEN DATA SHEET
Laboratory Name Mead CompuChemCase Number
'*i«WIR"
.Sw Mfe..ID Number
£Wt
rts"£i •<
..
. : "';nFractionVOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOA '•B/N/APesticidesDloxln
6C•fittictib}.*:Medium Level
X/i) ""
••„•« ..
... •.**••Wi
f,W
Pat*f.n**|WW-Screent-Sf-fV
. • • ,. .•
...
Levtl or: ••«/!**Analysis**t.
•.
. *',
014571*Ans«r Yes or No. . -"Indicated" for medium level 6C/MS analysis. fc *»
j * Irifllcate'L* for low level GC/MS analysis.
O~
RfJPUITUJE x.25 uV-*»contl* l_nUr««u ;
3 £ 2 £ S ST S S S S 3a Q a 01
•4...n9
pr 6->»Q.
8.11
558US.•On
• OS-o1Sfe
.79
16.22
.«!.••*,
0145728 . f . . . . . . . . . .
IQ \
Report i 3861,00 Channel t 4 0*2333 R35188anpl*>i VB 19559 Tnjncttd at BiSSiOB ON JAN 31, 1984ZERO Mtthodi HF.XA04 8nq> 8EQ43 Bubtq/Banpi 1/2 Btl. 2
.0-Lvj R,f-5T« XRTjf WJljf jgo' lf> ' ' * 1 """1.. ••'
Actual run tine.' ZO.OOB ninuttii
Enatd not on baitline ' ••.U<p."''.'.'1v • , •IV ' "'
RT |TH Factor Area .,;• AREA X Wane
1.00
.- . - ... ._ BB15.22 0.00 .1 IIIE+ll 7185817. 18 ,9
Total ATM • 76948410. Total AREA X • 7185897.000Procected data file. P430? Raw data file. R4302'
014573
00".fi!.l 5
• GC SCREEN DATA SHEET
Laboratory Name Mead ComouChemCase Number________J33.5 '__
*s*«iple .-ID Number.€Ar/?
*)*rtd
•
",, .,.*. „.,
• • ,. .r.
FractionVOAB/N/APesticidesDloxln
VOAB/N/APesticides01 oxl n
VOAB/N/APesticidesDloxln
VOA'B/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
Bp.'!|t'5jl''lfc» **'•»!'-rtecfiflrV'
Medium Level- .rM>*,fc>V|A/O *>••*?*
t. . , . ... .,..
. .,,.!»
l»t» •
.U'•'""h.
Mtl ..iWWidT"ScreenA3/. ?/
t •; *
..
. ••»>.,. .•
*V,..1.
.
,t«VU OfGC/NS
Analysis*'£_
..""7H.-...--
»»•.!«,•, f,f
»•
. ••.•
.
OH574*Answer Yes or No.**Ind1cate"M" for medium level 6C/MS analysis. ;,t IBIndlcate'L" for low level GC/HS analysis. ' *
Oor.fi ii,;
O
=« ?•bS-rt>S
flflPUTUDE x.26 uV-s»conas IfcnUryvu A OA.WO•>
2 S £t S So s «
n w u * 01 m M3 « 5 S •> « B
to
x? , •,V'.'H*W,.'. 'Jrt»V •,r. ltlli»tti-*V)f.?s»^M7«001.2Z NnI 8:s:sen M?»P fw?2'<•
3
:«
..-..«* :w..V' '••'••.ij, "'•6.28
t s?r.55j'; P
' w £» m16.22
2 • "."ti;; . "•"''..' ."*•$
S
014575
fc t«
~~> Rep or 1 1 3862. (I fl Channel i 4 0*2333 R3519'•••' Banpliti VB 19560 Injected at 9 1 19.14 ON JAN 31, 1984
ZERO Htthodi HEXA04 8«qi 8E043 8ubiq/8anpt I/ 3 Btli 3Bl-wldth HV/Hin ' lyin hinj-Ar Bunch'
, iActual run tint. 20.017 Winum'
atonal > 1 valtEnded not on baialint"
ITH .Factor -,. Arta ..;.«, AREA X Na-t
00 .iOOOOE+Oi 123. BB.10000E+01'-" E+01E+gi-•+01
E+01II -69269-6. Hi "9 074I &
Total Arta • 76334128. Total AREA X" 9*6916.000PrictMid data filet P4303 Raw 'data filtt *R03
014576
»«
GC SCREEN DATA SHEET
Laboratory Name Mead CornpuChemCase Number_______<zL3_&2>
._, .
ID Number„Ji>>O
/TS*/
.. ••;.... ,.*i(ii.-«o
•
V.
FractionVOAB/N/APesticidesD1ox1n
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesWoxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOA ,B/N/APesticidesDloxln
VOAB/N/A 'PesticidesDloxln
6C . ..,.Detectable*
Medium LevelAJn
••
.1
tfr.ijMte ...of J^
ScreenLii-tv
...
• •
Iff:
Lavil of-SC/HsAnalysis*4
_
™
'Answer Yes or No.**Ind1cate"M" for medium level GC/MS analysis. il £:Inl1cate"L" for low level GC/MS analysis. "
o ••rrt>8
nnrn luut. A.to uv~»«t.uiiu* tc.iu.ti yew n *..,,W M " * 01 Ol * •«So B s a B B
<B B B 0> B B„ a a « g g a3 a a a a a v• • « < . . .
u
-08
TZ
S•0
•i
?***WM
001
1 8 •»a
r?ail.71
014578?LJ——i , .———,———,———J
o " '"
Report. 3BA3.00 Channeli 4 C*8333 R3520Sanplei W 19561 tnjecttd at 9<43i27 ON JAN 31, 1984ZERO Method. HEXA04 Beqi 8EB43 Subtq/Banpi i/ 4 Btlt 481-width HV/Min Delay Hin-Ar Bunch
.500 .300 0.00 100 Auto
Minutesi > 1 »olt tnot en battlint
RT ITM Factor Arta .t AREA X N«M. •„.'«" i ' ' '9.28 0 00 .iOOOOE+01' ~ O. .IOOOOE+01
13,00 015,78 0 00 .IOOOOE+01
Total Arta • 39123776. Total AREA X • 7707?66.000Procttned data file. P4304 Raw data file. R4304
T.
. 4 _ '?V». .4.
,.,«' -
014579
GC SCREEN DATA SHEET
Laboratory Name Mead ComouChemCase Number
"Sa'mpTe 'ID Number#*&.!
/$STM
, . •. ...".aawFractionVOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesD1ox1n
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
"''betectio'ie*'Medium Level'A/a .*•*••
..
- • -,j
"iW" *
.•.-,
*ty*»*ScreenA-SA P*.
—v fS"
... .....
'<«?'*
..,..,,
... V -.;
iAtjrti ofGC/MS
Analysis**•' L.
.•.•.•.nw'
k " •-"!
0145801 *Answer Yes or No.! "Indicate^* for medium level GC/MS analysis.,> Inllcate'L" for ION level GC/HS analysis. Olr.Qf)
A.CD UT-»«UUIIU» thii , .
U * 01
O
*v
Ql4581r • i . • • • • • • • •
\Q>» 4.8
Report i 3B64,00 Channel. 4 (W.333 R3581Banplei VB 19562 Tnjecttd at 10.07.34 ON JAN 31, 1984ZERO Method i HEXA04 8eq. 8ES43 8ubtiq/8anpi I/ 5 Btlt 5Si-width MV/Mln Djlav Min-Ar Bunch'
.500 .300 .O.Ot 100 Auto8up-Unl< DvT ID-Lu} Rtf-RTH XRTH XDil-f . l«o
Actual run tintV''20.017 ninuttiI > 1 voltnot en baitlint
ITH Factor Area ..;.„.. AREA .X. Nant• • •
Total Arta • 75035600. Total AREA X • 4343794.000Procemed data fil-. P4305 Raw data file. R4305
014582
p
GC SCREEN DATA SHEET
Laboratory Name Head CompuChtmCase Number
ID Number
"**
.,*«*••FractionVOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/N/APesticides•Otoxln""'
VOAB/N/APesticidesDloxln
VOAB/N/APesticidesDloxln
VOAB/K/APesticidesDloxln
VOAB/N/APesticidesDloxln
6CDetectable*Medium Level
_/A "•'
•' ' I
( '
... ./.a...1 .,'••••
Screen1-ZtJV
....
Analysis**L.
••
•814583
| "Answer Yes or No.«*Ind1cate"N" for medium level GC/MS analysis.
.: j IntJlcate'L" for low level GC/MS analysis.
!O
flflPLlTUDE *.25 uV-mono* luuargea *, 00.57.o\1 U A Ml 0V * N
i i
»REss
O S*:
-i a
,vt"t( • ..«h*|»ti.
IP
R<M»rt i 3865.00 Channel' 4 G»P.333 R3522Sanplti VB 19563 Injected at 10.31.40 ON JAN 31, 1984ZERO Method i HF.XA04 Snqi 8EQ43 Bubnq/Sanpi 1/6 Btl. 681-width «V/gin ptljs Hinjjj Bunch
. .«• • . .t',.
Actual run tint. 80.017 ninutttSlonal > 1 voltEnded not tn baitlint
RT :"*!!« Factor Arta AREA X Nan-
O
00 .lOOO.E+Pt
o .iooiiE+oi.lllf- --
I !•i 01
:ilO°O
i
Total Aria • • 7S0271B4. Total AREA X - 3942153.000Proct.ted data file. P4306 Raw data file. R4306
,., . 01.585